High-throughput characterisation of materials by photoluminescence spectroscopy.

An automatic system for high-throughput (HT) characterisation of large libraries of solid materials by photoluminescence spectroscopy is described. The system provides time-resolved transient emission spectra in the microsecond scale and can be employed for characterisation of materials of interest in the fields of catalysis and electroluminescence, amongst others. Here, we present its application to the optimisation of the ship-in-a-bottle synthesis of a novel electroluminescent polymer (PPV) and a photocatalyst (TP+), both encapsulated in large-pore zeolites.

[1]  José M. Serra,et al.  Styrene from toluene by combinatorial catalysis , 2003 .

[2]  J. Grunwaldt,et al.  High-throughput screening under demanding conditions: Cu/ZnO catalysts in high pressure methanol synthesis as an example , 2003 .

[3]  J. M. Serra,et al.  Application of artificial neural networks to combinatorial catalysis: modeling and predicting ODHE catalysts. , 2002, Chemphyschem : a European journal of chemical physics and physical chemistry.

[4]  H. Koinuma,et al.  High-throughput optical characterization for the development of a ZnO-based ultraviolet semiconductor-laser , 2002 .

[5]  B. Ferrer,et al.  Remarkably high electrochemical charge uptake for modified electrodes of polyacetylene molecular wires encapsulated within zeolites and mesoporous MCM-41 aluminosilicate , 2002 .

[6]  J Honerkamp,et al.  High-throughput evaluation of olefin copolymer composition by means of attenuated total reflection Fourier tranform infrared spectroscopy. , 2001, Journal of combinatorial chemistry.

[7]  Claude Mirodatos,et al.  Combinatorial Approaches to Heterogeneous Catalysis: Strategies and Perspectives for Academic Research , 2001 .

[8]  R. Swenson,et al.  Applications of Raman Spectroscopy to Combinatorial Chemistry , 1999 .

[9]  Jandeleit,et al.  Combinatorial Materials Science and Catalysis. , 1999, Angewandte Chemie.

[10]  Howard Turner,et al.  Kombinatorische Materialforschung und Katalyse , 1999 .

[11]  H. García,et al.  2, 4, 6-Triphenylpyrylium ion encapsulated in Y zeolite as photocatalyst. A co-operative contribution of the zeolite host to the photodegradation of 4-chlorophenoxyacetic acid using solar light , 1998 .

[12]  Peter G. Schultz,et al.  A Combinatorial Approach to Materials Discovery , 1995, Science.

[13]  T. Bein,et al.  Encapsulation of polyaniline in zeolite Y and mordenite , 1989 .

[14]  Zhongmin Liu,et al.  High-throughput characterization of heterogeneous catalysts by temperature-programmed analysis method , 2004 .

[15]  H. García,et al.  2,4,6-Triphenylpyrylium ion encapsulated within Y zeolite as photocatalyst for the degradation of methyl parathion , 2000 .

[16]  Donal D. C. Bradley,et al.  Precursor route chemistry and electronic properties of poly(p-phenylenevinylene), poly[(2,5-dimethyl-p-phenylene)vinylene] and poly[(2,5-dimethoxy-p-phenylene)vinylene] , 1992 .

[17]  T. Bein,et al.  ENCAPSULATION OF CONDUCTING POLYMERS WITHIN ZEOLITES , 1990 .