New Permittivity Measurement Methods Using Resonant Phenomena For High-Permittivity Materials

This paper describes the characterization of high-permittivity materials with a dielectric constant (<inline-formula> <tex-math notation="LaTeX">$\epsilon _{r}$ </tex-math></inline-formula>) up to 3000 using resonant phenomena. We propose and demonstrate two types of measurement techniques: the rectangular resonator method by controlling the sample insertion length and the waveguide reflection method with a sample terminated by a short circuit. We investigate the validity and the range of application of both methods by performing numerical calculations. We also experimentally demonstrate these two methods by measuring dielectric materials with <inline-formula> <tex-math notation="LaTeX">$\epsilon _{r}$ </tex-math></inline-formula> ~100 and 200 for the former method and those with <inline-formula> <tex-math notation="LaTeX">$\epsilon _{r}$ </tex-math></inline-formula> ~200, 1400, 1700, and 2900 for the latter method. By estimating the measurement uncertainty using Monte Carlo calculations, we clarify that the results obtained by both methods for a dielectric material with <inline-formula> <tex-math notation="LaTeX">$\epsilon _{r}$ </tex-math></inline-formula> ~ 200 are almost consistent within the ranges of the uncertainties.

[1]  J. Grigas Microwave Dielectric Spectroscopy of Ferroelectrics and Related Materials , 1996 .

[2]  Richard G. Geyer,et al.  Transmission/Reflection and Short-Circuit Line Methods for Measuring Permittivity and Permeability , 1992 .

[3]  J. Carru,et al.  Dispersion and loss of ferroelectric Ba0.5Sr0.5TiO3 thin films up to 110 GHz , 2008 .

[4]  R. N. Clarke,et al.  A guide to the characterisation of dielectric materials at RF and microwave frequencies. , 2003 .

[5]  J. Booth,et al.  Microwave-frequency loss and dispersion in ferroelectric Ba0.3Sr0.7TiO3 thin films , 2005 .

[6]  Lu Wang,et al.  Broadband Microwave Characterization of Nanostructured Thin Film With Giant Dielectric Response , 2015, IEEE Transactions on Microwave Theory and Techniques.

[7]  Hong Wang,et al.  Dielectric resonator antennas using high permittivity ceramics , 2004 .

[8]  Katsuaki Suganuma,et al.  A Miniaturized Flexible Antenna Printed on a High Dielectric Constant Nanopaper Composite , 2015, Advanced materials.

[9]  Matteo Pasquali,et al.  Noncontact conductivity and dielectric measurement for high throughput roll-to-roll nanomanufacturing , 2015, Scientific Reports.

[10]  Pavel Kabos,et al.  Dielectric Characterization by Microwave Cavity Perturbation Corrected for Nonuniform Fields , 2014, IEEE Transactions on Microwave Theory and Techniques.

[11]  Jan Obrzut,et al.  Input impedance of a coaxial line terminated with a complex gap capacitance - numerical and experimental analysis , 2004, IEEE Transactions on Instrumentation and Measurement.

[12]  Jan Obrzut,et al.  High-frequency input impedance characterization of dielectric films for power-ground planes , 2003, IEEE Trans. Instrum. Meas..

[13]  J. Krupka,et al.  Complex permittivity measurements of low-loss microwave ceramics employing higher order quasi TE0np modes excited in a cylindrical dielectric sample , 2005 .

[14]  M. Sebastian,et al.  CeO2–La0.5Sr0.5CoO3−δ composites for giant permittivity applications , 2009 .

[15]  J. Obrzut,et al.  Surface conductance of graphene from non-contact resonant cavity. , 2016, Measurement : journal of the International Measurement Confederation.

[16]  Masahiro Horibe,et al.  Comparison of Calculation Techniques for Q-Factor Determination of Resonant Structures Based on Influence of VNA Measurement Uncertainty , 2014, IEICE Trans. Electron..

[17]  Jerzy Krupka,et al.  Frequency domain complex permittivity measurements at microwave frequencies , 2006 .

[18]  T. Lo,et al.  Planar inverted F antenna loaded with high permittivity material , 1995 .

[19]  Di Zhang,et al.  High permittivity and microwave absorption of porous graphitic carbons encapsulating Fe nanoparticles , 2012 .

[20]  C. P. L. Rubinger,et al.  Building a resonant cavity for the measurement of microwave dielectric permittivity of high loss materials , 2007 .

[21]  Relationship between permittivity and loss tangent , 1971 .