Permittivity Spectrum of Low-Loss Liquid and Powder Geomaterials Using Multipoint Reentrant Cavities

Permittivity is a useful tool to characterize the composition and quality of many geomaterials. In general, the non-resonant permittivity measurement methods exhibit a higher degree of uncertainty than their resonant counterparts. In resonant measurements, the reduction in uncertainty comes typically with a loss in broadband. This article describes the theory, design, and application of multipoint coaxial reentrant resonant cavities applied to low-loss geomaterials at different temperatures. Specifically, a full-wave method based on circuit analysis is developed and applied for a circular corrugated waveguide. Moreover, the mode-matching method is applied to calculate the generalized admittance matrix (GAM). Two multipoint cavities and software were built and validated. The first cavity has five resonant frequencies, between 170 MHz and 2.3 GHz, and the second has four resonant frequencies, between 1.3 and 8.6 GHz. Thus, this method allows for “broadband-resonant” measurements. The permittivity values of liquid hydrocarbons, powdered kerogen, and pyrite are shown.

[1]  Jose Oliverio Alvarez,et al.  Multi-Frequency Microwave Resonance Cavity for Nondestructive Core Plug Measurements , 2018, IGARSS 2018 - 2018 IEEE International Geoscience and Remote Sensing Symposium.

[2]  C. Liang,et al.  ANALYSIS OF RESONANCE AND QUALITY FACTOR OF ANTENNA AND SCATTERING SYSTEMS USING COMPLEX FREQUENCY METHOD COMBINED WITH MODEL-BASED PARAMETER ESTIMATION , 2004 .

[3]  A.J. Canos,et al.  A novel technique for deembedding the unloaded resonance frequency from measurements of microwave cavities , 2006, IEEE Transactions on Microwave Theory and Techniques.

[4]  Jose M. Catala-Civera,et al.  Circuital analysis of a coaxial re-entrant cavity for performing dielectric measurement , 2009, 2009 IEEE MTT-S International Microwave Symposium Digest.

[5]  M. Fingas,et al.  Handbook of Oil Spill Science and Technology , 2015 .

[6]  Kjetil Folgerø,et al.  Broad-band dielectric spectroscopy of low-permittivity fluids using one measurement cell , 1998, IEEE Trans. Instrum. Meas..

[7]  Greg Bernero,et al.  Dielectric characterization of geochemical properties of crude oils and gas condensate at 25°C , 2017, 2017 IEEE International Geoscience and Remote Sensing Symposium (IGARSS).

[8]  Uta Dresdner,et al.  Introduction To Geochemistry , 2016 .

[9]  M. Bustin,et al.  The effects and distribution of moisture in gas shale reservoir systems , 2010 .

[10]  R. Harrington Time-Harmonic Electromagnetic Fields , 1961 .

[11]  W. Fertl Kerogen, Insoluble Organic Matter from Sedimentary Rocks , 1982 .

[12]  E. Iso,et al.  Measurement Uncertainty and Probability: Guide to the Expression of Uncertainty in Measurement , 1995 .

[13]  Arnt-Børre Salberg,et al.  Oil Spill Detection in Hybrid-Polarimetric SAR Images , 2014, IEEE Transactions on Geoscience and Remote Sensing.

[14]  Felipe L. Peñaranda-Foix,et al.  Enhanced Full-Wave Circuit Analysis for Modeling of a Split Cylinder Resonator , 2017, IEEE Transactions on Microwave Theory and Techniques.

[15]  Swen Kortig,et al.  Foundations For Microwave Engineering , 2016 .

[16]  B. Durand Kerogen: Insoluble Organic Matter from Sedimentary Rocks , 1980 .

[17]  Camilla Brekke,et al.  Analysis of Evolving Oil Spills in Full-Polarimetric and Hybrid-Polarity SAR , 2017, IEEE Transactions on Geoscience and Remote Sensing.

[18]  Dielectric properties of nonaqueous drilling fluids from 1 MHz up to 20 GHz , 2014, IEEE Transactions on Dielectrics and Electrical Insulation.

[19]  Vitaliy Zhurbenko,et al.  Passive Microwave Components and Antennas , 2010 .

[20]  P. Domich,et al.  Analysis of an open-ended coaxial probe with lift-off for nondestructive testing , 1994 .

[21]  J. Baker-Jarvis,et al.  Dielectric measurements using a reentrant cavity :: mode-Matching analysis James Baker-Jarvis, Bill F. Riddle. , 1996 .

[22]  Benjamin Holt,et al.  SAR Imagery for Detecting Sea Surface Slicks: Performance Assessment of Polarization-Dependent Parameters , 2018, IEEE Transactions on Geoscience and Remote Sensing.

[23]  Benjamin Holt,et al.  Polarimetric Analysis of Backscatter From the Deepwater Horizon Oil Spill Using L-Band Synthetic Aperture Radar , 2012, IEEE Transactions on Geoscience and Remote Sensing.

[24]  B. Garcia-Banos,et al.  A nondestructive method of measuring the dielectric and magnetic properties of laminate materials in open cavities , 2004, 2004 IEEE MTT-S International Microwave Symposium Digest (IEEE Cat. No.04CH37535).

[25]  M. D. Janezic,et al.  Full-Wave Analysis of Dielectric-Loaded Cylindrical Waveguides and Cavities Using a New Four-Port Ring Network , 2012, IEEE Transactions on Microwave Theory and Techniques.

[26]  B. Hascakir,et al.  Stability Determination of Asphaltenes through Dielectric Constant Measurements of Polar Oil Fractions , 2017 .