Simple, Portable, and Inexpensive Spectrophotometers for High Schools Lab Activity

A simple, portable and inexpensive spectrophotometer for chemical analysis and laboratory activities is a growing topic of research in chemical education. The purpose of this study was to investigate how academics develop simple, portable and inexpensive spectrophotometers in the chemistry classes. This study used a systematic literature review method. A total of 46 related journal articles from 2009 to 2019 were used as sources for review. Sources of the articles reviewed were mostly obtained from the Journal of Chemical Education. As a guide to the study conducted, three formulations of the problem were used. First, what type of instruments developed. Second, what specific technology used and third, what pedagogical approach used. The results of the study conducted indicate that the UV-Vis instrument is the most developed one. This opens up opportunities for other researchers to develop other types of spectrometry instruments. The use of LED technology as a light source and a smartphone camera as a detector is a currently developing innovation. The development and the use of simple spectrophotometer have been successfully conducted at various levels of education including high school. This proves that simple, portable and inexpensive spectrophotometers can be used and developed at the high school level.

[1]  W. Pomerantz,et al.  Quantifying Protein Concentrations Using Smartphone Colorimetry: A New Method for an Established Test. , 2017, Journal of chemical education.

[2]  H. Floyd Davis,et al.  A Low-Cost Quantitative Absorption Spectrophotometer , 2012 .

[3]  Rodney A. Kreuter,et al.  The Characterization of an Easy-to-Operate Inexpensive Student-Built Fluorimeter , 2011 .

[4]  Anna L. Adams-McNichol,et al.  Accurate, Photoresistor-Based, Student-Built Photometer and Its Application to the Forensic Analysis of Dyes , 2019, Journal of Chemical Education.

[5]  Christopher Hardacre,et al.  Using a Systematic Approach To Develop a Chemistry Course Introducing Students to Instrumental Analysis , 2013 .

[6]  T. Melø,et al.  Demonstrating Basic Properties of Spectroscopy Using a Self-Constructed Combined Fluorimeter and UV-Photometer , 2017 .

[7]  Sulaiman M. Al-Balushi,et al.  The Effectiveness of Interacting with Scientific Animations in Chemistry Using Mobile Devices on Grade 12 Students’ Spatial Ability and Scientific Reasoning Skills , 2016, Journal of Science Education and Technology.

[8]  Martin A. Lema,et al.  Using a homemade spectrophotometer in teaching biosciences , 2002 .

[9]  V. Remcho,et al.  Cost Effective Paper-Based Colorimetric Microfluidic Devices and Mobile Phone Camera Readers for the Classroom , 2015 .

[10]  Ian Pelse,et al.  Using a Homemade Flame Photometer To Measure Sodium Concentration in a Sports Drink , 2013 .

[11]  E. Moraes,et al.  Integrating Mobile Phones into Science Teaching to Help Students Develop a Procedure to Evaluate the Corrosion Rate of Iron in Simulated Seawater. , 2015 .

[12]  C. Haynes,et al.  Quantifying Gold Nanoparticle Concentration in a Dietary Supplement Using Smartphone Colorimetry and Google Applications. , 2016 .

[13]  E. J. Davis,et al.  Project-Based Learning in Undergraduate Environmental Chemistry Laboratory: Using EPA Methods To Guide Student Method Development for Pesticide Quantitation , 2017 .

[14]  Brian Martin,et al.  Developing Tools for Undergraduate Spectroscopy: An Inexpensive Visible Light Spectrometer , 2013 .

[15]  Buchari,et al.  Using Project-Based Learning To Design, Build, and Test Student-Made Photometer by Measuring the Unknown Concentration of Colored Substances , 2018 .

[16]  Thomas S. Kuntzleman,et al.  Teaching Beer’s Law and Absorption Spectrophotometry with a Smart Phone: A Substantially Simplified Protocol , 2016 .

[17]  B. Stankus,et al.  Effective and Inexpensive HPLC Analogue for First-Year Students: Buret Chromatography of Food Dyes in Drinks , 2019, Journal of Chemical Education.

[18]  J. Quattrucci Problem-Based Approach to Teaching Advanced Chemistry Laboratories and Developing Students’ Critical Thinking Skills , 2018 .

[19]  E. Maxwell,et al.  Build Your Own Photometer: A Guided-Inquiry Experiment to Introduce Analytical Instrumentation. , 2016 .

[20]  J. Maslowsky Comparison of the Electromagnetic Spectra of Common Light Sources: A General Chemistry Laboratory Exercise , 2013 .

[21]  D. J. Beussman,et al.  Simulating a Time-of-Flight Mass Spectrometer: A LabView Exercise , 2013 .

[22]  B. S. Hosker Demonstrating Principles of Spectrophotometry by Constructing a Simple, Low-Cost, Functional Spectrophotometer Utilizing the Light Sensor on a Smartphone , 2018 .

[23]  Jocelyn Wishart,et al.  Mobile phone images and video in science teaching and learning , 2014 .

[24]  Robert T Kennedy,et al.  An Inexpensive, Open-Source USB Arduino Data Acquisition Device for Chemical Instrumentation. , 2016, Journal of chemical education.

[25]  B. Place Activity Analysis of Iron in Water Using a Simple LED Spectrophotometer , 2019, Journal of Chemical Education.

[26]  A. Shidiq,et al.  Pre-service chemistry teachers’ attitudes and attributes toward the twenty-first century skills , 2019, Journal of Physics: Conference Series.

[27]  Robert L. McClain,et al.  Construction of a Photometer as an Instructional Tool for Electronics and Instrumentation , 2014 .

[28]  J. Quagliano,et al.  Demystifying Spectroscopy with Secondary Students: Designing and Using a Custom-Built Spectrometer , 2013 .

[29]  D. Thiel,et al.  Using Open-Source, 3D Printable Optical Hardware To Enhance Student Learning in the Instrumental Analysis Laboratory , 2018 .

[30]  Ellen J. Yezierski,et al.  Detecting Art Forgeries: A Problem-Based Raman Spectroscopy Lab , 2014 .

[31]  C. Haynes,et al.  A Fresh Look at the Crystal Violet Lab with Handheld Camera Colorimetry , 2015 .

[32]  R. Verley,et al.  Simple and Inexpensive UV-Photometer Using LEDs as Both Light Source and Detector , 2016 .

[33]  M. H. Torcasio,et al.  Teaching UV–Vis Spectroscopy with a 3D-Printable Smartphone Spectrophotometer , 2016 .

[34]  Agus Setiabudi,et al.  Students’ construction of a simple steam distillation apparatus and development of creative thinking skills: A project-based learning , 2017 .

[35]  E. Maxwell,et al.  Demonstration of the Spectrophotometric Complementary Color Wheel Using LEDs and Indicator Dyes , 2016 .

[36]  Tuck Wah Ng,et al.  Developing and Demonstrating an Augmented Reality Colorimetric Titration Tool. , 2018 .

[37]  A. Nandiyanto,et al.  A simple, rapid analysis, portable, low-cost, and Arduino-based spectrophotometer with white LED as a light source for analyzing solution concentration , 2018 .

[38]  G. Crespo,et al.  Camping Burner-Based Flame Emission Spectrometer for Classroom Demonstrations , 2014 .

[39]  F. Triawan,et al.  TECHNO-ECONOMIC FEASIBILITY STUDY OF LOW-COST AND PORTABLE HOME-MADE SPECTROPHOTOMETER FOR ANALYZING SOLUTION CONCENTRATION , 2019 .

[40]  Daniel Sykes,et al.  Construction and Characterization of a Compact, Portable, Low-Cost Colorimeter for the Chemistry Lab , 2016 .

[41]  R. Verley,et al.  A Simple, Small-Scale Lego Colorimeter with a Light-Emitting Diode (LED) Used as Detector , 2014 .

[42]  Jessica L. Bonjour,et al.  Introducing High School Students to NMR Spectroscopy through Percent Composition Determination Using Low-Field Spectrometers , 2015 .

[43]  Yong Tang,et al.  A Portable Smart-Phone Readout Device for the Detection of Mercury Contamination Based on an Aptamer-Assay Nanosensor , 2016, Sensors.

[44]  Jo-Anne Ferreira,et al.  Approaches to embedding sustainability in teacher education: A synthesis of the literature , 2017 .

[45]  Rodney A. Kreuter,et al.  A Portable, Low-Cost, LED Fluorimeter for Middle School, High School, and Undergraduate Chemistry Labs , 2011 .

[46]  Camilo L. M. Morais,et al.  Low-Cost Method for Quantifying Sodium in Coconut Water and Seawater for the Undergraduate Analytical Chemistry Laboratory: Flame Test, a Mobile Phone Camera, and Image Processing , 2014 .

[47]  M. Vergne,et al.  Escape the Lab: An Interactive Escape-Room Game as a Laboratory Experiment , 2019, Journal of Chemical Education.

[48]  Fumitaka Wakabayashi,et al.  A DVD Spectroscope: A Simple, High-Resolution Classroom Spectroscope , 2006 .

[49]  James P. Grinias,et al.  Use of Augmented Reality in the Instruction of Analytical Instrumentation Design , 2019, Journal of Chemical Education.

[50]  Eric Kehoe,et al.  Introducing Colorimetric Analysis with Camera Phones and Digital Cameras: An Activity for High School or General Chemistry , 2013 .

[51]  Mark V. Wilson,et al.  Authentic Performance in the Instrumental Analysis Laboratory: Building a Visible Spectrophotometer Prototype , 2017 .