Rigorous dynamic modelling and identification of distillation column using Aspen Plus

Knowledge of dynamic behavior of process plants is essential in designing, commissioning and operating process plants. Several advanced model based technologies require explicit dynamic models of the process plant. However, even the development of the dynamic model of a simple unit operation is very daunting, costly and time-consuming. This paper presents a rigorous dynamic simulation using Aspen Plus. The data from the dynamic simulation is then used to develop transfer function model of the column. This case study considers a distillation column with an ethanol-water feed. A 2×3 distillation column transfer function model is developed from step responses of the Aspen plus dynamic simulation, i.e. with feed valve opening %, reflux flow rate and reboiler duty as input and top and the bottom compositions as an output. A separate SISO transfer function from condenser duty to column pressure is also developed.

[1]  J. Prausnitz,et al.  Statistical thermodynamics of liquid mixtures: A new expression for the excess Gibbs energy of partly or completely miscible systems , 1975 .

[2]  William L. Luyben,et al.  Control of a multiunit heterogeneous azeotropic distillation process , 2006 .

[3]  R. K. Wood,et al.  Terminal composition control of a binary distillation column , 1973 .

[4]  S. Skogestad DYNAMICS AND CONTROL OF DISTILLATION COLUMNS A tutorial introduction , 1997 .

[5]  Stanley H. Johnson,et al.  Use of Hammerstein Models in Identification of Nonlinear Systems , 1991 .

[6]  M. Ramasamy,et al.  System Identification Using Orthonormal Basis Filters , 2010 .

[7]  W. Luyben Distillation Design and Control Using Aspen Simulation , 2006 .

[8]  S Hurowitz,et al.  Distillation control configuration selection , 2003 .

[9]  Lemma Dendena Tufa,et al.  Optimization and Dynamics of Distillation Column Using Aspen Plus , 2016 .

[10]  Rik Pintelon,et al.  System Identification: A Frequency Domain Approach , 2012 .

[11]  Fahim Uddin,et al.  Development of Regression Models by Closed–Loop Identification of Distillation Column - A Case Study , 2017 .

[12]  M. Rovaglio,et al.  Rigorous dynamics and control of continuous distillation systems—simulation and experimental results , 1990 .

[13]  William L. Luyben Aspen Dynamics simulation of a middle-vessel batch distillation process , 2015 .

[14]  Alexandre C. Dimian,et al.  Integrated design and simulation of chemical processes , 2003 .

[15]  Aidan O'Dwyer,et al.  Comparison of open and closed loop process identification techniques in the time domain , 2002 .

[16]  William L. Luyben Rigorous dynamic models for distillation safety analysis , 2012, Comput. Chem. Eng..

[17]  Iván D. Gil,et al.  Control of an extractive distillation process to dehydrate ethanol using glycerol as entrainer , 2012, Comput. Chem. Eng..

[18]  C. Marangoni,et al.  Dynamic Study of Distillation Column Operated with Tray Heat Source Combined with Reboiler , 2016 .

[19]  Jose Alvarez-Ramirez,et al.  An indirect feedforward composition controller for distillation columns , 2002 .

[20]  K. Boots,et al.  A Sustainable Ethanol Distillation System , 2012 .

[21]  William L. Luyben,et al.  Design and Control of Distillation Systems for Separating Azeotropes: Luyben/Azeotropes Distillation , 2010 .

[22]  B. Bruggen,et al.  Application of the mass-based UNIQUAC model to membrane systems: A critical revision , 2012 .