The use of chemical and infrared methods for analysis of milk and dairy products

INTRODUCTION Accurate food compositional analysis has been a key factor in helping the food industry to improve and standardize both its processes and its products. In dairy products protein and fat are two of the most important compositional elements that must be determined. Traditionally, laboratories have depended on a wide range of chemical analysis techniques to measure the levels of these components. Many of these methods expose laboratory personnel to toxic substances and, subsequently, potential health hazards. More recently, however, a number of rapid and accurate instrumental methods have been gradually introduced which have many advantages compared to older techniques.' A further factor leading to the introduction of such methods is the fact that harmful gases from current analytical methods will no longer be tolerated by international administrative agencies. Finally, the desire to improve the efficiency of food manufacturing processes is also driving the development of instruments which can monitor lev& of food components in-line. Effective process control depends upon inputs from sensors such as pH meters, temperature sensors, flow-meters and conductivity meters which can accurately and reliably track the continuous variation within a material during processing.' Continuous inprocess monitoring is now a fundamental requirement of the modem food industry and has become increasingly important due to the developing interest in computer based automation and manufacturing.

[1]  Yizeng Liang,et al.  Preprocessing of analytical profiles in the presence of homoscedastic or heteroscedastic noise , 1994 .

[2]  P. F. Fox,et al.  Dairy Chemistry and Biochemistry , 1998 .

[3]  U. S. Ashworth,et al.  Factors affecting the dye binding of milk proteins. , 1957 .

[4]  L. Bokobza Near Infrared Spectroscopy , 1998 .

[5]  Hiromi Kamishikiryo-Yamashita,et al.  Protein content in milk by near-infrared spectroscopy , 1994 .

[6]  Robert A. Witte Spectrum and network measurements , 1991 .

[7]  R. Grappin,et al.  Bases and Experiences of Expressing the Protein Content of Milk—France , 1992 .

[8]  B S Lanher Evaluation of Aegys Mi 600 Fourier transform infrared milk analyzer for analysis of fat, protein, lactose, and solids nonfat: a compilation of eight independent studies. , 1996, Journal of AOAC International.

[9]  Gerard Downey,et al.  Authentication of Food and Food Ingredients by near Infrared Spectroscopy , 1996 .

[10]  William E. Keiser,et al.  Introduction to Infrared Spectroscopy , 1970 .

[11]  D A Biggs,et al.  Instrumental infrared estimation of fat, protein, and lactose in milk: collaborative study. , 1978, Journal - Association of Official Analytical Chemists.

[12]  Pieter Walstra Payment of Milk According to Protein Content in The Netherlands , 1992 .

[13]  S. Pochet,et al.  Determination of fat, protein, and lactose in raw milk by Fourier transform infrared spectroscopy and by analysis with a conventional filter-based milk analyzer. , 1996, Journal of AOAC International.

[14]  W. Horwitz Official Methods of Analysis , 1980 .

[15]  Fred A. Payne,et al.  Fiber Optic Sensor for Predicting the Cutting Time of Coagulating Milk for Cheese Production , 1993 .

[16]  Christopher N.G. Scotter,et al.  Non-destructive spectroscopic techniques for the measurement of food quality , 1997 .

[17]  Tom Fearn,et al.  Practical Nir Spectroscopy With Applications in Food and Beverage Analysis , 1993 .

[18]  J. A. Phelan,et al.  Standardisation of milk for cheesemaking at factory level , 1981 .

[19]  R. Grappin,et al.  Protein definition for milk payment to farmers , 1995 .

[20]  R. Grappin,et al.  Analytical methods for milk proteins. , 1992 .

[21]  R. Wehling,et al.  Determination of moisture in Cheddar cheese by near infrared reflectance spectroscopy. , 1988, Journal - Association of Official Analytical Chemists.

[22]  O. H. Lowry,et al.  Protein measurement with the Folin phenol reagent. , 1951, The Journal of biological chemistry.

[23]  K. B. Whetsel Near-Infrared Spectrophotometry , 1968 .

[24]  W. Fred McClure,et al.  Near infrared spectroscopy : the giant is running strong , 1994 .

[25]  J. D. S. Goulden,et al.  Analysis of milk by infra-red absorption , 1964, Journal of Dairy Research.

[26]  M. Scott,et al.  On-line measurement techniques using NIR spectroscopy. , 1993 .

[27]  J. W. Sherbon,et al.  Rapid determination of protein in milk by dye binding. , 1967 .

[28]  David M. Barbano,et al.  Crude and Protein Nitrogen Bases for Protein Measurement and Their Impact on Current Testing Accuracy , 1992 .

[29]  C. A. Ernstrom,et al.  Enzymic Coagulation of Milk Casein Micelles , 1984 .