The study utilized thermophoresis, the directed motion of molecules in a temperature gradient to quantify DNA and proteins for point-of-care applications. Because the direction and speed of thermophoretic motion is dependent on the size, charge, and conformation of the molecules, the binding between molecules can induce changes in their thermophoretic motion. To quantify biomolecules using thermophoresis, we mixed fluorescently-labeled capture probes with samples and then used an infrared laser to create a temperature gradient in the solution. By adding a small fraction of polymers to the buffer solution, we accumulated the fluorescent probes in a temperature gradient using the thermophoretic effects. The thermophoretic motion of the fluorescent probes significantly changed as the target molecules bind to the specially designed capture probes. Consequently, the level of the thermophoretic accumulation, which was determined by the spatial distribution of fluorescent probes, could be used to quantify molecules. This method functioned well even when the buffer contained 10% serum, which suggested that the detection was resistant to the interferences from the molecules in serum. The thermophoresis-based detection method developed in this study only requires a laser and an epi-fluorescence microscope during the detection. Unlike many other commonly seen biosensing methods, quantifying molecules using thermophoresis does not need any fluid channels or pumps for washing away unbound molecules during the detection process. In addition, the detection does not rely on any micro- or nanofabricated chips. In short, this thermophoresis-based biosensing method can be a simple, robust, and sensitive method for quantifying proteins and DNA.
[1]
Dieter Braun,et al.
Protein-binding assays in biological liquids using microscale thermophoresis.
,
2010,
Nature communications.
[2]
Dieter Braun,et al.
Direct detection of antibody concentration and affinity in human serum using microscale thermophoresis.
,
2012,
Analytical chemistry.
[3]
A. Libchaber,et al.
Thermal separation: interplay between the Soret effect and entropic force gradient.
,
2011,
Physical review letters.
[4]
Dieter Braun,et al.
Trapping of DNA by thermophoretic depletion and convection.
,
2002,
Physical review letters.
[5]
T. Tlusty,et al.
Effects of long DNA folding and small RNA stem–loop in thermophoresis
,
2012,
Proceedings of the National Academy of Sciences.
[6]
Hong-Ren Jiang,et al.
Manipulation of colloids by a nonequilibrium depletion force in a temperature gradient.
,
2009,
Physical review letters.
[7]
Dieter Braun,et al.
Why molecules move along a temperature gradient
,
2006,
Proceedings of the National Academy of Sciences.
[8]
Roberto Piazza,et al.
Thermophoresis: moving particles with thermal gradients
,
2008
.
[9]
Dieter Braun,et al.
Label-Free Microscale Thermophoresis Discriminates Sites and Affinity of Protein–Ligand Binding
,
2012,
Angewandte Chemie.