SCANNING ELECTRON MICROSCOPE AND ACOUSTIC EMISSION STUDIES OF CRACK DEVELOPMENT IN ROCKS

Abstract The microcracks and voids contained in rocks affect their fracture, elastic, thermal and electrical properties. This investigation assesses methods for revealing cracks in unstressed rock and cracks developed during uniaxial and triaxial compression up to failure, using three different rocks: microgranodiorite, dolerite and marble. The techniques used are scanning electron microscope (SEM) analysis of ion-beam etched surfaces, and acoustic emission (AE) measurements. The results are compared with other published data on cracks in rocks and from this a more general picture can be drawn of void/crack development and of damage growth during deformation from zero load up to failure in compression.

[1]  Surface morphology during ion etching The influence of redeposition , 1983 .

[2]  The Theory of Brittle Fracture Initiation under Triaxial Stress Conditions—II , 1970 .

[3]  Failure Prediction in Structural Ceramics Using Acoustic Emission , 1973 .

[4]  Kiyoo Mogi,et al.  Study of Elastic Shocks Caused by the Fracture of Heterogeneous Materials and its Relations to Earthquake Phenomena , 1962 .

[5]  Makoto Terada,et al.  A study on the time-dependent microfracturing and strength of Oshima granite , 1982 .

[6]  Michael V. Swain,et al.  Some observations of overlapping interacting cracks , 1978 .

[7]  S. Murrell,et al.  Some New Rheological Experiments on Igneous Rocks at Temperatures up to 1120°C , 1973 .

[8]  Edward D. Pittman,et al.  Use of Pore Casts and Scanning Electron Microscope to Study Pore Geometry , 1970 .

[9]  C. Scholz The frequency-magnitude relation of microfracturing in rock and its relation to earthquakes , 1968 .

[10]  S. G. Sarkisyan Application of the scanning electron microscope in the investigation of oil and gas reservoir rocks , 1971 .

[11]  Christopher H. Scholz,et al.  Microfracturing and the inelastic deformation of rock in compression , 1968 .

[12]  L. Dengler Microcracks in Crystalline Rocks , 1976 .

[13]  W. Brace,et al.  Direct observation of microcavities in crystalline rocks , 1974 .

[14]  S. Murrell,et al.  Experimental observations on rock fracture at pressures up to 7 kbar and the implications for earthquake faulting , 1973 .

[15]  Carla W. Montgomery,et al.  Micropores in plagioclase , 1975 .

[16]  R. M. Weinbrandt,et al.  A Scanning Electron Microscope Study of the Pore Structure of Sandstone , 1969 .

[17]  B. Gutenberg,et al.  Seismicity of the Earth and associated phenomena , 1950, MAUSAM.

[18]  C. B. Scruby,et al.  Quantitative acoustic emission source characterisation during low temperature cleavage and intergranular fracture , 1981 .

[19]  W. B. Hempkins,et al.  Scanning electron microscope study of pore systems in rocks , 1971 .

[20]  B. Lawn,et al.  Cleavage step deformation in brittle solids , 1974 .

[21]  R. Kranz,et al.  Crack-crack and crack-pore interactions in stressed granite , 1979 .

[22]  D. Lockner,et al.  Acoustic emission and creep in rock at high confining pressure and differential stress , 1977 .

[23]  D. J. Barber Thin foils of non-metals made for electron microscopy by sputter-etching , 1970 .

[24]  S. Murrell,et al.  An Experimental Study of the Effect of Temperature and Stress on the Creep of Rocks , 1965 .

[25]  Makoto Terada,et al.  Influence of strain rate on dilatancy and strength of Oshima granite under uniaxial compression , 1981 .

[26]  D. J. Barber,et al.  Development of the surface topography on silica glass due to ion-bombardment , 1972 .

[27]  A. Heuer,et al.  An Improved Ion Thinning Apparatus , 1971 .

[28]  M. Paterson Experimental Rock Deformation: The Brittle Field , 1978 .

[29]  M. Paulus,et al.  Dispositif de bombardement ionique pour préparations micrographiques , 1961 .

[30]  S. Murrell The theory of the propagation of elliptical Griffith cracks under various conditions of plane strain or plane stress: Part I , 1964 .

[31]  C. H. Scholz,et al.  Experimental study of the fracturing process in brittle rock , 1968 .

[32]  D. L. Anderson,et al.  Travel times, apparent velocities and amplitudes of body waves , 1968 .

[33]  R. Kranz,et al.  CRACK GROWTH AND DEVELOPMENT DURING CREEP OF BARRE GRANITE , 1979 .

[34]  Francis T. Wu,et al.  Microfracturing and deformation of westerly granite under creep condition , 1975 .

[35]  G. Simmons,et al.  Effects of stress on cracks in Westerly granite , 1976 .

[36]  E. D. Pittman,et al.  Some Applications of Scanning Electron Microscopy to the Study of Reservoir Rock , 1979 .

[37]  J. E. Sinclair,et al.  The origin of acoustic emission during deformation of aluminium and an aluminium–magnesium alloy , 1981 .

[38]  Paul Tapponnier,et al.  Development of stress-induced microcracks in Westerly Granite , 1976 .

[39]  K. Mogi,et al.  Frequency characteristics of acoustic emission in rocks under uniaxial compression and its relation to the fracturing process to failure , 1982 .

[40]  S. Murrell,et al.  The effect of temperature on the strength at high confining pressure of granodiorite containing free and chemically-bound water , 1976 .

[41]  Mitiyasu Ohnaka,et al.  Frequency Dependence of Acoustic Emission Activity in Rocks under Incremental, Uniaxial Compression , 1981 .

[42]  D. J. Barber,et al.  Prediction of ion-bombarded surface topographies using Frank's kinematic theory of crystal dissolution , 1973 .

[43]  M. Ohnaka,et al.  Acoustic emission during creep of brittle rock , 1983 .

[44]  E. Silver,et al.  Cracks and Pores: A Closer Look , 1972, Science.

[45]  G. Fonseka,et al.  Ion beam etching in the study of cementitious materials , 1979 .

[46]  J. B. Auden,et al.  The Seismicity of the Earth 1953-1965 , 1970 .

[47]  A Statistical Study on the Occurrence of Small Earthquakes III , 1953 .

[48]  H. Bach Application of ion sputtering in preparing glasses and their surface layers for electron microscope investigations , 1970 .