Effects of mathematical models and algorithms on quantitative characterization of areal step height with optical and stylus profilometers

Abstract Step height characterization is essential for the quality control of various functional components, such as graphene and the step features of semiconductor devices. Two methods are proposed to characterize the areal step heights. The first method extends the two-dimensional characterization in the ISO specification into a three-dimensional one by extracting multiple parallel profiles. The second method calculates the step heights by projecting from the measurement points to the normal vector at the surface centroid. Mathematical models and algorithms of the two methods are introduced and validated by synthetic data. Experiments are conducted by comparing the assessment results of the two methods and of a method proposed in a previous research. The calibrated values of the standards are utilized for validation. The characterization results may differ notably or slightly, depending on the properties of the data and the algorithm.

[1]  K. Kokh,et al.  Step-height standards based on the rapid formation of monolayer steps on the surface of layered crystals , 2017 .

[2]  Chen Wang,et al.  Confidence Distance Matrix for outlier identification: A new method to improve the characterizations of surfaces measured by confocal microscopy , 2019, Measurement.

[4]  K. Creath Step height measurement using two-wavelength phase-shifting interferometry. , 1987, Applied optics.

[5]  Richard Leach,et al.  Metrological characteristics for the calibration of surface topography measuring instruments: a review , 2020, Measurement Science and Technology.

[6]  E. Hæggström,et al.  Step height standards based on self-assembly for 3D metrology of biological samples , 2020, Measurement Science and Technology.

[7]  Development of dual-wavelength fiber ring laser and its application to step-height measurement using self-mixing interferometry. , 2016, Optics express.

[8]  Zhuangde Jiang,et al.  A sub-50 nm three-step height sample for AFM calibration , 2014 .

[9]  Peter de Groot,et al.  Measurement, certification and use of step-height calibration specimens in optical metrology , 2017, Optical Metrology.

[10]  Sean Li,et al.  Microstructure, post thermal treatment response, and tribological properties of 3D printed 17-4 PH stainless steel , 2020 .

[11]  Anand Asundi,et al.  3D profile measurement for stepped microstructures using region-based transport of intensity equation , 2019, Measurement science and technology.

[12]  H Han Haitjema International comparison of depth-setting standards , 1997 .

[13]  U. Brand,et al.  Step height measurement of microscale thermoplastic polymer specimens using contact stylus profilometry , 2016 .

[14]  Chen Wang,et al.  Comparison of methods for outlier identification in surface characterization , 2018 .

[15]  Chen Wang,et al.  Procedure for Calibrating the Z-axis of a Confocal Microscope: Application for the Evaluation of Structured Surfaces , 2019, Sensors.

[16]  Richard K. Leach,et al.  Characterisation of Areal Surface Texture , 2013 .

[17]  Kebin Shi,et al.  Time-of-flight detection of femtosecond laser pulses for precise measurement of large microelectronic step height. , 2018, Optics letters.

[18]  Richard K. Leach,et al.  Calibration and verification of areal surface texture measuring instruments , 2015 .

[19]  Liam Blunt,et al.  Paradigm shifts in surface metrology. Part I. Historical philosophy , 2007, Proceedings of the Royal Society A: Mathematical, Physical and Engineering Sciences.

[21]  F. Gao,et al.  Rapid measurement of large step heights using a microscopic white-light spectral interferometer , 2019, Surface Topography: Metrology and Properties.

[22]  Hyo Mi Park,et al.  Dual low coherence scanning interferometry for rapid large step height and thickness measurements. , 2016, Optics express.

[23]  Shu Zhang,et al.  Calibration method of curvature distortion in step height measurement by atomic force microscopy , 2020, IOP Conference Series: Materials Science and Engineering.