Non-Destructive Testing of Archaeological Findings by Grating-Based X-Ray Phase-Contrast and Dark-Field Imaging

The analysis of archaeological findings reveals the remaining secrets of human history. However, it is a challenging task to investigate and simultaneously preserve the unique remains. Available non-destructive examination methods are limited and often insufficient. Thus, we considered X-ray grating interferometry as a non-destructive and advanced X-ray imaging method to retrieve more information about archaeological findings. In addition to the conventional attenuation image, the differential phase and the dark-field image are obtained. We studied the potential of the scattering-sensitive dark-field and the phase-shift sensitive differential phase image to analyse archaeological findings. Hereby, the focus lies on organic remnants. Usually, the organic materials have vanished due to decomposition processes, but the structures are often preserved by mineralisation and penetration of corrosion products. We proved that the combination of the attenuation and the dark-field image in particular, enables a separation of structural properties for fabric remnants. Furthermore, we achieved promising results for the reconstruction of sub-pixel sized fibre orientations of woven fabric remnants by employing the directional dark-field imaging method. We conclude from our results that a further application of X-ray dark-field imaging on wet organic findings and on the distinction of different types of organic remnants at archaeological findings is promising.

[1]  A. Ritter,et al.  Simulation framework for coherent and incoherent X-ray imaging and its application in Talbot-Lau dark-field imaging. , 2014, Optics express.

[2]  Richard J. Fitzgerald,et al.  Phase‐Sensitive X‐Ray Imaging , 2000 .

[3]  T J Suleski,et al.  Generation of Lohmann images from binary-phase Talbot array illuminators. , 1997, Applied optics.

[4]  Franz Pfeiffer,et al.  X-ray tensor tomography , 2014 .

[5]  Franz Pfeiffer,et al.  X-ray Dark-Field Vector Radiography—A Novel Technique for Osteoporosis Imaging , 2015, Journal of computer assisted tomography.

[6]  A. Momose,et al.  On the origin of visibility contrast in x-ray Talbot interferometry. , 2010, Optics express.

[7]  Georg Pelzer,et al.  Optimization procedure for a Talbot-Lau x-ray phase-contrast imaging system , 2017 .

[8]  Franz Pfeiffer,et al.  Inverse geometry for grating-based x-ray phase-contrast imaging , 2009 .

[9]  Franz Pfeiffer,et al.  X-ray phase imaging with a grating interferometer. , 2005, Optics express.

[10]  Nikolay Kardjilov,et al.  Wavelength‐dispersive dark‐field contrast: micrometre structure resolution in neutron imaging with gratings , 2016 .

[11]  O. Bunk,et al.  Phase retrieval and differential phase-contrast imaging with low-brilliance X-ray sources , 2006 .

[12]  Franz Pfeiffer,et al.  Nondestructive characterization of fiber orientation in short fiber reinforced polymer composites with X-ray vector radiography , 2017 .

[13]  Franco Casali,et al.  Chapter 2 X-ray and neutron digital radiography and computed tomography for cultural heritage , 2006 .

[14]  Andreas Fehringer,et al.  Constrained X-ray tensor tomography reconstruction. , 2015, Optics express.

[15]  Thilo Michel,et al.  Reconstruction of scalar and vectorial components in X-ray dark-field tomography , 2014, Proceedings of the National Academy of Sciences.

[16]  Franz Pfeiffer,et al.  Quantitative x-ray dark-field computed tomography , 2010, Physics in medicine and biology.

[17]  J. Schulz,et al.  Deep X-Ray Lithography , 2015 .

[18]  Atsushi Momose,et al.  Effect of beam hardening on a visibility-contrast image obtained by X-ray grating interferometry. , 2015, Optics express.

[19]  Atsushi Momose,et al.  Effects of unresolvable edges in grating-based X-ray differential phase imaging. , 2015, Optics express.

[20]  Y. Nesterets,et al.  On the origins of decoherence and extinction contrast in phase-contrast imaging , 2008 .

[21]  M. P. Morigi,et al.  Application of X-ray Computed Tomography to Cultural Heritage diagnostics , 2010 .

[22]  Franz Pfeiffer,et al.  Six dimensional X-ray Tensor Tomography with a compact laboratory setup , 2016 .

[23]  Timm Weitkamp,et al.  X-ray vector radiography for bone micro-architecture diagnostics , 2012, Physics in medicine and biology.

[24]  T. Johnson,et al.  Dual-energy CT: general principles. , 2012, AJR. American journal of roentgenology.

[25]  Urs Sennhauser,et al.  Sensing small angle scattering with an X-ray grating interferometer , 2010, IEEE Nuclear Science Symposuim & Medical Imaging Conference.

[26]  Franz Pfeiffer,et al.  Directional x-ray dark-field imaging , 2010, Physics in medicine and biology.

[27]  Simon Zabler,et al.  Projection angle dependence in grating-based X-ray dark-field imaging of ordered structures. , 2013, Optics express.

[28]  Marco Stampanoni,et al.  Quantitative x-ray radiography using grating interferometry: a feasibility study , 2013, Physics in medicine and biology.

[29]  Georg Pelzer,et al.  A beam hardening and dispersion correction for x-ray dark-field radiography. , 2016, Medical physics.

[30]  Urs Sennhauser,et al.  Sub-pixel porosity revealed by x-ray scatter dark field imaging , 2011 .

[31]  O. Bunk,et al.  Hard-X-ray dark-field imaging using a grating interferometer. , 2008, Nature materials.

[32]  Franz Pfeiffer,et al.  Correlation of X-Ray Vector Radiography to Bone Micro-Architecture , 2014, Scientific Reports.

[33]  Johann Kastner,et al.  Laminate fibre structure characterisation of carbon fibre-reinforced polymers by X-ray scatter dark field imaging with a grating interferometer , 2013 .

[34]  Manfred Schreiner,et al.  X‐ray fluorescence spectrometry in art and archaeology , 2000 .

[35]  Franz Pfeiffer,et al.  Improved Diagnostics by Assessing the Micromorphology of Breast Calcifications via X-Ray Dark-Field Radiography , 2016, Scientific Reports.

[36]  Franz Pfeiffer,et al.  Directional x-ray dark-field imaging of strongly ordered systems , 2010 .

[37]  Claus Urban,et al.  Dual energy phase contrast x-ray imaging with Talbot-Lau interferometer , 2010 .

[38]  尚弘 島影 National Institute of Standards and Technologyにおける超伝導研究及び生活 , 2001 .

[39]  Victor Arrizón,et al.  Binary phase grating for array generation at 1/16 of Talbot length , 1995 .

[40]  Alex Dommann,et al.  Orientation-selective X-ray dark field imaging of ordered systems , 2012 .