: From the perspective of cultivating innovative talents in the new era, this paper expounds the necessity of reforming the teaching method of basic analytical chemistry experiment. In view of the basic analytical chemistry experiment in college, this paper puts forward the concrete rectification scheme from pre-class preparation, classroom teaching, experimental guidance, after-class discussion and summary to the method of experimental examination at the end of the semester. Compared with the traditional experimental teaching method, the implementation of the new method effectively improves the students’ initiative in learning, and cultivates the students’ solid experimental skills and innovative ability.