Optimized liquid chromatography-mass spectrometry approach for the isolation of minor stress biomarkers in plant extracts and their identification by capillary nuclear magnetic resonance.

[1]  Serge Rudaz,et al.  Development of a two-step screening ESI-TOF-MS method for rapid determination of significant stress-induced metabolome modifications in plant leaf extracts: the wound response in Arabidopsis thaliana as a case study. , 2007, Journal of separation science.

[2]  P. Petersson,et al.  Characterisation of RPLC columns packed with porous sub-2 μm particles , 2007 .

[3]  D. Leibfritz,et al.  Characterization of sphingomyelins in lipid extracts using a HPLC-MS-Offline-NMR method. , 2007, Analytical chemistry.

[4]  Serge Rudaz,et al.  Multivariate data analysis of rapid LC-TOF/MS experiments from Arabidopsis thaliana stressed by wounding , 2007 .

[5]  Yuichi Kobayashi,et al.  First total synthesis of tuberonic acid , 2007 .

[6]  J. Vervoort,et al.  Identification of the major constituents of Hypericum perforatum by LC/SPE/NMR and/or LC/MS. , 2007, Phytochemistry.

[7]  Y. Shachar-Hill,et al.  Innovations: Towards the plant metabolome and beyond , 2007, Nature Reviews Molecular Cell Biology.

[8]  Jean-Luc Wolfender,et al.  Identification of natural products using HPLC-SPE combined with CapNMR. , 2007, Analytical chemistry.

[9]  D. Kell.  Systems biology, metabolic modelling and metabolomics in drug discovery and development. , 2006, Drug discovery today.

[10]  F. Schroeder,et al.  Extending the scope of NMR spectroscopy with microcoil probes. , 2006, Angewandte Chemie.

[11]  John E Hale,et al.  The role of mass spectrometry in biomarker discovery and measurement. , 2006, Current drug metabolism.

[12]  Y. Choi,et al.  Metabolic differentiation of Arabidopsis treated with methyl jasmonate using nuclear magnetic resonance spectroscopy , 2006 .

[13]  Zheng Yang,et al.  Online hyphenated liquid chromatography-nuclear magnetic resonance spectroscopy-mass spectrometry for drug metabolite and nature product analysis. , 2006, Journal of pharmaceutical and biomedical analysis.

[14]  R. Hall,et al.  Plant metabolomics: from holistic hope, to hype, to hot topic. , 2006, The New phytologist.

[15]  W. Weckwerth,et al.  Metabolomics: from pattern recognition to biological interpretation. , 2005, Drug discovery today.

[16]  Kothandaraman Narasimhan,et al.  Metabolomics and its role in understanding cellular responses in plants , 2005, Plant Cell Reports.

[17]  Jean-Luc Wolfender,et al.  Phytochemistry in the microgram domain—a LC–NMR perspective , 2005, Magnetic resonance in chemistry : MRC.

[18]  P. Carr,et al.  A practical approach to transferring linear gradient elution methods. , 2005, Journal of chromatography. A.

[19]  M. O'Neil-Johnson,et al.  Application of capillary-scale NMR for the structure determination of phytochemicals. , 2005, Phytochemical analysis : PCA.

[20]  A. G. Wilson,et al.  Microflow NMR: concepts and capabilities. , 2004, Analytical chemistry.

[21]  T. Jira,et al.  Extracolumn band broadening in capillary liquid chromatography. , 2003, Journal of chromatography. A.

[22]  E. Farmer,et al.  Jasmonates and related oxylipins in plant responses to pathogenesis and herbivory. , 2003, Current opinion in plant biology.

[23]  R. Sparks,et al.  Optimizing Preparative LC/MS Configurations and Methods for Parallel Synthesis Purification , 2003 .

[24]  Manfred Spraul,et al.  LC-NMR-MS in drug discovery. , 2003, Drug discovery today.

[25]  C. Wasternack,et al.  Biochemical and Molecular Characterization of a Hydroxyjasmonate Sulfotransferase from Arabidopsis thaliana * , 2003, The Journal of Biological Chemistry.

[26]  R. Dixon,et al.  Plant metabolomics: large-scale phytochemistry in the functional genomics era. , 2003, Phytochemistry.

[27]  W. Niessen,et al.  Developing strategies for isolation of minor impurities with mass spectrometry-directed fractionation. , 2002, Journal of chromatography. A.

[28]  J. Dolan,et al.  Maintaining fixed band spacing when changing column dimensions in gradient elution. , 1998, Journal of chromatography. A.

[29]  B. Shushan,et al.  Automated analytical/preparative high-performance liquid chromatography–mass spectrometry system for the rapid characterization and purification of compound libraries , 1998 .

[30]  E. Farmer,et al.  Dinor-oxo-phytodienoic acid: a new hexadecanoid signal in the jasmonate family. , 1997, Proceedings of the National Academy of Sciences of the United States of America.

[31]  G. Cordell,et al.  A general method for the dereplication of flavonoid glycosides utilizing high performance liquid chromatography/mass spectrometric analysis , 1997 .

[32]  J. Quail,et al.  Importance of the Chiral Centers of Jasmonic Acid in the Responses of Plants (Activities and Antagonism between Natural and Synthetic Analogs) , 1997, Plant physiology.

[33]  E. Lesellier,et al.  Computerized optimization of RP-HPLC separation with nonaqueous or partially aqueous mobile phases , 1997 .

[34]  M. Nakayama,et al.  Two Jasmonoid Glucosides and a Phenylvaleric Acid Glucoside from Perilla frutescens , 1996 .

[35]  D. Vreugdenhil,et al.  Occurrence of hydroxylated jasmonic acids in leaflets of Solanum demissum plants grown under long- and short-day conditions. , 1993, Physiologia plantarum.