Analysis of deformation behavior and workability of advanced 9Cr-Nb-V ferritic heat resistant steels

Abstract Hot compression tests were carried out on 9Cr–Nb–V heat resistant steels in the temperature range of 600–1200 °C and the strain rate range of 10−2–100 s−1 to study their deformation characteristics. The full recrystallization temperature and the carbon-free bainite phase transformation temperature were determined by the slope-change points in the curve of mean flow stress versus the inverse of temperature. The parameters of the constitutive equation for the experimental steels were calculated, including the stress exponent and the activation energy. The lower carbon content in steel would increase the fraction of precipitates by increasing the volume of dynamic strain-induced (DSIT) ferrite during deformation. The ln(ec) versus ln(Z) and the ln(σc) versus ln(Z) plots for both steels have similar trends. The efficiency of power dissipation maps with instability maps merged together show excellent workability from the strain of 0.05 to 0.6. The microstructure of the experimental steels was fully recrystallized upon deformation at low Z value owing to the dynamic recrystallization (DRX), and exhibited a necklace structure under the condition of 1050 °C/0.1 s−1 due to the suppression of the secondary flow of DRX. However, there were barely any DRX grains but elongated pancake grains under the condition of 1000 °C/1 s−1 because of the suppression of the metadynamic recrystallization (MDRX).

[1]  Wei Yan,et al.  Hot deformation characteristics of a nitride strengthened martensitic heat resistant steel , 2014 .

[2]  Seung-Chan Hong,et al.  Influence of deformation induced ferrite transformation on grain refinement of dual phase steel , 2002 .

[3]  T. Charlton Progress in Solid Mechanics , 1962, Nature.

[4]  X. L. He,et al.  Nb(C, N) Precipitation and Austenite Recrystallization , 1992, Metallurgical and Materials Transactions A.

[5]  P. Wray Onset of recrystallization during the tensile deformation of austenitic iron at intermediate strain rates , 1975 .

[6]  J. Poirier Plasticité à haute température des solides cristallins , 1976 .

[7]  Kamran Dehghani,et al.  Hot working behavior of 2205 austenite–ferrite duplex stainless steel characterized by constitutive equations and processing maps , 2011 .

[8]  J. Jonas,et al.  Measurement and modelling of the effects of precipitation on recrystallization under multipass deformation conditions , 1993 .

[9]  J. M. Rodriguez-Ibabe,et al.  Transition between static and metadynamic recrystallization kinetics in coarse Nb microalloyed austenite , 2003 .

[10]  H. J. McQueen,et al.  Constitutive analysis in hot working , 2002 .

[11]  J. M. Rodriguez-Ibabe,et al.  Dynamic recrystallization behavior covering a wide austenite grain size range in Nb and Nb–Ti microalloyed steels , 2003 .

[12]  C. M. Sellars,et al.  Mechanism and kinetics of strain induced precipitation of Nb(C,N) in austenite , 1992 .

[13]  Hyun Seon Hong,et al.  Effects of Nb on strain induced ferrite transformation in C–Mn steel , 2003 .

[14]  John J. Jonas,et al.  A one-parameter approach to determining the critical conditions for the initiation of dynamic recrystallization , 1996 .

[15]  H. Mcqueen,et al.  Hot working characteristics of steels in austenitic state , 1995 .

[16]  Wei Sha,et al.  The impact toughness of a nitride-strengthened martensitic heat resistant steel , 2012 .