Direct Observation and Characterization of Effect of Preparing Condition on Particle Assembling State in Suspension

Particle assembling state in suspensions prepared by different ways was numerically characterized by direct observation method. The aqueous suspensions of alumina powder were prepared by ultrasonication and ball milling. The particle assembling state was characterized by settling test and particle size measurement in addition to the direct observation. From the comparison, the particle images in a suspension getting by the direct observation method can much more distinguish coarse aggregates from primary particles than the other ways. And the black and whiteness of the particle images were classified into 256 steps. The mean values and standard deviations of the black and whiteness distributions were calculated. The variation coefficient determined by the standard deviation over the mean value can show the existence of coarse aggregates that were not ground or re-aggregated.

[1]  J. Tsubaki,et al.  Direct Observation and Characterization of Particle Assembling State in Suspension , 2011 .

[2]  J. Tsubaki,et al.  Effects of sintering additives on dispersion properties of Al2O3 slurry containing polyacrylic acid dispersant , 2011 .

[3]  K. Uematsu,et al.  Correlation between slurry properties and structures and properties of granules , 2010 .

[4]  J. Tsubaki,et al.  Effects of Dispersant Dosage on Settling Behavior , 2010 .

[5]  Suresh C. Sharma,et al.  Novel Coagulation Method for Direct Coagulation Casting of Aqueous Alumina Slurries Prepared Using a Poly(Acrylate) Dispersant , 2008 .

[6]  I. Santacruz,et al.  Rheological Characterization and Coagulation Casting of Al2O3–Nano Zirconia Suspensions , 2007 .

[7]  Naoki Omura,et al.  Fabrication of Stable Al2O3 Slurries and Dense Green Bodies Using Wet Jet Milling , 2006 .

[8]  K. Watari,et al.  Slip casting of Al2O3 slurries prepared by wet jet milling , 2005 .

[9]  J. Tsubaki,et al.  Effects of Solid Concentration and Dispersant Dosage on Sedimentation Behavior , 2004 .

[10]  Naoki Itoh,et al.  Effect of Small Size Beads on Dispersion of Nanometer-Sized Silica Particle by Wet Beads Mill Process , 2004 .

[11]  J. Tsubaki,et al.  Analysis of Sedimentation and Settling Process of Dense Alumina Slurries by Hydrostatic Pressure Measurement , 2003 .

[12]  K. Mohanty,et al.  Batch gravitational sedimentation of slurries. , 2002, Journal of colloid and interface science.

[13]  F. Lange,et al.  Effect of Silica Nanoparticle Size on the Stability of Alumina/Silica Suspensions , 2001 .

[14]  F. Saito,et al.  Effect of grinding on synthesis of MgAl2O4 spinel from a powder mixture of Mg(OH)2 and Al(OH)3 , 2000 .

[15]  Q. Zeng,et al.  Influence of milling conditions on magnetic properties of Nd(Fe,Mo)12Nx compounds , 1999 .

[16]  Q. Zhao,et al.  The Grinding Equilibrium Size of In-Water Grinding of Silica Sand by a Planetary Ball Mill. , 1991 .