Competitive grain growth and dendrite morphology evolution in selective laser melting of Inconel 718 superalloy

Abstract Microstructure control is a great challenge for selective laser melting (SLM) mainly because of nonuniform and ultra-rapid heating and cooling in the process. It is related to the control of dendrite morphology evolution and competitive grain growth by adjusting the process parameters of SLM. In this study, a multiscale simulation approach, which combines the finite element method (FEM) and the phase field (PF) method, is performed to investigate the dendrite morphology and stray grain growth under various SLM parameters for Inconel 718 superalloy. The cooling characteristics of melt pool, including the cooling rate, thermal gradient/solidification ratio (G/R), and the slope of the solidification front are investigated. Meanwhile, experiment verification adopting the manufacturing parameters identical to the simulation is performed. It is shown that simultaneously increasing or decreasing the laser power and scan speed leads to a drastic change of melt pool aspect ratio (MPAR), and this in turn affects the competitive growth of stray grains. Overall, a larger MPAR is found to suppress the growth of stray grains more effectively. Also, the experimental results are found to agree well with the simulation results. Three mechanisms of stray grain growth are revealed from the simulation results, and their roles are analzyed. This study provides important insights into the microstructure control in the laser additive manufacturing processes.

[1]  Wei Li,et al.  A two-dimensional simulation of grain structure growth within the substrate and the fusion zone during direct metal deposition , 2018, Comptes Rendus Mécanique.

[2]  Li Ma,et al.  Application of Finite Element, Phase-field, and CALPHAD-based Methods to Additive Manufacturing of Ni-based Superalloys. , 2017, Acta materialia.

[3]  Toshio Suzuki,et al.  Phase-field model for binary alloys. , 1999, Physical review. E, Statistical physics, plasmas, fluids, and related interdisciplinary topics.

[4]  Ryan R. Dehoff,et al.  Site specific control of crystallographic grain orientation through electron beam additive manufacturing , 2015 .

[5]  Yizhou Zhou,et al.  Formation of stray grains during directional solidification of a nickel-based superalloy , 2011 .

[6]  Rémy Glardon,et al.  Influence of Nd : YAG parameters on the selective laser sintering of metallic powders , 2001 .

[7]  K. Glasner Solute trapping and the non-equilibrium phase diagram for solidification of binary alloys , 2001 .

[8]  W. Liu,et al.  An extended free dendritic growth model incorporating the nonisothermal and nonisosolutal nature of the solid–liquid interface , 2015 .

[9]  Yucheng Liu,et al.  Investigation on Microsegregation of IN718 Alloy During Additive Manufacturing via Integrated Phase-Field and Finite-Element Modeling , 2018, Journal of Materials Engineering and Performance.

[10]  K. Chou,et al.  Microstructure simulations of Inconel 718 during selective laser melting using a phase field model , 2018, The International Journal of Advanced Manufacturing Technology.

[11]  C. Y. Wang,et al.  Multi-scale simulation of dendrite growth for direct energy deposition of nickel-based superalloys , 2019, Materials & Design.

[12]  Gerald L. Knapp,et al.  Experiments and simulations on solidification microstructure for Inconel 718 in powder bed fusion electron beam additive manufacturing , 2019, Additive Manufacturing.

[13]  Xibing Gong,et al.  Phase-Field Modeling of Microstructure Evolution in Electron Beam Additive Manufacturing , 2015 .

[14]  Richard J. Wakeman,et al.  Packing densities of particles with log-normal size distributions , 1975 .

[15]  Tahany Ibrahim El-Wardany,et al.  Phase Field Simulations of Microstructure Evolution in IN718 using a Surrogate Ni–Fe–Nb Alloy during Laser Powder Bed Fusion , 2018, Metals.

[16]  A. Chiba,et al.  Molten pool behavior and effect of fluid flow on solidification conditions in selective electron beam melting (SEBM) of a biomedical Co-Cr-Mo alloy , 2019, Additive Manufacturing.

[17]  Moataz M. Attallah,et al.  On the role of melt flow into the surface structure and porosity development during selective laser melting , 2015 .

[18]  Li Ma,et al.  On the primary spacing and microsegregation of cellular dendrites in laser deposited Ni–Nb alloys , 2017, 1705.06669.

[19]  Mark F. Horstemeyer,et al.  Insight into the mechanisms of columnar to equiaxed grain transition during metallic additive manufacturing , 2019, Additive Manufacturing.

[20]  T. DebRoy,et al.  Crystal growth during keyhole mode laser welding , 2017 .

[21]  T. DebRoy,et al.  Laser weld geometry and microstructure of cast Uranium-6 wt% niobium alloy , 2018, Journal of Nuclear Materials.

[22]  C. Gandin,et al.  A 3D Cellular Automaton algorithm for the prediction of dendritic grain growth , 1997 .

[23]  Strongly Out-of-Equilibrium Columnar Solidification During Laser Powder-Bed Fusion in Additive Manufacturing , 2018, Physical Review Applied.

[24]  Matthias Markl,et al.  3D multi-layer grain structure simulation of powder bed fusion additive manufacturing , 2018, Acta Materialia.

[25]  J. Kruth,et al.  Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder , 2013 .

[26]  Matthias Markl,et al.  A coupled Cellular Automaton–Lattice Boltzmann model for grain structure simulation during additive manufacturing , 2016 .

[27]  Yuwen Zhang,et al.  Partial Melting and Resolidification of Metal Powder in Selective Laser Sintering , 2006 .

[28]  M. Knezevic,et al.  Microstructure and mechanical behavior of direct metal laser sintered Inconel alloy 718 , 2016 .

[29]  Alexandre Furtado Ferreira,et al.  Simulation of the solidification of pure nickel via the phase-field method , 2006 .

[30]  Pradip Dutta,et al.  Three-dimensional double-diffusive convection and macrosegregation during non-equilibrium solidification of binary mixtures , 2003 .

[31]  Ming Gao,et al.  Effects of processing parameters on tensile properties of selective laser melted 304 stainless steel , 2013 .

[32]  Y. Shin,et al.  Multi-scale modeling of solidification and microstructure development in laser keyhole welding process for austenitic stainless steel , 2015 .

[33]  Wilfried Kurz,et al.  Solidification microstructures: A conceptual approach , 1994 .

[34]  R. Kobayashi Modeling and numerical simulations of dendritic crystal growth , 1993 .

[35]  Jean-Pierre Kruth,et al.  Quality control of laser- and powder bed-based Additive Manufacturing (AM) technologies , 2010 .

[36]  Kui Liu,et al.  Effect of cooling rate on microstructure, microsegregation and mechanical properties of cast Ni-based superalloy K417G , 2017 .

[37]  Andreas Lundbäck,et al.  Simulation and validation of TIG-welding and post weld heat treatment of an Inconel 718 plate , 2005 .

[38]  V. Pavlyk,et al.  Simulation of weld solidification microstructure and its coupling to the macroscopic heat and fluid flow modelling , 2004 .

[39]  P. Sahm,et al.  Primary spacing in directional solidification , 1998 .

[40]  Jose María Cabrera,et al.  High temperature deformation of Inconel 718 , 2006 .

[41]  Philip B. Prangnell,et al.  Effect of build geometry on the β-grain structure and texture in additive manufacture of Ti6Al4V by selective electron beam melting , 2013 .

[42]  Jie Yin,et al.  Simulation of temperature distribution in single metallic powder layer for laser micro-sintering , 2012 .

[43]  Non-equilibrium solidification of undercooled metallic metls , 1994 .

[44]  W. Kurz,et al.  SINGLE-CRYSTAL LASER DEPOSITION OF SUPERALLOYS: PROCESSING-MICROSTRUCTURE MAPS , 2001 .

[45]  Robert F. Singer,et al.  Grain structure evolution in Inconel 718 during selective electron beam melting , 2016 .

[46]  Y. F. Wang,et al.  Density and molar volume of liquid Ni–Co binary alloys , 2006 .

[47]  O. Ojo,et al.  Numerical modeling of microstructure evolution during laser additive manufacturing of a nickel-based superalloy , 2014 .

[48]  John W. Elmer,et al.  Origin of grain orientation during solidification of an aluminum alloy , 2016 .