Micropillar compression of Al/SiC nanolaminates

Abstract Al/SiC nanolaminates possess an excellent combination of mechanical strength and flexibility. While nanoindentation provides a reasonable estimate of the mechanical properties such as Young’s modulus and hardness of these materials, the stress state under nanoindentation is extremely complex. Micropillar compression has become an attractive method of studying the mechanical properties of materials at small length scales in a nominally homogeneous stress state. In this work, micropillars of Al/SiC nanolaminate were fabricated using focused ion beam milling. Compression testing was carried out using a flat-end nanoindenter head. The actual displacement of the pillar during micropillar compression was deconvoluted by subtracting the “extraneous” displacements of the system. Fractographic analysis showed that Al squeezes out between the SiC layers and that a mutual constraint is observed between the hard and soft layers. Numerical finite element modeling was also employed to provide physical insight into the deformation features of the multilayered pillar structure and agreed well with the experimental observations.

[1]  Amit Misra,et al.  Length-scale-dependent deformation mechanisms in incoherent metallic multilayered composites , 2005 .

[2]  Reinhard Pippan,et al.  Mechanical properties of micro-sized copper bending beams machined by the focused ion beam technique , 2005 .

[3]  G. Pharr,et al.  Compressive strengths of molybdenum alloy micro-pillars prepared using a new technique , 2007 .

[4]  Effect of material heterogeneity on the evolution of internal deformation during nanoindentation , 2009 .

[5]  K. T. Ramesh,et al.  The Design of Accurate Micro-Compression Experiments , 2006 .

[6]  N. Chawla,et al.  Elastic properties of metal–ceramic nanolaminates measured by nanoindentation , 2009 .

[7]  G. Tang,et al.  Indentation mechanics and fracture behavior of metal/ceramic nanolaminate composites , 2008 .

[8]  N. Chawla,et al.  Focused Ion Beam (FIB) tomography of nanoindentation damage in nanoscale metal/ceramic multilayers , 2010 .

[9]  Julia R. Greer,et al.  Size dependence of mechanical properties of gold at the sub-micron scale , 2005 .

[10]  T. Nieh,et al.  Sample size effect and microcompression of Mg65Cu25Gd10 metallic glass , 2007 .

[11]  Jussi Hiltunen,et al.  BaTiO3–SrTiO3 multilayer thin film electro-optic waveguide modulator , 2006 .

[12]  E. Bauer,et al.  Length scale effects on the electronic transport properties of nanometric Cu/Nb multilayers , 2007 .

[13]  D. Dimiduk,et al.  Sample Dimensions Influence Strength and Crystal Plasticity , 2004, Science.

[14]  Amit Misra,et al.  Deformability of ultrahigh strength 5 nm Cu/Nb nanolayered composites , 2008 .

[15]  Yun-Che Wang,et al.  Fatigue properties of nanoscale Cu/Nb multilayers , 2006 .

[16]  Margit Zacharias,et al.  Multilevel charge storage in silicon nanocrystal multilayers , 2005 .

[17]  Helicon plasma deposition of a TiO2/SiO2 multilayer optical filter with graded refractive index profiles , 1998 .

[18]  H. Fraser,et al.  Application of micro-sample testing to study fundamental aspects of plastic flow , 2006 .

[19]  Desiderio Kovar,et al.  Superplastic deformation of Al2O3/Y-TZP particulate composites and laminates , 2004 .

[20]  K. Chawla,et al.  Mechanical Behavior of Multilayered Nanoscale Metal‐Ceramic Composites , 2005 .

[21]  K. Chawla,et al.  Nanoindentation behavior of nanolayered metal-ceramic composites , 2005 .

[22]  Johannes Boneberg,et al.  Magnetic multilayers on nanospheres , 2005, Nature materials.

[23]  H. Espinosa,et al.  Dislocation escape-related size effects in single-crystal micropillars under uniaxial compression , 2007 .

[24]  S. Deevi,et al.  Single layer and multilayer wear resistant coatings of (Ti,Al)N: a review , 2003 .

[25]  Michael D. Uchic,et al.  A methodology to investigate size scale effects in crystalline plasticity using uniaxial compression testing , 2005 .

[26]  G. Pharr,et al.  Effects of focused ion beam milling on the nanomechanical behavior of a molybdenum-alloy single crystal , 2007 .

[27]  Michael D. Uchic,et al.  Micro-compression testing of fcc metals: A selected overview of experiments and simulations , 2009 .

[28]  I. N. Sneddon The relation between load and penetration in the axisymmetric boussinesq problem for a punch of arbitrary profile , 1965 .