Design and Optimization of Fully Thermally Coupled Distillation Columns: Part 1: Preliminary Design and Optimization Methodology

The design of a fully thermally coupled distillation column, or its thermodynamically equivalent arrangement, the dividing wall distillation column, is more complex than conventional arrangements because of the greater number of degrees of freedom. All of these degrees of freedom must be initialized before rigorous simulation can be performed. The distribution of stages in the various sections of the column, the reflux ratio, vapour and liquid splits on either side of the fully thermally coupled columns and feed condition must all be initialized. Yet these are important degrees of freedom that all interact with each other in the design. A new approach to the design of fully thermally coupled columns is proposed in this paper. The procedure uses the equilibrium stage composition concept developed for the design of azeotropic distillation systems 1 . The method is semi-rigorous in nature, providing an initial design that is very close to the results of rigorous simulation. The approach then allows the degrees of freedom to be optimized simultaneously and an optimized initial design established for rigorous simulation. A case study has been used to demonstrate the application of the new method.

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