Determining fractal dimension from nuclear magnetic resonance data in rocks with internal magnetic field gradients

ABSTRACTPore size distributions in rocks may be represented by fractal scaling, and fractal descriptions of pore systems may be used for prediction of petrophysical properties such as permeability, tortuosity, diffusivity, and electrical conductivity. Transverse relaxation time (T2) distributions determined by nuclear magnetic resonance (NMR) measurements may be used to determine the fractal scaling of the pore system, but the analysis is complicated when internal magnetic field gradients at the pore scale are sufficiently large. Through computations in ideal porous media and laboratory measurements of glass beads and sediment samples, we found that the effect of internal magnetic field gradients was most pronounced in rocks with larger pores and a high magnetic susceptibility contrast between the pore fluid and mineral grains. We quantified this behavior in terms of pore size and Carr-Purcell-Meiboom-Gill (CPMG) half-echo spacing through scaling arguments. We additionally found that the effects of intern...

[1]  J F Pepper,et al.  Geology of the Bedford Shale and Berea Sandstone in the Appalachian Basin. , 1954, Science.

[2]  Partha P. Mitra,et al.  Mechanism of NMR Relaxation of Fluids in Rock , 1994 .

[3]  H. Eugene Stanley,et al.  Application of fractal concepts to polymer statistics and to anomalous transport in randomly porous media , 1984 .

[4]  N. Bird,et al.  Water retention models for fractal soil structures , 1996 .

[5]  Antonio Saa,et al.  Fractal and multifractal analysis of pore-scale images of soil , 2006 .

[6]  Roy H Wilkens,et al.  The physical properties of a set of sandstones—Part I. The samples , 1985 .

[7]  J. Freeman,et al.  Restricted Diffusion And Internal Field Gradients , 1999 .

[8]  Christoph Clauser,et al.  Permeability prediction based on fractal pore‐space geometry , 1999 .

[9]  HuangGuanhua,et al.  A review of fractal, prefractal and pore-solid-fractal models for parameterizing the soil water retention curve , 2011 .

[10]  H. Daigle,et al.  Nuclear magnetic resonance characterization of shallow marine sediments from the Nankai Trough, Integrated Ocean Drilling Program Expedition 333 , 2014 .

[11]  Thompson,et al.  Fractal sandstone pores: Implications for conductivity and pore formation. , 1985, Physical review letters.

[12]  E. Pittman,et al.  Bimodal Porosity in Oolitic Reservoir--Effect on Productivity and Log Response, Rodessa Limestone (Lower Cretaceous), East Texas Basin , 1983 .

[13]  R. Kleinberg 9. Nuclear Magnetic Resonance , 1999 .

[14]  Benoit B. Mandelbrot,et al.  Fractal Geometry of Nature , 1984 .

[15]  E. Purcell,et al.  Effects of Diffusion on Free Precession in Nuclear Magnetic Resonance Experiments , 1954 .

[16]  E. Purcell,et al.  Relaxation Effects in Nuclear Magnetic Resonance Absorption , 1948 .

[17]  H. C. Torrey Bloch Equations with Diffusion Terms , 1956 .

[18]  Garrison Sposito,et al.  Fractal Fragmentation, Soil Porosity, and Soil Water Properties: I. Theory , 1991 .

[19]  G. Sposito,et al.  MODELS OF THE WATER RETENTION CURVE FOR SOILS WITH A FRACTAL PORE SIZE DISTRIBUTION , 1996 .

[20]  Lizhi Xiao,et al.  NMR logging : principles and applications , 1999 .

[21]  E. Perfect Estimating soil mass fractal dimensions from water retention curves 1 Kentucky Agric. Exp. Stn. Cont , 1999 .

[22]  K. H. Lee,et al.  Interpretation of water nuclear magnetic resonance relaxation times in heterogeneous systems , 1974 .

[23]  E. R. Andrew,et al.  Nuclear Magnetic Resonance , 1955 .

[24]  K. Brownstein,et al.  Importance of classical diffusion in NMR studies of water in biological cells , 1979 .

[25]  John W. Crawford,et al.  The relation between the moisture-release curve and the structure of soil , 1995 .

[26]  R. Bryant,et al.  Translational diffusion of liquids at surfaces of microporous materials: Theoretical analysis of field-cycling magnetic relaxation measurements , 1997 .

[27]  David P Gallegos,et al.  A NMR technique for the analysis of pore structure: Determination of continuous pore size distributions , 1988 .

[28]  Mark A. Horsfield,et al.  Transverse relaxation processes in porous sedimentary rock , 1990 .

[29]  B. Dugan,et al.  Data report: permeability, consolidation, stress state, and pore system characteristics of sediments from Sites C0011, C0012, and C0018 of the Nankai Trough 1 , 2014 .

[30]  B. Audoly,et al.  Correlation functions for inhomogeneous magnetic field in random media with application to a dense random pack of spheres. , 2003, Journal of magnetic resonance.

[31]  H. Pfeifer Nuclear Magnetic Resonance and Relaxation of Molecules Adsorbed on Solids , 1972 .

[32]  D. J. Bergman,et al.  Nuclear Magnetic Resonance: Petrophysical and Logging Applications , 2011 .

[33]  W. E. Kenyon,et al.  A Three-Part Study of NMR Longitudinal Relaxation Properties of Water-Saturated Sandstones , 1988 .

[34]  M. Sahimi,et al.  Percolation Theory Generates a Physically Based Description of Tortuosity in Saturated and Unsaturated Porous Media , 2013 .

[35]  Scott W. Tyler,et al.  Fractal processes in soil water retention , 1990 .

[36]  R. L. Kleinberg,et al.  T1/T2 Ratio and Frequency Dependence of NMR Relaxation in Porous Sedimentary Rocks , 1993 .

[37]  Abdurrahman Sezginer,et al.  Nuclear magnetic resonance properties of rocks at elevated temperatures , 1992 .

[38]  R. H. Brooks,et al.  Hydraulic properties of porous media , 1963 .

[39]  C. H. Neuman Spin echo of spins diffusing in a bounded medium , 1974 .