Influence of temperature gradient and growth rate on the mechanical properties of directionally solidified Sn–3.5 wt% Ag eutectic solder

The Sn–3.5 wt% Ag eutectic alloy was directionally solidified upward with a constant growth rate (V = 16.5 μm/s) at different temperature gradients (G = 1.43–4.28 K/mm) and with a constant temperature gradient (G = 3.93 K/mm) at different growth rates (V = 8.3–500 μm/s) in a Bridgman-type directional solidification furnace. The rod spacings (longitudinal section, λL and transverse section, λT) and mechanical properties (microhardness, HV and ultimate tensile strength, σUTS) of Sn–3.5 wt% Ag eutectic alloy were measured. The dependency of the microhardness, ultimate tensile strength on the temperature gradient, growth rate and rod spacings were determined. According to experimental results, the microhardness and ultimate tensile strength of the solidified samples increase with increasing G and V, but decrease with the increasing the rod spacing.

[1]  A. Fawzy Effect of Zn addition, strain rate and deformation temperature on the tensile properties of Sn–3.3 wt.% Ag solder alloy , 2007 .

[2]  R. Smith,et al.  The hardness of Al-Si eutectic alloys , 1979 .

[3]  Hwa-Teng Lee,et al.  Influence of Lanthanum Additions on the Microstructure and Microhardness of Sn-3.5Ag Solder , 2009 .

[4]  E. Çadırlı,et al.  Variation of microindentation hardness with solidification and microstructure parameters in the Al based alloys , 2008 .

[5]  Morten Mattrup Smedskjær,et al.  Effect of thermal history and chemical composition on hardness of silicate glasses , 2010 .

[6]  A. Kumar,et al.  Composition dependence of thermal stability, micro-hardness and compactness in glassy Se90In10−xGex alloys , 2009 .

[7]  R. Elliott,et al.  Eutectic spacing selection in Al–Cu system , 1994 .

[8]  J. Glazer Microstructure and mechanical properties of Pb-free solder alloys for low-cost electronic assembly: A review , 1994 .

[9]  A. Telli,et al.  Effect of antimony additions on hardness and tensile properties of directionally solidified Al–Si eutectic alloy , 1988 .

[10]  R. Wu,et al.  Effects of Cu addition on the microstructure and hardness of Mg–5Li–3Al–2Zn alloy , 2010 .

[11]  Amauri Garcia,et al.  Design of mechanical properties of a Zn27Al alloy based on microstructure dendritic array spacing , 2007 .

[12]  Sungho Jin,et al.  New, lead-free solders , 1994 .

[13]  K. S. Kim,et al.  Effects of cooling speed on microstructure and tensile properties of Sn–Ag–Cu alloys , 2002 .

[14]  Ikuo Shohji,et al.  Tensile properties of Sn–Ag based lead-free solders and strain rate sensitivity , 2004 .

[15]  E. Hall,et al.  The Deformation and Ageing of Mild Steel: III Discussion of Results , 1951 .

[16]  M. Mccormack,et al.  A lower-melting-point solder alloy for surface mounts , 1996 .

[17]  Fu Guo,et al.  Evaluation of creep behavior of near-eutectic Sn–Ag solders containing small amount of alloy additions , 2003 .

[18]  M. Mahdy,et al.  Some mechanical properties of Sn–3.5 Ag eutectic alloy at different temperatures , 2004 .

[19]  M. Amagai A study of nanoparticles in Sn-Ag based lead free solders , 2008 .

[20]  P. Geffroy,et al.  Microstructural evolution and mechanical properties of SnAgCu alloys , 2006 .

[21]  F. Vnuk,et al.  Mechanical properties of the Sn-Zn eutectic alloys , 1980 .

[22]  Leon M Keer,et al.  Energy-Based Micromechanics Analysis on Fatigue Crack Propagation Behavior in Sn-Ag Eutectic Solder , 2008 .

[23]  G. R. Edwards,et al.  Microstructural control in lead alloys for storage battery application , 1975 .

[24]  Sungho Jin,et al.  New Pb‐free solder alloy with superior mechanical properties , 1993 .

[25]  Chun-ming Liu,et al.  Effects of different tempers on precipitation hardening of 6000 series aluminium alloys , 2007 .

[26]  O. Uzun,et al.  Effect of growth rate and lamellar spacing on microhardness in the directionally solidified Pb-Cd, Sn-Zn and Bi-Cd eutectic alloys , 2004 .

[27]  Chen Wei,et al.  Effects of cooling rates on microstructure and microhardness of lead-free Sn-3.5% Ag solders , 2006 .

[28]  J. Heinrich,et al.  Permeability for cross flow through columnar-dendritic alloys , 1995 .

[29]  R. Elliott,et al.  Hardness and mechanical property relationships in directionally solidified aluminium-silicon eutectic alloys with different silicon morphologies , 1993, Journal of Materials Science.

[30]  Z. Xia,et al.  Effects of nano-structured particles on microstructure and microhardness of Sn–Ag solder alloy , 2010 .

[31]  Da-Yuan Shih,et al.  An Investigation of Microstructure and Microhardness of Sn-Cu and Sn-Ag Solders as Functions of Alloy Composition and Cooling Rate , 2009 .

[32]  I. Anderson Development of Sn–Ag–Cu and Sn–Ag–Cu–X alloys for Pb-free electronic solder applications , 2006 .

[33]  Toshio Narita,et al.  The effect of strain rate and temperature on the tensile properties of Sn–3.5Ag solder , 2005 .

[34]  F. Vnuk,et al.  Mechanical properties of Sn-Ag3Sn alloys , 1983 .

[35]  Amauri Garcia,et al.  Modeling dendritic structure and mechanical properties of Zn–Al alloys as a function of solidification conditions , 2002 .

[36]  Mustafa Kamal,et al.  Effect of Rapid Solidification on Structure and Properties of Some Lead-Free Solder Alloys , 2006 .

[37]  Lawrence H. Bennett,et al.  Binary alloy phase diagrams , 1986 .

[38]  S. Nai,et al.  Reinforcements at nanometer length scale and the electrical resistivity of lead-free solders , 2009 .

[39]  W. J. Plumbridge,et al.  Effects of strain rate and temperature on the stress–strain response of solder alloys , 1999 .

[40]  A. Ülgen,et al.  Effect of the temperature gradient, growth rate, and the interflake spacing on the microhardness in the directionally solidified Al-Si eutectic alloy , 2003 .

[41]  D. R. Poirier,et al.  Permeability for flow parallel to primary dendrite arms , 1992 .

[43]  E. Gouda,et al.  Effect of zinc additions on structure and properties of Sn–Ag eutectic lead-free solder alloy , 2008 .