Fabrication of copper oxide nanofluid using submerged arc nanoparticle synthesis system (SANSS)

The optimal parameters are found for preparing nanofluid in our submerged arc nanoparticle synthesis system (SANSS) using a copper electrode. A suspended copper oxide nanofluid is thus produced at the current of 8.5–10 A, voltage of 220 V, pulse duration of 12 μs, and dielectric liquid temperature of 2°C. The CuO nanoparticle are characterized by transmission electron microscopy (TEM), field emission scanning electron microscope (FESEM), X-ray diffraction (XRD), electron diffraction pattern (SAD) and electron spectroscopy for chemical analysis (ESCA). The equality volume spherical diameter of the obtained copper oxide particle is 49.1 nm, regular shape and narrow size distribution.

[1]  Rajesh Kumar,et al.  Sonochemical Synthesis and Characterization of Nanometer-Size Transition Metal Oxides from Metal Acetates , 2000 .

[2]  Chii-Ruey Lin,et al.  A Study of Magnetic Field Effect on Nanofluid Stability of CuO , 2004 .

[3]  Mukund R. Patel,et al.  Theoretical models of the electrical discharge machining process. III. The variable mass, cylindrical plasma model , 1993 .

[4]  G. Aeppli,et al.  Resonance as a measure of pairing correlations in the high-T c superconductor YBa2Cu3O6.6 , 2000, Nature.

[5]  Wei Ji,et al.  PREPARATION AND CHARACTERIZATION OF CUO NANOCRYSTALS , 1999 .

[6]  J. Goschnick,et al.  CuO catalytic membrane as selectivity trimmer for metal oxide gas sensors , 2000 .

[7]  A. Vertegel,et al.  Complexes of Cu(II) with polyvinyl alcohol as precursors for the preparation of CuO/SiO2 nanocomposites , 2000 .

[8]  Mukund R. Patel,et al.  Theoretical models of the electrical discharge machining process. II. The anode erosion model , 1989 .

[9]  Sun Qi,et al.  A novel process for preparation of a Cu/ZnO/Al2O3 ultrafine catalyst for methanol synthesis from CO2 + H2: comparison of various preparation methods , 1996 .

[10]  Congkang Xu,et al.  Preparation and characterization of CuO nanorods by thermal decomposition of CuC2O4 precursor , 2002 .

[11]  Ho Chang,et al.  Development of Pressure Control Technique of An Arc-Submerged Nanoparticle Synthesis System (ASNSS) for Copper Nanoparticle Fabrication , 2003 .

[12]  T. Shripathi,et al.  Quantum size effects in CuO nanoparticles , 2000 .

[13]  T. Maruyama Copper oxide thin films prepared by chemical vapor deposition from copper dipivaloylmethanate , 1998 .