Fabrication of piezoelectric MEMS devices-from thin film to bulk PZT wafer

Integrating patterned functional piezoelectric layer onto silicon substrate is a key technique challenge in fabrication of piezoelectric Micro Electro Mechanical System (pMEMS) devices. Different device applications have different requirements on the thickness and in-plane geometry of the piezoelectric layers and thus have their own processing difficulties. In this paper, the techniques of integrating piezoelectric function into pMEMS has been discussed together with some diaphragm-based pMEMS devices which have relatively lenient requirement on patterning of the piezoelectric layers. Sol-gel thin film can meet the requirement of most of the sensor applications. The composite thick film is one of the promising solutions for thick film devices due to its good processing compatibility. Si/Pb(ZrxTi1 − x)O3 wafer bonding technique makes it possible to thin down the ceramic wafer to less than 10 μm by using chemical mechanical polishing, which, therefore, provide us another approach to integrate thick piezoelectric layer on silicon to cover the need of most of the thick film devices. Directly make double side aligned electrode patterns on bulk piezoelectric wafer/plate by using photolithography opens up a new area of pMEMS. The advantage of using bulk piezoelectric wafer/plate in pMEMS is that we can select commercial available ceramics or single crystals with excellent piezoelectric properties and thus ensure the overall performance of the devices.

[1]  Jong-Uk Bu,et al.  Calibration of Non Linear Properties of Pb(Zr, Ti)O3 Cantilever Using Integrated Piezoresistive Sensor for High Speed Atomic Force Microscopy , 2002 .

[2]  A. Barzegar,et al.  Piezoelectric micromachined ultrasonic transducers based on PZT thin films , 2005, IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control.

[3]  S. J. Milne,et al.  Characterization of sol-gel Pb(Zr_0.53Ti_0.47)O_3 films in the thickness range 0.25–10 μm , 1999 .

[4]  Cheng-Kuei Jen,et al.  High-temperature piezoelectric film ultrasonic transducers by a sol-gel spray technique and their application to process monitoring of polymer injection molding , 2006, IEEE Sensors Journal.

[5]  J. Baborowski Microfabrication of Piezoelectric MEMS , 2004 .

[6]  Eun Sok Kim,et al.  Micromachined acoustic resonant mass sensor , 2005 .

[7]  S. Sugiyama,et al.  Fabrication of Microdevices Using Bulk Ceramics of Lead Zirconate Titanate , 2005 .

[8]  K.K. Li,et al.  Micromachined high frequency ferroelectric sonar transducers , 1997, IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control.

[9]  Susumu Sugiyama,et al.  Wafer bonding of lead zirconate titanate to Si using an intermediate gold layer for microdevice application , 2006 .

[10]  Jianmin Miao,et al.  Analytical modeling for bulk-micromachined condenser microphones , 2006 .

[11]  C. Steinem,et al.  Piezoelectric Mass-Sensing Devices as Biosensors-An Alternative to Optical Biosensors? , 2000, Angewandte Chemie.

[12]  Seiji Aoyagi,et al.  Arrayed ultrasonic microsensors with high directivity for in-air use using PZT thin film on silicon diaphragms ☆ , 2002 .

[13]  Chen Chao,et al.  Micromachined thick film piezoelectric ultrasonic transducer array , 2005, The 13th International Conference on Solid-State Sensors, Actuators and Microsystems, 2005. Digest of Technical Papers. TRANSDUCERS '05..

[14]  J. Miao,et al.  24 – Piezoelectric thick films for MEMS application , 2008 .

[15]  S. Bhansali,et al.  A low-temperature bonding technique using spin-on fluorocarbon polymers to assemble microsystems , 2002 .

[16]  Geunbae Lim,et al.  A self-excited micro cantilever biosensor actuated by PZT using the mass micro balancing technique , 2006 .

[17]  H. Hng,et al.  Low Temperature Processing of Nanocrystalline Lead Zirconate Titanate (PZT) Thick Films and Ceramics by a Modified Sol-Gel Route , 2002 .

[18]  Jian Lu,et al.  A Novel Wet Etching Process of Pb(Zr,Ti)O3 Thin Films for Applications in Microelectromechanical System , 2004 .

[19]  Chen Chao,et al.  Fabrication and characterization of piezoelectric micromachined ultrasonic transducers with thick composite PZT films. , 2005, IEEE transactions on ultrasonics, ferroelectrics, and frequency control.

[20]  Takashi Iijima,et al.  Preparation of Lead Zirconate Titanate Thick Films by Arc-Discharged Reactive Ion-Plating Method , 2001 .

[21]  Srinivas Tadigadapa,et al.  Lead zirconate titanate films for d33 mode cantilever actuators , 2003 .

[22]  Zhihong Wang,et al.  Dense PZT thick films derived from sol-gel based nanocomposite process , 2003 .

[23]  Richard M. White,et al.  Analytic comparison of the sensitivities of bulk‐wave, surface‐wave, and flexural plate‐wave ultrasonic gravimetric sensors , 1989 .

[24]  Jianmin Miao,et al.  Piezoelectric thick films and their application in MEMS , 2007 .

[25]  R. Dorey,et al.  Effect of sintering aid and repeated sol infiltrations on the dielectric and piezoelectric properties of a PZT composite thick film , 2002 .

[26]  D. A. Barrow,et al.  Characterization of thick lead zirconate titanate films fabricated using a new sol gel based process , 1997 .

[27]  J. Akedo,et al.  Influence of Carrier Gas Conditions on Electrical and Optical Properties of Pb(Zr, Ti)O3 Thin Films Prepared by Aerosol Deposition Method , 2001 .

[28]  R. Dorey,et al.  Electroceramic Thick Film Fabrication for MEMS , 2004 .

[29]  Abdullah Atalar,et al.  Micromachined two-dimensional array piezoelectrically actuated transducers , 1998 .