Damage-Resistant SiC–AlN Layered Composites with Surface Compressive Stresses

Three-layer samples in the SiC-AlN system with outer layers richer in SiC, as well as monolithic samples of uniform composition, were fabricated by hot-pressing. The strain gage technique, previously described, was used to estimate residual compressive stress in the outer layers developed because of the difference in coefficients of thermal expansion between inner and outer layers. Bar-shaped samples were indented using a Vickers indenter under loads as high as 20 kg (196 N) on outer layers and were fractured in three-point bending. Three-layer samples with outer layers under compression exhibited increased resistance to the contact-induced damage in comparison to the monoclinic samples.

[1]  Jow-Lay Huang,et al.  Strengthening of Oxide Ceramics by Transformation‐Induced Stress , 1987 .

[2]  Chun-Hway Hsueh,et al.  Toughening Behavior in Whisker‐Reinforced Ceramic Matrix Composites , 1988 .

[3]  D. Shetty,et al.  Strength Improvement in Transformation‐Toughened Alumina by Selective Phase Transformation , 1987 .

[4]  B. Lawn,et al.  Residual stress effects in sharp contact cracking , 1979 .

[5]  G. C. Wei,et al.  Toughening Behavior in Sic‐Whisker‐Reinforced Alumina , 1984 .

[6]  M. Janney Mechanical properties and oxidation behavior of a hot-pressed SiC-15-vol%-TiB/sub 2/ composite , 1987 .

[7]  R. Ruh,et al.  Phase Relationships in the Silicon Carbide‐Aluminum Nitride System , 1988 .

[8]  R. Ruh,et al.  Composition and Properties of Hot‐Pressed SiC‐AIN Solid Solutions , 1982 .

[9]  A. Virkar,et al.  Indentation Fracture Response and Damage Resistance of Al2O3‐ZrO2 Composites Strengthened by Transformation‐Induced Residual Stresses , 1988 .

[10]  G. C. Wei,et al.  Development of SiC-whisker-reinforced ceramics , 1985 .

[11]  M. Swain Grinding-induced tempering of ceramics containing metastable tetragonal zirconia , 1980 .

[12]  J. Garnier,et al.  Microstructure and material properties of SiC-TiB/sub 2/ particulate composites , 1987 .

[13]  A. Virkar,et al.  Measurement of Residual Stresses in Oxide–ZrO2 Three‐Layer Composites , 1988 .

[14]  F. Lange,et al.  Compressive Surface Stresses Developed in Ceramics by an Oxidation-Induced Phase Change , 1980 .

[15]  A. Virkar,et al.  Fabrication and characterization of SiC-AIN alloys , 1981 .

[16]  Brian R. Lawn,et al.  Residual stress effects in sharp contact cracking , 1979 .

[17]  D. J. Green A Technique for Introducing Surface Compression into Zirconia Ceramics , 1983 .

[18]  T. Masaki,et al.  Mechanical properties of highly toughened ZrO2Y2O3 , 1987 .