Experimental Investigation of Spontaneous Imbibition in a Tight Reservoir with Nuclear Magnetic Resonance Testing

Hydraulic fracturing is the significant technology for exploiting tight resources. Spontaneous water imbibition is an important mechanism governing the process of hydraulic fracturing, and the water imbibition from the fracture into the matrix is an essential factor that affects the reservoir production performance. In this study, imbibition experiments and nuclear magnetic resonance (NMR) testing were combined to analyze fluid flow tight core samples in a pore-scale level. The imbibition experiments were categorized into two systems, the gas/water/rock system and the oil/water/rock system. The NMR measurements were performed at different times for these two systems. The relationship between T2 relaxation time, pore radius, and pore types was established. Theoretical models describing water imbibition into porous media were used to facilitate the interpretation of the experimental results. The results demonstrate that the volume of imbibed water is large during the early imbibition period and that the imb...

[1]  T. Babadagli Analysis of Oil Recovery by Spontaneous Imbibition of Surfactant Solution , 2003 .

[2]  B. J. Bourbiaux,et al.  Experimental study of cocurrent and countercurrent flows in natural porous media , 1990 .

[3]  Mark A. Knackstedt,et al.  Spontaneous imbibition in Small Cores , 2007 .

[4]  Hossein Kazemi,et al.  Experimental and Numerical Simulation Of Surfactant-Assisted Oil Recovery In Tight Fractured Carbonate Reservoir Cores , 2012 .

[5]  M. Girard,et al.  A New Technique For Reservoir Wettability Characterization , 1994 .

[6]  H. Dehghanpour,et al.  Liquid uptake of gas shales: A workflow to estimate water loss during shut-in periods after fracturing operations , 2014 .

[7]  Zou Cai,et al.  First discovery of nano-pore throat in oil and gas reservoir in China and its scientific value , 2011 .

[8]  Ramez Masoud Azmy,et al.  Wettability Challenges in Carbonate Reservoirs , 2010 .

[9]  S. Saleh,et al.  Oil recovery in fractured oil reservoirs by low IFT imbibition process , 1996 .

[10]  Q. Lan,et al.  Spontaneous Imbibition of Brine and Oil in Gas Shales: Effect of Water Adsorption and Resulting Microfractures , 2013 .

[11]  Xiangyun Hu,et al.  An analytical model for spontaneous imbibition in fractal porous media including gravity , 2012 .

[12]  L. Larrondo,et al.  Experimental Investigation of the Effects of Temperature, Pressure, and Crude Oil Composition on Interfacial Properties , 1986 .

[13]  William G. Anderson,et al.  Wettability Literature Survey- Part 2: Wettability Measurement , 1986 .

[14]  N. Morrow,et al.  INITIAL WATER SATURATION AND OIL RECOVERY FROM CHALK AND SANDSTONE BY SPONTANEOUS IMBIBITION , 1999 .

[15]  Zengmin Lun,et al.  Nuclear Magnetic Resonance Study on Mechanisms of Oil Mobilization in Tight Reservoir Exposed to CO 2 in Pore Scale , 2016 .

[16]  K. Mohanty,et al.  Wettability Alteration in a Tight Oil Reservoir , 2013 .

[17]  Kewen Li,et al.  Characterization of Spontaneous Water Imbibition into Gas-Saturated Rocks , 2000 .

[18]  Robert P. Ewing,et al.  Low pore connectivity in natural rock. , 2012, Journal of contaminant hydrology.

[19]  Carl H. Sondergeld,et al.  NMR Study of Shale Wettability , 2011 .

[20]  Roland N. Horne,et al.  Generalized Scaling Approach for Spontaneous Imbibition: An Analytical Model , 2006 .

[21]  Anjani Kumar,et al.  Shale Gas Modeling Workflow: From Microseismic to Simulation -- A Horn River Case Study , 2011 .

[22]  Charles Flaum,et al.  Wettability, Saturation, and Viscosity From NMR Measurements , 2003 .

[23]  Generalized Scaling Of Spontaneous Imbibition Data For Strongly Water-Wet Systems , 1995 .

[24]  Mingzhen Wei,et al.  Microfracture and Surfactant Impact on Linear Cocurrent Brine Imbibition in Gas-Saturated Shale , 2015 .

[25]  Aifen Li,et al.  Spontaneous Imbibition Laws and the Optimal Formulation of Fracturing Fluid during Hydraulic Fracturing in Ordos Basin , 2015 .

[26]  Walter Rose,et al.  Modeling forced versus spontaneous capillary imbibition processes commonly occurring in porous sediments , 2001 .

[27]  A. Firoozabadi,et al.  Cocurrent and Countercurrent Imbibition in a Water-Wet Matrix Block , 2000 .

[28]  Jianchao Cai,et al.  Fractal Characterization of Spontaneous Co-current Imbibition in Porous Media , 2010 .

[29]  F. Orr,et al.  Low IFT drainage and imbibition , 1994 .

[30]  Anthony R. Kovscek,et al.  Scaling of counter-current imbibition processes in low-permeability porous media , 2002 .

[31]  Zhengfu Ning,et al.  Applicability Comparison of Nuclear Magnetic Resonance and Mercury Injection Capillary Pressure in Characterisation Pore Structure of Tight Oil Reservoirs , 2015 .

[32]  M. Mørk,et al.  Complexity of Wettability Analysis in Heterogeneous Carbonate Rocks, A Case Study , 2012 .

[33]  Roland N. Horne,et al.  An Analytical Scaling Method for Spontaneous Imbibition in Gas/Water/Rock Systems , 2004 .

[34]  R. Seright,et al.  Wettability Survey in Bakken Shale Using Surfactant Formulation Imbibition , 2012 .

[35]  Randall S. Seright,et al.  Wettability Survey in Bakken Shale With Surfactant-Formulation Imbibition , 2012 .

[36]  T. Babadagli Scaling capillary imbibition during static thermal and dynamic fracture flow conditions , 2002 .

[37]  A. Mirzaei-Paiaman Analysis of counter-current spontaneous imbibition in presence of resistive gravity forces: Displacement characteristics and scaling , 2015 .

[38]  Basabdatta Roychaudhuri,et al.  An Experimental and Numerical Investigation of Spontaneous Imbibition in Gas Shales , 2011 .

[39]  Dongmei Wang,et al.  Flow-Rate Behavior and Imbibition in Shale , 2011 .

[40]  Wenming Ji,et al.  Research on the auto-removal mechanism of shale aqueous phase trapping using low field nuclear magnetic resonance technique , 2016 .

[41]  G. Hamon Field-Wide Variations of Wettability , 2000 .

[42]  H. Zhiming,et al.  Microscopic pore characteristics of different lithological reservoirs , 2016 .

[43]  Hasan O. Yildiz,et al.  Effect of shape factor, characteristic length, and boundary conditions on spontaneous imbibition , 2006 .

[44]  Zhi Yang,et al.  Nano-hydrocarbon and the accumulation in coexisting source and reservoir , 2012 .

[45]  C. Sondergeld,et al.  Nuclear-Magnetic-Resonance Response of Brine, Oil, and Methane in Organic-Rich Shales , 2015 .

[46]  Roland Glantz,et al.  Tight dual models of pore spaces , 2008 .

[47]  Shouxiang Ma,et al.  Experimental verification of a modified scaling group for spontaneous imbibition , 1996 .

[48]  A. Kovscek,et al.  Spontaneous countercurrent imbibition and forced displacement characteristics of low-permeability, siliceous shale rocks , 2010 .

[49]  C. C. Mattax,et al.  Imbibition Oil Recovery from Fractured, Water-Drive Reservoir , 1962 .