Crystallography of Fatigue Crack Initiation and Growth in Fully Lamellar Ti-6Al-4V

Fatigue crack initiation in titanium alloys is typically accompanied by the formation of planar, faceted features on the fracture surface. In the present study, quantitative tilt fractography, electron backscatter diffraction (EBSD), and the focused ion beam (FIB) have been used to provide a direct link between facet topography and the underlying microstructure, including the crystallographic orientation. In contrast to previous studies, which have focused mainly on the α-phase crystal orientation and the spatial orientation of the facets, the present analysis concentrates on the features that lie in the plane of the facet and how they relate to the underlying constituent phases and their crystallographic orientations. In addition, due to the anisotropic deformation behavior of the three basal slip systems, the orientation of the β phase as it relates to facet crystallography was investigated for the first time. The implication of the β-phase orientation on fatigue crack initiation was discussed in terms of its effect on slip behavior in lamellar microstructures. The effect of the local crystallographic orientation on fatigue crack initiation was also investigated by studying cracks that initiated naturally in the earliest stages of growth, which were revealed by FIB milling. The results indicate that boundaries that are crystallographically suited for slip transfer tend to initiate fatigue cracks. Several observations on the effect of the crystallographic orientation on the propagation of long fatigue cracks were also reported.

[1]  W. G. Burgers On the process of transition of the cubic-body-centered modification into the hexagonal-close-packed modification of zirconium , 1934 .

[2]  J. Nye Physical Properties of Crystals: Their Representation by Tensors and Matrices , 1957 .

[3]  R. Pelloux,et al.  Electron Fractography—A Tool for the Study of Micromechanisms of Fracturing Processes , 1965 .

[4]  A. Bowen The influence of crystallographic orientation on fatigue crack growth in strongly textured Ti6A14V , 1975 .

[5]  J. Chesnutt,et al.  Fracture topography—microstructure correlations in the SEM , 1977 .

[6]  A. Thompson,et al.  Influence of Metallurgical Factors on the Fatigue Crack Growth Rate in Alpha-Beta Titanium Alloys. , 1978 .

[7]  D. Eylon Fatigue crack initiation in hot isostatically pressed Ti-6Al-4V castings , 1979 .

[8]  K. Chan,et al.  Deformation of an alloy with a lamellar microstructure: experimental behavior of individual widmanstatten colonies of an α-β titanium alloy , 1980 .

[9]  U. Dahmen Orientation relationships in precipitation systems , 1982 .

[10]  D. Koss,et al.  Stage I fatigue crack propagation in a titanium alloy , 1988 .

[11]  J. Weertman,et al.  Determination of the orientation of CuBi grain boundary facets using a photogrammetric technique , 1990 .

[12]  S. Suresh Fatigue of materials , 1991 .

[13]  R. H. Wagoner,et al.  On the criteria for slip transmission across interfaces in polycrystals , 1992 .

[14]  Anil K. Jain,et al.  Texture Analysis , 2018, Handbook of Image Processing and Computer Vision.

[15]  R. Gangloff,et al.  Determining fracture facet crystallography using electron backscatter patterns and quantitative tilt fractography , 1993 .

[16]  J. Petit,et al.  Electron backscattering pattern identification of surface morphology of fatigue cracks in TA6V , 1994 .

[17]  W. Evans,et al.  Dwell-sensitive fatigue under biaxial loads in the near-alpha titanium alloy IMI685 , 1994 .

[18]  M. Morris,et al.  Compatibility of deformation in two-phase Ti-Al alloys: Dependence on microstructure and orientation relationships , 1995 .

[19]  W. M. Rainforth,et al.  TEM observations of fatigue damage accumulation at the surface of the near-α titanium alloy IMI 834 , 1996 .

[20]  H. Davies,et al.  Electron back scattered diffraction (EBSD) analysis of quasi-cleavage and hydrogen induced fractures under cyclic and dwell loading in titanium alloys , 1997 .

[21]  Á. Barna,et al.  Amorphisation and surface morphology development at low-energy ion milling , 1998 .

[22]  U. F. Kocks,et al.  Texture and Anisotropy: Preferred Orientations in Polycrystals and their Effect on Materials Properties , 1998 .

[23]  M. Caturla,et al.  Defect production in collision cascades in elemental semiconductors and fcc metals , 1998 .

[24]  G. Lütjering Influence of processing on microstructure and mechanical properties of (α+β) titanium alloys , 1998 .

[25]  R. Wilson,et al.  Characterization of mechanical anisotropy in titanium alloys , 1998 .

[26]  M. Mills,et al.  Room temperature deformation and mechanisms of slip transmission in oriented single-colony crystals of an α/β titanium alloy , 1999 .

[27]  Mukul Kumar,et al.  Electron Backscatter Diffraction in Materials Science , 2000 .

[28]  V. Randle,et al.  Combined application of electron backscatter diffraction and stereo‐photogrammetry in fractography studies , 2001, Journal of microscopy.

[29]  J. McCaffrey,et al.  Surface damage formation during ion-beam thinning of samples for transmission electron microscopy. , 2001, Ultramicroscopy.

[30]  M. Savage,et al.  Deformation mechanisms and microtensile behavior of single colony Ti-6242Si , 2001 .

[31]  H. Wenk,et al.  Texture and Anisotropy , 2004 .

[32]  James C. Williams,et al.  Deformation behavior of HCP Ti-Al alloy single crystals , 2002 .

[33]  T. Bieler,et al.  The origins of heterogeneous deformation during primary hot working of Ti–6Al–4V , 2002 .

[34]  M. Starink,et al.  Effect of self-accommodation on α/α boundary populations in pure titanium , 2003 .

[35]  G. Lütjering,et al.  Alpha + Beta Alloys , 2003 .

[36]  T. Bieler,et al.  A factor to predict microcrack nucleation at γ-γ grain boundaries in TiAl , 2003 .

[37]  T. Bieler,et al.  An automated method to determine the orientation of the high-temperature beta phase from measured EBSD data for the low-temperature alpha-phase in Ti–6Al–4V , 2003 .

[38]  H. Fraser,et al.  The role of crystallographic and geometrical relationships between α and β phases in an α/β titanium alloy , 2003 .

[39]  M. Savage,et al.  Anisotropy in the room-temperature deformation of α–β colonies in titanium alloys: role of the α–β interface , 2004 .

[40]  K. Chan A micromechanical analysis of the yielding behavior of individual widmanstätten colonies of an α + β titanium alloy , 2004 .

[41]  T. Bieler,et al.  Fracture initiation/propagation parameters for duplex TiAl grain boundaries based on twinning, slip, crystal orientation, and boundary misorientation , 2005 .

[42]  S. Agnew,et al.  Uncertainty in the determination of fatigue crack facet crystallography , 2005 .

[43]  M. Mills,et al.  Crystallography of fracture facets in a near-alpha titanium alloy , 2006 .

[44]  T. Bieler,et al.  The effect of grain boundary normal on predicting microcrack nucleation using fracture initiation parameters in duplex TiAl , 2006 .

[45]  M. Mills,et al.  Observations on the faceted initiation site in the dwell-fatigue tested ti-6242 alloy: Crystallographic orientation and size effects , 2006 .

[46]  M. Mills,et al.  Determination of crystallographic orientation of dwell-fatigue fracture facets in Ti-6242 alloy , 2007 .

[47]  T. Bieler,et al.  On Predicting Nucleation of Microcracks Due to Slip-Twin Interactions at Grain Boundaries in Duplex Near γ-TiAl , 2008 .

[48]  M. Miller,et al.  Measuring Stress Distributions in Ti-6Al-4V Using Synchrotron X-Ray Diffraction , 2008 .

[49]  J. Mendez,et al.  Slip and fatigue crack formation processes in an α/β titanium alloy in relation to crystallographic texture on different scales , 2008 .

[50]  P. Bocher,et al.  Texture heterogeneities in αp/αs titanium forging analysed by EBSD‐Relation to fatigue crack propagation , 2009, Journal of microscopy.

[51]  A. Pilchak,et al.  Low ΔK faceted crack growth in titanium alloys , 2009 .

[52]  A. Pilchak,et al.  Effect of Yttrium on the Fatigue Behavior of Investment-Cast and Wrought Ti-6Al-4V , 2009 .