Improved accuracy of 15N–1H scalar and residual dipolar couplings from gradient-enhanced IPAP-HSQC experiments on protonated proteins

[1]  A. Bax,et al.  NMR determination of amide N-H equilibrium bond length from concerted dipolar coupling measurements. , 2008, Journal of the American Chemical Society.

[2]  Antonio Rosato,et al.  Faculty Opinions recommendation of Recognition dynamics up to microseconds revealed from an RDC-derived ubiquitin ensemble in solution. , 2008 .

[3]  Oliver F. Lange,et al.  Self-consistent residual dipolar coupling based model-free analysis for the robust determination of nanosecond to microsecond protein dynamics , 2008, Journal of biomolecular NMR.

[4]  Ad Bax,et al.  Simultaneous NMR study of protein structure and dynamics using conservative mutagenesis. , 2008, The journal of physical chemistry. B.

[5]  A. Bax,et al.  Modulating protein alignment in a liquid-crystalline medium through conservative mutagenesis. , 2007, Journal of the American Chemical Society.

[6]  A. Bax,et al.  Mixed-time parallel evolution in multiple quantum NMR experiments: sensitivity and resolution enhancement in heteronuclear NMR , 2007, Journal of biomolecular NMR.

[7]  G. Bouvignies,et al.  Simultaneous determination of protein backbone structure and dynamics from residual dipolar couplings. , 2006, Journal of the American Chemical Society.

[8]  N. Tjandra,et al.  On the accurate measurement of amide one-bond 15N-1H couplings in proteins: effects of cross-correlated relaxation, selective pulses and dynamic frequency shifts. , 2006, Journal of magnetic resonance.

[9]  N. Tjandra,et al.  Interference between Cross-correlated Relaxation and the Measurement of Scalar and Dipolar Couplings by Quantitative J , 2006, Journal of biomolecular NMR.

[10]  Ke Ruan,et al.  NMR residual dipolar couplings as probes of biomolecular dynamics. , 2006, Chemical reviews.

[11]  Jens Meiler,et al.  A Thorough Dynamic Interpretation of Residual Dipolar Couplings in Ubiquitin , 2006, Journal of biomolecular NMR.

[12]  Rafael Brüschweiler,et al.  Identification of slow correlated motions in proteins using residual dipolar and hydrogen-bond scalar couplings. , 2005, Proceedings of the National Academy of Sciences of the United States of America.

[13]  D. Fushman,et al.  Characterization of the overall and local dynamics of a protein with intermediate rotational anisotropy: Differentiating between conformational exchange and anisotropic diffusion in the B3 domain of protein G , 2003, Journal of biomolecular NMR.

[14]  Rafael Brüschweiler,et al.  Self-consistency analysis of dipolar couplings in multiple alignments of ubiquitin. , 2003, Journal of the American Chemical Society.

[15]  Rafael Brüschweiler,et al.  New approaches to the dynamic interpretation and prediction of NMR relaxation data from proteins. , 2003, Current opinion in structural biology.

[16]  J. R. Tolman A novel approach to the retrieval of structural and dynamic information from residual dipolar couplings using several oriented media in biomolecular NMR spectroscopy. , 2002, Journal of the American Chemical Society.

[17]  G. Bodenhausen,et al.  Accurate measurement of residual dipolar couplings in anisotropic phase , 2002, Journal of biomolecular NMR.

[18]  A. Bax,et al.  Evaluation of uncertainty in alignment tensors obtained from dipolar couplings , 2002, Journal of biomolecular NMR.

[19]  Jens Meiler,et al.  Model-free analysis of protein backbone motion from residual dipolar couplings. , 2002, Journal of the American Chemical Society.

[20]  J H Prestegard,et al.  NMR structures of biomolecules using field oriented media and residual dipolar couplings , 2000, Quarterly Reviews of Biophysics.

[21]  L. Mueller,et al.  Tunable alignment of macromolecules by filamentous phage yields dipolar coupling interactions , 1998, Nature Structural Biology.

[22]  F. Delaglio,et al.  Measurement of dipolar couplings for methylene and methyl sites in weakly oriented macromolecules and their use in structure determination. , 1998, Journal of magnetic resonance.

[23]  A. Bax,et al.  Measurement of J and dipolar couplings from simplified two-dimensional NMR spectra. , 1998, Journal of magnetic resonance.

[24]  T. Schulte-Herbrüggen,et al.  SPIN-STATE-SELECTIVE POLARIZATION OR EXCITATION FOR SIMULTANEOUS E.COSY-TYPE MEASUREMENT OF 3J(C', HALPHA ) AND 3J(HN, HALPHA ) COUPLING CONSTANTS WIT H ENHANCED SENSITIVITY AND RESOLUTION IN MULTIDIMENSIONAL NMR SPECTROSCOPY OF 13C, 15N-LABELED PROTEINS , 1998 .

[25]  G. Marius Clore,et al.  Use of dipolar 1H–15N and 1H–13C couplings in the structure determination of magnetically oriented macromolecules in solution , 1997, Nature Structural Biology.

[26]  A. Bax,et al.  Measurement of dipolar contributions to 1JCH splittings from magnetic-field dependence of J modulation in two-dimensional NMR spectra. , 1997, Journal of magnetic resonance.

[27]  Ad Bax,et al.  Magnetic Field Dependence of Nitrogen−Proton J Splittings in 15N-Enriched Human Ubiquitin Resulting from Relaxation Interference and Residual Dipolar Coupling , 1996 .

[28]  A. Bax,et al.  Determination of the Backbone Dihedral Angles φ in Human Ubiquitin from Reparametrized Empirical Karplus Equations , 1996 .

[29]  S. Grzesiek,et al.  NMRPipe: A multidimensional spectral processing system based on UNIX pipes , 1995, Journal of biomolecular NMR.

[30]  J H Prestegard,et al.  Nuclear magnetic dipole interactions in field-oriented proteins: information for structure determination in solution. , 1995, Proceedings of the National Academy of Sciences of the United States of America.

[31]  A. Bax,et al.  Reparametrization of the Karplus Relation for 3J(H.alpha.-N) and 3J(HN-C') in Peptides from Uniformly 13C/15N-Enriched Human Ubiquitin , 1995 .

[32]  S. Grzesiek,et al.  The Importance of Not Saturating H2o in Protein NMR : application to Sensitivity Enhancement and Noe Measurements , 1993 .

[33]  Paul A. Keifer,et al.  Pure absorption gradient enhanced heteronuclear single quantum correlation spectroscopy with improved sensitivity , 1992 .

[34]  A. Bax,et al.  An alternative 3D NMR technique for correlating backbone 15N with side chain Hβ resonances in larger proteins , 1991 .

[35]  P. Schmieder,et al.  A new 1H15N13C triple-resonance experiment for sequential assignments and measuring homonuclear HαHN vicinal coupling constants in polypeptides , 1991 .

[36]  Ray Freeman,et al.  Band-selective radiofrequency pulses , 1991 .

[37]  R. R. Ernst,et al.  Correlation of connected transitions by two‐dimensional NMR spectroscopy , 1986 .

[38]  R. R. Ernst,et al.  Two-dimensional correlation of connected NMR transitions , 1985 .

[39]  M. Goldman,et al.  Interference effects in the relaxation of a pair of unlike spin-1/2 nuclei , 1984 .

[40]  M. S. Silver,et al.  Highly selective {π}/{2} and π pulse generation , 1984 .

[41]  C. Gayathri,et al.  Dipolar magnetic field effects in NMR spectra of liquids , 1982 .

[42]  Daiwen Yang,et al.  A Sensitivity-Enhanced Method for Measuring Heteronuclear Long-Range Coupling Constants from the Displacement of Signals in Two 1D Subspectra , 1996 .

[43]  Robin K. Harris,et al.  Encyclopedia of nuclear magnetic resonance , 1996 .

[44]  G. Montelione,et al.  Accurate measurements of homonuclear HN-H.alpha. coupling constants in polypeptides using heteronuclear 2D NMR experiments , 1989 .

[45]  V. Bystrov Spin—spin coupling and the conformational states of peptide systems , 1976 .