Macromolecular Crystallography Protocols

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[2]  Bong-Gyoon Han,et al.  Structural basis of water-specific transport through the AQP1 water channel , 2001, Nature.

[3]  A. Puustinen,et al.  The structure of the ubiquinol oxidase from Escherichia coli and its ubiquinone binding site , 2000, Nature Structural Biology.

[4]  Raymond C Stevens,et al.  Structural Adaptations in a Membrane Enzyme That Terminates Endocannabinoid Signaling , 2002, Science.

[5]  K. Diederichs,et al.  Crystallization and preliminary X-ray diffraction analysis of ScrY, a specific bacterial outer membrane porin. , 1993, Journal of molecular biology.

[6]  Colin Hughes,et al.  Crystal structure of the bacterial membrane protein TolC central to multidrug efflux and protein export , 2000, Nature.

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[8]  G. Schulz,et al.  Structure of maltoporin from Salmonella typhimurium ligated with a nitrophenyl-maltotrioside. , 1997, Journal of molecular biology.

[9]  G. Schulz,et al.  Crystallization and preliminary X‐ray crystallographic analysis of squalene‐hopene cyclase from Alicyclobacillus acidocaldarius , 1997, Protein science : a publication of the Protein Society.

[10]  P. Loll,et al.  The X-ray crystal structure of the membrane protein prostaglandin H2 synthase-1 , 1994, Nature.

[11]  P Gros,et al.  Crystal structure of the outer membrane protease OmpT from Escherichia coli suggests a novel catalytic site , 2001, The EMBO journal.

[12]  N. Navaratnam,et al.  Optimization of apolipoprotein B mRNA editing by APOBEC1 apoenzyme and the role of its auxiliary factor, ACF. , 2004, RNA.

[13]  D. Eisenberg,et al.  Fusion proteins as tools for crystallization: the lactose permease from Escherichia coli. , 1994, Acta crystallographica. Section D, Biological crystallography.

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[16]  K. Ingham Precipitation of proteins with polyethylene glycol. , 1990, Methods in enzymology.

[17]  S. Iwata,et al.  Purification and crystallization of the respiratory complex formate dehydrogenase-N from Escherichia coli. , 2002, Acta crystallographica. Section D, Biological crystallography.

[18]  K. Moore,et al.  NH3-dependent NAD+ synthetase from Bacillus subtilis at 1 A resolution. , 2002, Acta crystallographica. Section D, Biological crystallography.

[19]  S Kriminski,et al.  Heat transfer from protein crystals: implications for flash-cooling and X-ray beam heating. , 2003, Acta crystallographica. Section D, Biological crystallography.

[20]  Roderick MacKinnon,et al.  Gating the Selectivity Filter in ClC Chloride Channels , 2003, Science.

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[23]  H Luecke,et al.  Structure of bacteriorhodopsin at 1.55 A resolution. , 1999, Journal of molecular biology.

[24]  Youxing Jiang,et al.  Crystal structure and mechanism of a calcium-gated potassium channel , 2002, Nature.

[25]  P. Vekilov,et al.  Lower dimer impurity incorporation may result in higher perfection of HEWL crystals grown in microgravity: A case study , 1999 .

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[27]  M. Jansson,et al.  Fusion protein approach to improve the crystal quality of cytochrome bo(3) ubiquinol oxidase from Escherichia coli. , 2000, Biochimica et biophysica acta.

[28]  J. Møller,et al.  Interaction of membrane proteins and lipids with solubilizing detergents. , 2000, Biochimica et biophysica acta.

[29]  C. Carter,et al.  Quantitative analysis of crystal growth. Tryptophanyl-tRNA synthetase crystal polymorphism and its relationship to catalysis. , 1994, Journal of molecular biology.

[30]  R. H. Hardin,et al.  A new approach to the construction of optimal designs , 1993 .

[31]  K. Schulten,et al.  The crystal structure of the light-harvesting complex II (B800-850) from Rhodospirillum molischianum. , 1996, Structure.

[32]  G. Schulz,et al.  Structure and function of a squalene cyclase. , 1997, Science.

[33]  J. Deisenhofer,et al.  Crystallization and preliminary structure of beef heart mitochondrial cytochrome-bc1 complex. , 1996, Biochimica et biophysica acta.

[34]  E. Garman,et al.  Cryocooling of macromolecular crystals: optimization methods. , 2003, Methods in enzymology.

[35]  J. Barber,et al.  Using rational screening and electron microscopy to optimize the crystallization of succinate:ubiquinone oxidoreductase from Escherichia coli. , 2003, Acta crystallographica. Section D, Biological crystallography.

[36]  D. Oesterhelt,et al.  Structure of the light-driven chloride pump halorhodopsin at 1.8 A resolution. , 2000, Science.

[37]  S. Veesler,et al.  Comparison of solubilities and molecular interactions of BPTI molecules giving different polymorphs , 1997 .

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[39]  G. Eichele,et al.  Repeated seeding technique for growing large single crystals of proteins. , 1981, Journal of molecular biology.

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[41]  H. Michel,et al.  New crystal form of the photosynthetic reaction centre from Rhodobacter sphaeroides of improved diffraction quality. , 1993, Journal of molecular biology.

[42]  A. McPherson A comparison of salts for the crystallization of macromolecules , 2001, Protein science : a publication of the Protein Society.

[43]  B. Hanson,et al.  The well-tempered protein crystal: annealing macromolecular crystals. , 2003, Methods in enzymology.

[44]  A. Puustinen,et al.  Purification, crystallization and preliminary crystallographic studies of an integral membrane protein, cytochrome bo3 ubiquinol oxidase from Escherichia coli. , 2000, Acta crystallographica. Section D, Biological crystallography.

[45]  D. Rees,et al.  Structure of the Escherichia coli fumarate reductase respiratory complex. , 1999, Science.

[46]  G. Rummel,et al.  Trigonal crystals of porin from Escherichia coli. , 1991, Journal of molecular biology.

[47]  J Koepke,et al.  Structure at 2.3 A resolution of the cytochrome bc(1) complex from the yeast Saccharomyces cerevisiae co-crystallized with an antibody Fv fragment. , 2000, Structure.

[48]  Z. Chen,et al.  Crystallization and preliminary diffraction studies of two quinoprotein alcohol dehydrogenases (ADHs): a soluble monomeric ADH from Pseudomonas putida HK5 (ADH-IIB) and a heterotrimeric membrane-bound ADH from Gluconobacter suboxydans (ADH-GS). , 1999, Acta crystallographica. Section D, Biological crystallography.

[49]  E H Snell,et al.  A test of macromolecular crystallization in microgravity: large well ordered insulin crystals. , 2001, Acta crystallographica. Section D, Biological crystallography.

[50]  S. Iwata,et al.  Structure and Mechanism of the Lactose Permease of Escherichia coli , 2003, Science.

[51]  P. Fromme,et al.  Photosystem I at 4 Å resolution represents the first structural model of a joint photosynthetic reaction centre and core antenna system , 1996, Nature Structural Biology.

[52]  Andrea Mattevi,et al.  Structure of human monoamine oxidase B, a drug target for the treatment of neurological disorders , 2002, Nature Structural Biology.

[53]  J. Deisenhofer,et al.  Crystallization and preliminary X-ray analysis of ferric enterobactin receptor FepA, an integral membrane protein from Escherichia coli. , 1998, Acta crystallographica. Section D, Biological crystallography.

[54]  M. Schiffer,et al.  The structure of a mutant photosynthetic reaction center shows unexpected changes in main chain orientations and quinone position. , 2002, Biochemistry.

[55]  R. Thorne,et al.  X-ray topographic studies of protein crystal perfection and growth. , 1997, Acta Crystallographica Section D: Biological Crystallography.

[56]  M. Achtman,et al.  Expression, refolding and crystallization of the OpcA invasin from Neisseria meningitidis. , 2001, Acta crystallographica. Section D, Biological crystallography.

[57]  R. Huber,et al.  Structure and mechanism of the aberrant ba3‐cytochrome c oxidase from Thermus thermophilus , 2000, The EMBO journal.

[58]  P. Vekilov Molecular mechanisms of defect formation. , 2003, Methods in enzymology.

[59]  A. Ducruix,et al.  No salting-in of lysozyme chloride observed at low ionic strength over a large range of pH. , 1997, Biophysical journal.

[60]  C. Hunte Insights from the structure of the yeast cytochrome bc 1 complex: crystallization of membrane proteins with antibody fragments , 2001, FEBS letters.

[61]  Rosenberger,et al.  Nonlinear response of layer growth dynamics in the mixed kinetics-bulk-transport regime. , 1996, Physical review. E, Statistical physics, plasmas, fluids, and related interdisciplinary topics.

[62]  V. Cherezov,et al.  Crystallization screens: compatibility with the lipidic cubic phase for in meso crystallization of membrane proteins. , 2001, Biophysical journal.

[63]  E. Pebay-Peyroula,et al.  X-ray structure of bacteriorhodopsin at 2.5 angstroms from microcrystals grown in lipidic cubic phases. , 1997, Science.

[64]  A. Ducruix,et al.  Relative effectiveness of various ions on the solubility and crystal growth of lysozyme. , 1989, The Journal of biological chemistry.

[65]  R. Schekman,et al.  Ten proteins required for conversion of phiX174 single-stranded DNA to duplex form in vitro. Resolution and reconstitution. , 1975, The Journal of biological chemistry.

[66]  Mitsuo Ataka,et al.  Systematic studies on the crystallization of lysozyme: Determination and use of phase diagrams , 1988 .

[67]  M. Kokkinidis,et al.  Solubility, crystallization and chromatographic properties of macromolecules strongly depend on substances that reduce the ionic strength of the solution. , 1997, Protein Engineering.

[68]  A G Leslie,et al.  Molecular architecture of the rotary motor in ATP synthase. , 1999, Science.

[69]  G. Borgstahl,et al.  Macromolecular crystal quality. , 2013, Methods in enzymology.

[70]  K. Diederichs,et al.  An internal affinity‐tag for purification and crystallization of the siderophore receptor fhua, integral outer membrane protein from escherichia coli K‐12 , 1998, Protein science : a publication of the Protein Society.

[71]  C. Carter,et al.  Quantitative analysis in the characterization and optimization of protein crystal growth. , 1994, Acta crystallographica. Section D, Biological crystallography.

[72]  Reginald W. James,et al.  The Optical principles of the diffraction of X-rays , 1948 .

[73]  R. Dutzler,et al.  X-ray structure of a ClC chloride channel at 3.0 Å reveals the molecular basis of anion selectivity , 2002, Nature.

[74]  A. Engel,et al.  Large‐scale purification of functional recombinant human aquaporin‐2 , 2001, FEBS letters.

[75]  G. Schulz,et al.  Crystals of an integral membrane protein diffracting to 1.8 A resolution. , 1991, Journal of molecular biology.

[76]  G. Schulz,et al.  Strategy for membrane protein crystallization exemplified with OmpA and OmpX , 1999, Proteins.

[77]  T. Tomizaki,et al.  The Whole Structure of the 13-Subunit Oxidized Cytochrome c Oxidase at 2.8 Å , 1996, Science.

[78]  Manfred Auer,et al.  Structure of fumarate reductase from Wolinella succinogenes at 2.2 Å resolution , 1999, Nature.

[79]  N. Kamiya,et al.  Crystallization and the crystal properties of the oxygen-evolving photosystem II from Synechococcus vulcanus. , 2000, Biochemistry.

[80]  A. Ducruix,et al.  Relative effectiveness of various anions on the solubility of acidic Hypoderma lineatum collagenase at pH 7.2 , 1995, Protein science : a publication of the Protein Society.

[81]  Hartmut Michel,et al.  Structure at 2.8 Å resolution of cytochrome c oxidase from Paracoccus denitrificans , 1995, Nature.

[82]  K. Diederichs,et al.  Crystallization and preliminary X-ray crystallographic studies of the native and chemically modified anion-selective porin from Comamonas acidovorans. , 1998, Acta crystallographica. Section D, Biological crystallography.

[83]  Petra Fromme,et al.  Improved isolation and crystallization of photosystem I for structural analysis , 1998 .

[84]  A. Ducruix,et al.  [3] Inferences drawn from physicochemical studies of crystallogenesis and precrystalline state. , 1997, Methods in enzymology.

[85]  R. Kurumbail,et al.  Structural basis for selective inhibition of cyclooxygenase-2 by anti-inflammatory agents , 1997, Nature.

[86]  J. Deisenhofer,et al.  Crystal structure of the outer membrane active transporter FepA from Escherichia coli , 1999, Nature Structural Biology.

[87]  J. Chow,et al.  Flexibility of the NSAID binding site in the structure of human cyclooxygenase-2 , 1996, Nature Structural Biology.

[88]  R. MacKinnon,et al.  Chemistry of ion coordination and hydration revealed by a K+ channel–Fab complex at 2.0 Å resolution , 2001, Nature.

[89]  J. Gouaux,et al.  Subunit stoichiometry of staphylococcal alpha-hemolysin in crystals and on membranes: a heptameric transmembrane pore. , 1994, Proceedings of the National Academy of Sciences of the United States of America.

[90]  R. Dutzler,et al.  Crystal structure and functional characterization of OmpK36, the osmoporin of Klebsiella pneumoniae. , 1999, Structure.

[91]  T. A. Link,et al.  Complete structure of the 11-subunit bovine mitochondrial cytochrome bc1 complex. , 1998, Science.

[92]  M. Riès-Kautt,et al.  Strong and specific effects of cations on lysozyme chloride solubility. , 2002, Acta crystallographica. Section D, Biological crystallography.

[93]  K. H. Kalk,et al.  Structural evidence for dimerization-regulated activation of an integral membrane phospholipase. , 1999 .

[94]  W. Lehmann,et al.  Lipid patches in membrane protein oligomers: crystal structure of the bacteriorhodopsin-lipid complex. , 1998, Proceedings of the National Academy of Sciences of the United States of America.

[95]  M. Page,et al.  Crystallization and preliminary X-ray characterization of maltoporin from Escherichia coli. , 1990, Journal of molecular biology.

[96]  G. Rummel,et al.  Lipidic Cubic Phases: New Matrices for the Three-Dimensional Crystallization of Membrane Proteins. , 1998, Journal of structural biology.

[97]  J Deisenhofer,et al.  Crystal structure of the cytochrome bc1 complex from bovine heart mitochondria. , 1997, Science.

[98]  J. García-Ruiz,et al.  Counterdiffusion methods for macromolecular crystallization. , 2003, Methods in enzymology.

[99]  T. Tomizaki,et al.  Structures of metal sites of oxidized bovine heart cytochrome c oxidase at 2.8 A , 1995, Science.

[100]  D. Fu,et al.  Structure of a glycerol-conducting channel and the basis for its selectivity. , 2000, Science.

[101]  K. Diederichs,et al.  Crystallization and preliminary X-ray analysis of the trehalose/maltose ABC transporter MalFGK2 from Thermococcus litoralis. , 2002, Acta crystallographica. Section D, Biological crystallography.

[102]  Kay Diederichs,et al.  Structure of the sucrose-specific porin ScrY from Salmonella typhimurium and its complex with sucrose , 1998, Nature Structural Biology.

[103]  K. Diederichs,et al.  Siderophore-mediated iron transport: crystal structure of FhuA with bound lipopolysaccharide. , 1998, Science.

[104]  Gerry McDermott,et al.  Structural Basis of Multiple Drug-Binding Capacity of the AcrB Multidrug Efflux Pump , 2003, Science.

[105]  C. Carter,et al.  Incomplete factorial and response surface methods in experimental design: yield optimization of tRNA(Trp) from in vitro T7 RNA polymerase transcription. , 1996, Nucleic acids research.

[106]  F. Quiocho,et al.  Influence of divalent cations in protein crystallization , 1995, Protein science : a publication of the Protein Society.

[107]  A. Ducruix,et al.  Solubility diagram of the Rhodobacter sphaeroides reaction center as a function of PEG concentration , 1997, FEBS letters.

[108]  J. Hofrichter,et al.  Kinetics and mechanism of deoxyhemoglobin S gelation: a new approach to understanding sickle cell disease. , 1974, Proceedings of the National Academy of Sciences of the United States of America.

[109]  H. Michel,et al.  Fv fragment-mediated crystallization of the membrane protein bacterial cytochrome c oxidase , 1995, Nature Structural Biology.

[110]  Franz Rosenberger,et al.  Liquid-Liquid Phase Separation in Supersaturated Lysozyme Solutions and Associated Precipitate Formation/Crystallization , 1997 .

[111]  K. Inaka,et al.  Preliminary X‐ray crystallographic studies of photosynthetic reaction center from a thermophilic sulfur bacterium, Chromatium tepidum , 1994, FEBS letters.

[112]  G. Schulz,et al.  The structure of the outer membrane protein OmpX from Escherichia coli reveals possible mechanisms of virulence. , 1999, Structure.