Experimental investigations and modelling of the ball motion in planetary ball mills

Abstract Planetary ball mills feature attractive properties, like the possibility of dry or wet operation, straightforward handling, cleanability and moderate costs. Consequently they are very well suited for lab scale process development in diverse industries, including pharmaceuticals and new materials. A number of questions still remain unanswered regarding this mill type. These include the stress conditions as well as transfer of the grinding results to other types of mills with free moving balls, such as stirred media mills, which can be built in large scales and operated continuously. In order to measure the ball motion and, thus, the stress conditions, a planetary ball mill was equipped with a high speed video camera, so that the grinding ball motion during the comminution process can be recorded and analysed. The influence of important process parameters on the ball motion pattern was assessed in this study, namely speed ratio, ball filling ratio and friction conditions, the latter by applying different mill feeds. The experimental results show considerable influences of the ball filling ratio and friction conditions. The measured ball motion patterns differ significantly from ball trajectories which were calculated using kinetic equations proposed in older publications. In addition to the measurements the ball motion was simulated using a three dimensional Discrete Element Model (DEM). An attempt was made to account for mill feed via altered friction coefficients. Correlations of the DEM results and experimental findings at different operating conditions show a good agreement. Based on simulation data the frequency distribution of the stress energies in the mill could be calculated and compared for different operating conditions.

[1]  Brahmeshwar Mishra,et al.  A review of computer simulation of tumbling mills by the discrete element method: Part I—contact mechanics , 2003 .

[2]  Karl Höffl,et al.  Zerkleinerungs- und Klassiermaschinen , 1986 .

[3]  Youwei Du,et al.  Mechanochemical synthesis of sodium tungsten bronze nanocrystalline powders , 2003 .

[4]  Michael Juhnke,et al.  Accelerated Formulation Development for Nanomilled Active Pharmaceutical Ingredients Using a Screening Approach , 2010 .

[5]  Junya Kano,et al.  Ball mill simulation in wet grinding using a tumbling mill and its correlation to grinding rate , 2004 .

[6]  B. K Mishra,et al.  A review of computer simulation of tumbling mills by the discrete element method , 2003 .

[7]  Dejan Poleti,et al.  Mechanochemical synthesis of nanocrystalline titanium monoxide , 2008 .

[8]  B. Mishra Ball Charge Dynamics in a Planetary Mill , 1995 .

[9]  Jörg Schwedes,et al.  Measurement of flow properties of bulk solids , 1996 .

[10]  Arno Kwade,et al.  Breaking characteristics of different materials and their effect on stress intensity and stress number in stirred media mills , 2002 .

[11]  Raymond A. Serway,et al.  Printed test bank to accompany Physics for scientists and engineers with modern physics , 1982 .

[12]  Ákos Kukovecz,et al.  Spectroscopic studies on the formation kinetics of SnO2 nanoparticles synthesized in a planetary ball mill , 2007 .

[13]  Jürgen Raasch Trajectories and impact velocities of grinding bodies in planetary ball mills , 1992 .

[14]  Brahmeshwar Mishra,et al.  Simulation of charge motion in ball mills. Part 1: experimental verifications , 1994 .

[15]  Amlan Datta,et al.  A direct approach of modeling batch grinding in ball mills using population balance principles and impact energy distribution , 2002 .

[16]  R. Venugopal,et al.  3D simulation of charge motion in tumbling mills by the discrete element method , 2001 .

[17]  Junya Kano,et al.  Effects of rotational direction and rotation-to-revolution speed ratio in planetary ball milling , 2002 .

[18]  Junya Kano,et al.  Analysis of abrasion mechanism of grinding media in a planetary mill with DEM simulation , 2010 .

[19]  P. Cundall,et al.  A discrete numerical model for granular assemblies , 1979 .

[20]  Jörg Schwedes,et al.  Stress energy distribution in different stirred media mill geometries , 2004 .

[21]  V. Zyryanov,et al.  Processing of oxide ceramic powders for nanomaterials using high-energy planetary mills , 2003 .

[22]  Stefan Heinrich,et al.  A Discrete Element Study of Wet Particle-Particle Interaction During Granulation in a Spout Fluidized Bed , 2009 .

[23]  Manoj Khanal,et al.  Oblique impact simulations of high strength agglomerates , 2009 .

[24]  Martin R. Wolf,et al.  K3 User Guide , 2000 .

[25]  Paul W. Cleary,et al.  Centrifugal mill charge motion and power draw: comparison of DEM predictions with experiment , 2000 .

[26]  Arno Kwade Mill selection and process optimization using a physical grinding model , 2004 .

[27]  J. Schwedes,et al.  Measurement of flow properites of bulk solids , 1990 .

[28]  M. Röck,et al.  Investigations on the caking behaviour of bulk solids—macroscale experiments , 2005 .

[29]  Georg-Peter Ostermeyer,et al.  A Spiral Tribometer for Dynamic Friction Measurements , 2009 .

[30]  Xiaosong Tang,et al.  Application of micro-ball bearing on Si for high rolling life-cycle , 2010 .

[31]  Yutaka Tsuji,et al.  Lagrangian numerical simulation of plug flow of cohesionless particles in a horizontal pipe , 1992 .

[32]  Junya Kano,et al.  Ball mill simulation and powder characteristics of ground talc in various types of mill , 2000 .

[33]  Toshio Inoue,et al.  Grinding mechanism of centrifugal mills — a simulation study based on the discrete element method , 1996 .

[34]  Junya Kano,et al.  Scale-up method of planetary ball mill , 2004 .

[35]  M. Tavoosi,et al.  Fabrication of Al–Zn/α-Al2O3 nanocomposite by mechanical alloying , 2008 .

[36]  Mojtaba Ghadiri,et al.  Distinct element analysis of attrition of granular solids under shear deformation , 2006 .

[37]  Runyu Yang,et al.  Discrete particle simulation of particle flow in IsaMill-Effect of grinding medium properties , 2008 .

[38]  Manoj Khanal,et al.  Original PaperOblique impact simulations of high strength agglomerates , 2009 .