Microstructure of additive layer manufactured Ti–6Al–4V after exceptional post heat treatments

Abstract The microstructure of Ti–6Al–4V components, which were produced by an additive layer manufacturing (ALM) process, typically consists of columnar prior β-grains containing colony and/or basket-weave α + β with martensite. The microstructure is equivalent to microstructures neither of wrought nor of cast parts. However, the post heat treatments applied for the present investigation are derived from heat treatment specifications of those materials. This paper presents the microstructure and hardness of additive manufactured Ti–6Al–4V after heat treatments, which are not standardized or commonly applied, in order to suggest new ways forward. The experiments show that columnar prior β-grains can be transformed to globular prior β-grains without cold or hot working. The hardness and microstructure in a prior β-grain is a function of the cooling rate through β transus temperature rather than of the duration at above β transus. A heating cycle was determined which leads to a microstructure that is homogeneous in each prior β-grain and does not significantly differ from grain to grain.

[1]  Joseph R. Davis Properties and selection : nonferrous alloys and special-purpose materials , 1990 .

[2]  E. Collings,et al.  Materials Properties Handbook: Titanium Alloys , 1994 .

[3]  Omer Van der Biest,et al.  Texture and Crystal Orientation in Ti-6Al-4V Builds Fabricated by Shaped Metal Deposition , 2010 .

[4]  Zhengxiao Guo,et al.  Microstructural evolution of a Ti–6Al–4V alloy during β-phase processing: experimental and simulative investigations , 2004 .

[5]  S. S. Al-Bermani,et al.  The Origin of Microstructural Diversity, Texture, and Mechanical Properties in Electron Beam Melted Ti-6Al-4V , 2010 .

[6]  Christoph Leyens,et al.  Morphology, microstructure, and hardness of titanium (Ti-6Al-4V) blocks deposited by wire-feed additive layer manufacturing (ALM) , 2012 .

[7]  S. L. Semiatin,et al.  The laser additive manufacture of Ti-6Al-4V , 2001 .

[8]  G. Lütjering Influence of processing on microstructure and mechanical properties of (α+β) titanium alloys , 1998 .

[9]  C. Leyens,et al.  Titanium and titanium alloys : fundamentals and applications , 2005 .

[10]  Christoph Leyens,et al.  Mechanical properties of additive manufactured titanium (Ti–6Al–4V) blocks deposited by a solid-state laser and wire , 2011 .

[11]  Christoph Leyens,et al.  Deposition of Ti–6Al–4V using laser and wire, part I: Microstructural properties of single beads , 2011 .

[12]  J. Kruth,et al.  A study of the microstructural evolution during selective laser melting of Ti–6Al–4V , 2010 .

[13]  Omer Van der Biest,et al.  Wire based additive layer manufacturing: Comparison of microstructure and mechanical properties of Ti–6Al–4V components fabricated by laser-beam deposition and shaped metal deposition , 2011 .

[14]  Chun‐Sing Lee,et al.  Quasi-static and dynamic deformation behavior of Ti–6Al–4V alloy containing fine α2-Ti3Al precipitates , 2004 .