2-(Phenylcarbonothioylsulfanyl)acetic acid

The title compound, C9H8O2S2, can be used as a chain transfer agent and may be used to control the behavior of polymerization reactions. O—H⋯O hydrogen bonds of moderate character link the molecules into dimers. In the crystal, the dimers are linked into sheets by C—H⋯O interactions, forming R 4 2(12) and R 2 2(8) edge-fused rings running parallel to [101]. There are no intermolecular interactions involving the S atoms.

[1]  Monica Nordberg,et al.  Pharmacology , 1941, The Indian Medical Gazette.

[2]  C. Tanford Macromolecules , 1994, Nature.

[3]  I. C. Mcneill,et al.  Polymer Chemistry , 1961, Nature.

[4]  不破 博 ケミアブ訪問記 Chemical Abstracts Service , 1963 .

[5]  良二 上田 J. Appl. Cryst.の発刊に際して , 1970 .

[6]  R. Mason Complex Chemistry , 1971, Nature.

[7]  J. Emsley The composition, structure and hydrogen bonding of the β-diketones , 1984 .

[8]  Margaret C. Etter,et al.  Encoding and decoding hydrogen-bond patterns of organic compounds , 1990 .

[9]  M. Nardelli,et al.  PARST95 – an update to PARST: a system of Fortran routines for calculating molecular structure parameters from the results of crystal structure analyses , 1995 .

[10]  G. Giaccone,et al.  Chemotherapy , 1929, Reactions Weekly.

[11]  Louis J. Farrugia,et al.  ORTEP-3 for Windows - a version of ORTEP-III with a Graphical User Interface (GUI) , 1997 .

[12]  Graeme Moad,et al.  Living Radical Polymerization with Reversible Addition−Fragmentation Chain Transfer (RAFT Polymerization) Using Dithiocarbamates as Chain Transfer Agents , 1999 .

[13]  Louis J. Farrugia,et al.  WinGX suite for small-molecule single-crystal crystallography , 1999 .

[14]  F. Allen The Cambridge Structural Database: a quarter of a million crystal structures and rising. , 2002, Acta crystallographica. Section B, Structural science.

[15]  國郎 小笠原,et al.  Chem. Pharm. Bull.(オピニオン) , 2007 .

[16]  Yao-Ren Liang,et al.  Methylene bis(dithiobenzoate) , 2008, Acta crystallographica. Section E, Structure reports online.

[17]  G. Sheldrick A short history of SHELX. , 2008, Acta crystallographica. Section A, Foundations of crystallography.

[18]  R. Rosenfeld Nature , 2009, Otolaryngology--head and neck surgery : official journal of American Academy of Otolaryngology-Head and Neck Surgery.

[19]  Synlett , 2022 .