Proposal of an empirical viscosity model for quality control in the polymer extrusion process

An empirical model to evaluate the viscosities of thermoplastic polymers in the extrusion process for quality control is proposed in this article. The viscosity is calculated from the screw rotation speed, melt temperature, geometric dimensions of the extruder and material constants, which were experimentally determined. Polypropylene (PP) was used in this study to test the effectiveness of the model. Comparing the calculated results, it was found that the viscosities obtained with the present model are in agreement with those obtained by using an in-line rheometer. The result shows that the proposed method can be applied to control the polymer extrusion process without imbedding an in-line rheometer, which influences the output of the product.

[1]  Z. Lewandowski Application of a linear synthetic polymer to improve the properties of cellulose fibers made by the NMMO process , 2002 .

[2]  John M. Dealy,et al.  Process rheometers for molten plastics: A survey of existing technology , 1993 .

[3]  Stephen T. Balke,et al.  Development of an in-line rheometer suitable for reactive extrusion processes , 1991 .

[4]  Shih-Hsuan Chiu,et al.  In‐line viscosity fuzzy control , 2001 .

[5]  John M. Dealy,et al.  Closed loop viscosity control of reactive extrusion with an in‐line rheometer , 1996 .

[6]  M. Fujiyama,et al.  Rheological properties of polypropylenes with different molecular weight distribution characteristics , 2002 .

[7]  H. Schott Dependence of activation energy for viscous flow of polyhydrocarbons on bulk of substituents , 1962 .

[8]  R. Landel,et al.  The Temperature Dependence of Relaxation Mechanisms in Amorphous Polymers and Other Glass-Forming Liquids , 1955 .

[9]  M. Ghannam,et al.  Rheological properties of carboxymethyl cellulose , 1997 .

[10]  A. Malmberg,et al.  Thermal and rheological studies on the molecular composition and structure of metallocene- and Ziegler–Natta-catalyzed ethylene–α-olefin copolymers , 2002 .

[11]  C. Tzoganakis,et al.  Control of a LDPE reactive extrusion process , 2000 .

[12]  R. Pitchumani,et al.  Interlaminar contact development during thermoplastic fusion bonding , 2002 .

[13]  W. R. Cluett,et al.  Controller design and performance analysis for a reactive extrusion process , 1994 .

[14]  Ming-Chien Yang,et al.  Viscous behavior of ultrahigh molecular weight polyethylene solution , 1997 .

[15]  Shih-hsuan Chiu,et al.  In-line viscosity control in an extrusion process with a fuzzy gain scheduled PID controller , 1999 .

[16]  Imrich Klein,et al.  Engineering principles of plasticating extrusion , 1970 .