Effect of cantilever deformation and tip-sample contact area on AFM nanoscratching

The present work investigates the effect of cantilever deformation and tip-sample contact area on the performance of atomic force microscopy (AFM)-based scratching tests. Nanoscratching tests are carried out using a pyramidal diamond tip on aluminum alloy surfaces. Three typical AFM cantilever deformation states are illustrated, and the actual normal loads applied on the surface of the sample are obtained using a new method. A theoretical model for AFM-based nanoscratching using a three-sided pyramidal tip is also established to calculate the effect of the tip-sample contact area for different scratching directions. The corresponding theoretical normal loads can be obtained with this model. Experimental and theoretical results are compared for the normal loads at an expected machined depth, with different scratching directions. The contact length between the chip and the rake face of the tip is found to be the key factor leading to an increase in the tip-sample contact area. This results in an actual norm...

[1]  A. Tseng,et al.  Nanopatterning on silicon surface using atomic force microscopy with diamond-like carbon (DLC)-coated Si probe , 2011, Nanoscale research letters.

[2]  J. Heath,et al.  Fast nonlinear ion transport via field-induced hydrodynamic slip in sub-20-nm hydrophilic nanofluidic transistors. , 2009, Nano letters.

[3]  Zaili Dong,et al.  Atomic force microscopy-based repeated machining theory for nanochannels on silicon oxide surfaces , 2011 .

[4]  S. Jacobson,et al.  Ion transport in nanofluidic funnels. , 2010, ACS nano.

[5]  A. Tseng Three-dimensional patterning of nanostructures using atomic force microscopes , 2011 .

[6]  J. Alarie,et al.  A device for performing lateral conductance measurements on individual double-stranded DNA molecules. , 2012, ACS nano.

[7]  A. Tseng Removing material using atomic force microscopy with single- and multiple-tip sources. , 2011, Small.

[8]  Dong-Kwon Kim,et al.  Slip-enhanced reverse electrodialytic power generation in ion-selective nanochannels , 2013 .

[9]  Thomas George,et al.  A Nanochannel Fabrication Technique without Nanolithography , 2003 .

[10]  Zone-Ching Lin,et al.  A calculating method for the fewest cutting passes on sapphire substrate at a certain depth using specific down force energy with an AFM probe , 2012 .

[11]  J. Ramsey,et al.  Electrokinetically-driven transport of DNA through focused ion beam milled nanofluidic channels. , 2013, Analytical chemistry.

[12]  H. Craighead,et al.  Separation of long DNA molecules in a microfabricated entropic trap array. , 2000, Science.

[13]  C. Dekker,et al.  Fabrication of solid-state nanopores with single-nanometre precision , 2003, Nature materials.

[14]  Tao Sun,et al.  Effects of scratching directions on AFM-based abrasive abrasion process , 2009 .

[15]  Shen Dong,et al.  Investigation on AFM-based micro/nano-CNC machining system , 2007 .

[16]  Simon S. Park,et al.  Atomic force microscope probe-based nanometric scribing , 2010 .

[17]  T. Sun,et al.  Study on effects of tip geometry on AFM nanoscratching tests , 2007 .

[18]  Seong J. Cho,et al.  Tunable ionic transport for a triangular nanochannel in a polymeric nanofluidic system. , 2013, ACS nano.

[19]  Chung-Feng Jeffrey Kuo,et al.  Scratch direction and threshold force in nanoscale scratching using atomic force microscopes , 2011 .

[20]  S. H. Lee,et al.  Characterization and acoustic emission monitoring of AFM nanomachining , 2009 .

[21]  Jane E. Curtin,et al.  Nanochannel fabrication for chemical sensors , 1997 .

[22]  C. Chou,et al.  Fabrication of Size-Controllable Nanofluidic Channels by Nanoimprinting and Its Application for DNA Stretching , 2004 .

[23]  Kevin Ke,et al.  Label-free affinity assays by rapid detection of immune complexes in submicrometer pores. , 2006, Angewandte Chemie.

[24]  F. P. Bowden,et al.  The Friction and Lubrication of Solids , 1964 .

[25]  U. Wejinya,et al.  Atomic force microscopy based repeatable surface nanomachining for nanochannels on silicon substrates , 2012 .

[26]  Takashi Yamaguchi,et al.  Mechanism of Material Removal in Nanomachining of Fused Quartz using AFM Diamond Tip , 2010 .