Segregation of fluidized binary mixtures of granular solids

Fluidization behavior of binary mixtures of solids is addressed. Three binary systems were considered, obtained by mixing monodisperse granular solids of different size and/or density. A segmented fluidization column equipped with multiple pressure transducers was the experimental apparatus. Monitoring of pressure at different locations along the bed and direct characterization of solids contained in each segment were the experimental tools. The binary granular beds were in one of the following states, depending on gas superficial velocity and initial mixture fraction: fixed, bubbly-free fluidization, transient fluidization, and bubbling steady fluidization. Fluidization regimes were mapped in a gas superficial velocity vs. initial mixture fraction phase plane. Axial solids concentration profiles along the bed and solids segregation rates were also assessed for the three systems as a function of the operating conditions of the bed. Differences and similarities between the systems were analyzed and interpreted in the light of the basic segregation patterns. In particular whether a defluidized bottom layer of jetsam-rich solids is formed upon segregation appears to be an important key to the segregation phenomenology. The currently available models for the prediction of solids segregation in fluidized beds prove to be helpful to understand the qualitative features of the phenomenology, but fall short when quantitative prediction of segregation parameters is afforded. © 2004 American Institute of Chemical Engineers AIChE J, 50: 3095-3106, 2004

[1]  C. Laguerie,et al.  Experimental study of sawdust and coal particle mixing in sand or catalyst fluidized beds , 1990 .

[2]  L. Fan,et al.  Recent developments in solids mixing , 1990 .

[3]  D. Keairns,et al.  Rate of particle separation in a gas fluidized bed , 1982 .

[4]  L. Massimilla,et al.  The structure of bubble-free gas fluidized beds of fine fluid cracking catalyst particles , 1972 .

[5]  A. W. Nienow,et al.  Particle mixing and segregation in gas fluidised beds. A review , 1976 .

[6]  Rajamani Krishna,et al.  CFD modeling of gas‐fluidized beds with a bimodal particle mixture , 2001 .

[7]  J. Beeckmans,et al.  Studies on transport processes in a segregating fluidised bed , 1994 .

[8]  L. Massimilla,et al.  Bubble‐free expansion of gas‐fluidized beds of fine particles , 1973 .

[9]  Piero Salatino,et al.  Transient fluidization and segregation of binary mixtures of particles , 2000 .

[10]  L. G. Gibilaro,et al.  A model for a segregating gas fluidised bed , 1974 .

[11]  M. Menéndez,et al.  Segregation of straw/sand mixtures in fluidized beds in non-steady state , 1991 .

[12]  B Formisani,et al.  A fundamental approach to the phenomenology of fluidization of size segregating binary mixtures of solids , 2001 .

[13]  G. Donsì,et al.  The influence of bed moisture on fluidization characteristics of fine powders , 1979 .

[14]  J. Couderc,et al.  Incipient fluidization and particulate systems , 1985 .

[15]  A. W. Nienow,et al.  A quantitative analysis of the mixing of two segregating powders of different density in a gas-fluidised bed , 1978 .

[16]  H. H. Lee,et al.  Particle size distribution in fluidized beds for catalytic polymerization , 1997 .

[17]  M. Rasul,et al.  Segregation potential in binary gas fluidized beds , 1999 .

[18]  C. Laguérie,et al.  Vitesse minimale de fluidisation et expansion des couches de mélanges de particules solides fluidisées par un gaz , 1984 .

[19]  B.P.B. Hoomans,et al.  Granular dynamics simulation of segregation phenomena in bubbling gas-fluidised beds , 2000 .

[20]  A. W. Nienow,et al.  Fluidised binary mixtures in which the denser component may be flotsam , 1980 .

[21]  Alex C. Hoffmann,et al.  PARTICLE SEGREGATION IN FLUIDISED BINARY MIXTURES , 1993 .

[22]  S. Uchida,et al.  Minimum fluidization velocity of binary mixture of particles with large size ratio , 1986 .

[23]  I. Eames,et al.  Segregation patterns in gas-fluidized systems , 2001, Journal of Fluid Mechanics.

[24]  V. N. Dolgunin,et al.  Segregation modeling of particle rapid gravity flow , 1995 .

[25]  J. C. Villar,et al.  A study of segregation in a gas-solid fluidized bed: Particles of different density , 1989 .

[26]  B. Formisani Packing and fluidization properties of binary mixtures of spherical particles , 1991 .

[27]  A. W. Nienow,et al.  Parameter estimation for a solids mixing|segregation model for gas fluidised beds , 1982 .

[28]  J. Baeyens,et al.  Segregation by size difference in gas fluidized beds , 1998 .

[29]  He Yurong,et al.  Size segregation of binary mixture of solids in bubbling fluidized beds , 2003 .

[30]  O. Levenspiel,et al.  Drag coefficient and terminal velocity of spherical and nonspherical particles , 1989 .