Crack-healing behavior of Si3N4/SiC ceramics under stress and fatigue strength at the temperature of healing (1000 °C)

Abstract Si 3 N 4 /SiC composite ceramics were sintered and subjected to three-point bending specimens made according to the appropriate JIS standard. A semi-circular surface crack of 100 μm in diameter was made on each specimen. We systematically studied crack-healing behavior, and cyclic and static fatigue strengths at the service temperature (1000 °C) by using three kinds of specimens (smooth, cracked and crack-healed). The main conclusions are as follows: (1) Si 3 N 4 /SiC composite ceramics have the excellent ability to heal a crack at 1000 °C; (2) this sample could heal a crack even under cyclic stress at 1000 °C; (3) a new crack-healing process was proposed. The sample crack-healed at 1000 °C by the process exhibited a sufficient static and cyclic fatigue strength at 1000 °C.

[1]  Kotoji Ando,et al.  A PRELIMINARY STUDY ON CRACK HEALING BEHAVIOUR OF Si3 N4 /SiC COMPOSITE CERAMICS , 1998 .

[2]  F. F. Lange,et al.  Crack Healing by Heat Treatment , 1970 .

[3]  繁美 佐藤,et al.  炭化物粒子分散によるムライトの高強度化に関する研究 : 第2報, 添加SiC粒子径と熱処理の影響 , 1995 .

[4]  M. Chu,et al.  Crack Healing Behavior and High Temperature Strength of Mullite/SiC Composite Ceramics. , 1999 .

[5]  Shigemi Sato,et al.  The Study on Crack Healing Behaviour of Silicon Nitride Ceramics. , 1998 .

[6]  F. Lange,et al.  Healing of Surface Cracks in Polycrystalline Al2O3 , 1970 .

[7]  Shigemi Sato,et al.  Static and cyclic fatigue behaviour of crack-healed Si3N4/SiC composite ceramics , 2001 .

[8]  繁美 佐藤,et al.  炭化物粒子分散によるムライトの高強度化に関する研究 : 第1報,SiCおよびTiC粒子分散の効果 , 1994 .

[9]  Shigemi Sato,et al.  Crack Healing Behaviour and High Temperature Strength of Silicon Nitride Ceramics. , 1999 .

[10]  J. J. Petrovic,et al.  Controlled Surface Flaws in Hot‐Pressed SiC , 1975 .

[11]  Kotoji Ando,et al.  Fatigue strength of crack‐healed Si3N4/SiC composite ceramics , 1999 .

[12]  T. K. Gupta,et al.  Crack Healing and Strengthening of Thermally Shocked Alumina , 1976 .

[13]  Kotoji Ando,et al.  Crack-healing behavior, high temperature and fatigue strength of SiC-reinforced silicon nitride composite , 2000 .

[14]  Sung R. Choi,et al.  Crack healing behavior of hot pressed silicon nitride due to oxidation , 1992 .

[15]  Shigemi Sato,et al.  Strengthening of Mullite by Dispersion of Carbide Ceramics Particles , 1996 .

[16]  W. J. Plumbridge,et al.  High temperature crack annealing effects on fracture toughness of alumina and alumina-SiC composite , 1996 .

[17]  Shigemi Sato,et al.  (Crack-healing+proof test): a new methodology to guarantee the structural integrity of a ceramics component , 2002 .

[18]  Shigemi Sato,et al.  Fatigue Strength Properties of Crack Healed Mullite/SiC Composite Ceramics. , 1999 .

[19]  M. Chu,et al.  Crack healing behavior of silicon carbide ceramics , 2004 .

[20]  Shigemi Sato,et al.  Crack-healing behavior under stress of mullite/silicon carbide ceramics and the resultant fatigue strength , 2004 .