Rapid growth of KDP-type crystals

Growth of KDP-type crystals on the point seed made possible to accelerate growth rates from traditional 1 mm/day up to 50 mm/day. This acceleration gave base to a development of the rapid growth technique for production of single crystals with the linear sizes up to 90 cm to obtain plates for laser radiation conversion in world-largest lasers. Scientific bases and technological principles of the method are considered in this review.

[1]  Yuming Zhou,et al.  Three-dimensional computations of solution hydrodynamics during the growth of potassium dihydrogen phosphate I. Spin up and steady rotation , 1997 .

[2]  H. Miers,et al.  The spontaneous crystallisation of binary mixtures.— Experiments on Salol and Betol , 1907 .

[3]  G. Botsaris,et al.  Fundamental studies in secondary nucleation from solution , 1972 .

[4]  J. D. Lee,et al.  Oriented liquid inclusions in KDP crystals , 1996 .

[5]  Y. Kuznetsov,et al.  The effect of temperature on step motion; (101) ADP face , 1992 .

[6]  Chandrani Guin,et al.  Plastic strain and dislocation structure of the KDP group crystals , 1980 .

[7]  Tadashi Kanabe,et al.  Basic technology of fast growing for normal and partially deuterated KDP crystals , 1995, Other Conferences.

[8]  W. Kibalczyc,et al.  Light scattering study of KH2PO4 and BaSO4 nucleation process , 1986 .

[9]  V. M. Aleksandrov Contact problem taking into account the wear caused by local melting , 1986 .

[10]  A. E. Nielsen Kinetics of precipitation , 1964 .

[11]  P. F. Bordui Growth of large single crystals from aqueous solution: A review , 1987 .

[12]  M. S. Joshi,et al.  Nucleation in supersaturated potassium dihydrogen orthophosphate solutions , 1979 .

[13]  A. Chernov,et al.  Solution growth kinetics and mechanism: Prismatic face of ADP , 1986 .

[14]  A. Chernov,et al.  Secondary nucleation induced by the cracking of a growing crystal: KH2PO4 (KDP) and K(H,D)2PO4 (DKDP) , 1990 .

[15]  B. Shekunov,et al.  Morphology of growing vicinal surface; prismatic faces of ADP and KDP crystals in solutions , 1990 .

[16]  N. Kubota,et al.  Calculation of supercooling temperature for primary nucleation of potassium nitrate from aqueous solution by the two-kind active site model , 1986 .

[17]  J. Lindl Development of the indirect‐drive approach to inertial confinement fusion and the target physics basis for ignition and gain , 1995 .

[18]  A. Mersmann,et al.  How to predict the metastable zone width , 1998 .

[19]  K. Berglund,et al.  The structure of aqueous solutions of some dihydrogen orthophosphates by laser Raman spectroscopy , 1987 .

[20]  A. Chernov Stability of faceted shapes , 1974 .

[21]  H. Klapper Röntgentopographische untersuchungen der defektstrukturen im thioharnstoff , 1972 .

[22]  N. Zaitseva,et al.  Formation of “hair” inclusions in rapidly grown potassium dihydrogen phosphate crystals , 1996 .

[23]  O. Söhnel Surface tension of soluble inorganic salts, from crystallization measurements , 1978 .

[24]  James J. De Yoreo,et al.  Rapid growth of large-scale (40-55 cm) KDP crystals , 1997, Other Conferences.

[25]  A. Chernov,et al.  Growth of dipyramidal face of dislocation-free ADP crystals; free energy of steps , 1989 .

[26]  James J. De Yoreo,et al.  The evolution of growth modes and activity of growth sources on canavalin investigated by in situ atomic force microscopy , 2000 .

[27]  I. Nicolau Growth Kinetics of Potassium‐Dihydrogen Phosphate Crystals in Solution , 1974 .

[28]  R. Smoluchowski,et al.  Imperfections in crystals , 1961 .

[29]  W. Mccabe,et al.  Supersaturation and Crystal Formation in Seeded Solutions , 1934 .

[30]  S. Veintemillas-Verdaguer,et al.  Criteria for growing crystals from boiling solutions , 1987 .

[31]  E. Dieguez,et al.  Ultraviolet absorption and growth bands in KDP , 1985 .

[32]  V. F. Efimkov,et al.  Optical properties of KDP crystals grown at high growth rates , 1991, Other Conferences.

[33]  M. Cournil,et al.  Secondary nucleation of potassium dihydrogen phosphate (KDP): Interest of a turbidimetric study , 1992 .

[34]  Bruce W. Woods,et al.  Sources of optical distortion in rapidly grown crystals of KH2PO4 , 1996 .

[35]  J. Tejada,et al.  Unstable growth of ADP crystals , 1979 .

[36]  A. Chernov Formation of crystals in solutions , 1989 .

[37]  R. F. Strickland-Constable,et al.  Kinetics and Mechanism of Crystallization , 2018, Nucleation and Crystal Growth.

[38]  Predicting bulk damage in NIF triple harmonic generators , 1999, Laser Damage.

[39]  A. Yokotani,et al.  Growth of large KDP crystals for laser fusion experiments , 1990 .

[40]  E. Rudneva,et al.  Effect of the surface morphology on the grown‐in dislocation orientations in KDP crystals , 1994 .

[41]  N. Zaitseva,et al.  Growth phenomena in the surface layer and step generation from the crystal edges , 2001 .

[42]  S. J. Jančić,et al.  Crystallization from solution and the thermodynamics of electrolytes , 1977 .

[43]  G. Youngquist,et al.  Secondary nucleation of magnesium sulfate by fluid shear , 1973 .

[44]  Andrew Yeckel,et al.  Three-dimensional computations of solution hydrodynamics during the growth of potassium dihydrogen phosphate. II. Spin down , 1998 .

[45]  B. Tanner X-Ray Diffraction Topography , 1976 .

[46]  C. Bunn,et al.  Crystal growth from solution. I. Layer formation on crystal faces , 1949 .

[47]  G. Gilmer,et al.  An analysis of combined surface and volume diffusion processes in crystal growth , 1971 .

[48]  L. N. Rashkovich,et al.  Influence of Fe3+ and Al3+ ions on the kinetics of steps on the {1 0 0} faces of KDP , 1997 .

[49]  Y. Kuznetsov,et al.  Growth kinetics irregularities due to changed dislocation source activity; (101) ADP face , 1992 .

[50]  Natalia P. Zaitseva,et al.  The effect of impurities and supersaturation on the rapid growth of KDP crystals , 1999 .

[51]  A. Chernov,et al.  THE SPIRAL GROWTH OF CRYSTALS , 1961 .

[52]  Tadashi Kanabe,et al.  Optical properties of rapidly grown KDP crystal improved by thermal conditioning , 1997 .

[53]  Fred P. Milanovich,et al.  High‐laser‐damage‐threshold potassium dihydrogen phosphate crystals , 1990 .

[54]  A. Walker Growing piezoelectric crystals , 1950 .

[55]  A. R. Lang The projection topograph: a new method in X‐ray diffraction microradiography , 1959 .

[56]  A. Myerson,et al.  Thermodynamics, cluster formation and crystal growth in highly supersaturated solutions of KDP, ADP and TGS , 1997 .

[57]  David Turnbull,et al.  Kinetics of Heterogeneous Nucleation , 1950 .

[58]  Natalia P. Zaitseva,et al.  Design and benefits of continuous filtration in rapid growth of large KDP and DKDP crystals , 1999 .

[59]  J. Brice,et al.  Crystal Growth Processes , 1987 .

[60]  H. Scheel,et al.  Stable growth rates and temperature programming in flux growth , 1972 .

[61]  N. Zaitseva,et al.  X–ray topographic study of striation formation in layer growth of crystals from solutions , 1999, Philosophical Transactions of the Royal Society of London. Series A: Mathematical, Physical and Engineering Sciences.

[62]  R. Rosmalen,et al.  The Influence of the Hydrodynamic Environment on the Growth and the Formation of Liquid Inclusions in Large Potassium Dihydrogen Phosphate (KDP) Crystals , 1978 .

[63]  H. Fujita,et al.  Rapid growth over 50 mm/day of water-soluble KDP crystal , 1997 .

[64]  C. Belouet,et al.  Strong isotopic effects on the lattice parameters and stability of highly deuterated D-KDP single crystals and related growth problems , 1975 .

[65]  J. D. Yoreo,et al.  Recovery of surfaces from impurity poisoning during crystal growth , 1999, Nature.

[66]  Li Zhengdong,et al.  Rapid growth of KH2PO4 crystals in aqueous solution with additives , 1999 .

[67]  P. Niedermann,et al.  Growth mechanisms of YBa2Cu3O7 − x platelet crystals from STM/SEM investigations , 1989 .

[68]  O. Söhnel,et al.  Interfacial surface tension for crystallization and precipitation from aqueous solutions , 1990 .

[69]  G. Loiacono,et al.  Growth of KH2PO4 crystals at constant temperature and supersaturation , 1983 .

[70]  Su Genbo,et al.  Growth of KDP crystals by splicing “parallel”‐seed in aqueous solution and its mechanism , 1990 .

[71]  N. P. Zaitseva,et al.  Stability of KH2PO4 and K(H,D)2PO4 solutions at fast crystal growth rates , 1995 .

[72]  V. G. Lutsau,et al.  X‐ray diffraction topography study of defects in potassium dihydrogen phosphate (KDP) and ammonium dihydrogen phosphate (ADP) single crystals , 1970 .

[73]  Y. Kuznetsov,et al.  Interstep interaction in solution growth; (101) ADP face , 1992 .

[74]  O. Söhnel Metastable regions of aqueous solutions of inorganic soluble salts , 1976 .

[75]  D. Verdoes,et al.  Induction time and metastability limit in new phase formation , 1991 .

[76]  A. T. Amandosov,et al.  LETTERS TO THE EDITOR: Quality of ADP crystals formed by rapid growth from a point-like seed , 1983 .

[77]  R. Rosmalen,et al.  Evidence for spiral growth on the pyramidal faces of KDP and ADP single crystals , 1980 .

[78]  T. Ogawa,et al.  In situ observation of subcritical crystalline particles and their behavior on growth of KDP crystals from aqueous solution by light-scattering technique , 1992 .

[79]  S. Veintemillas Verdaguer,et al.  Crystal growth of KDP from boiling solutions in the presence of impurities , 1986 .

[80]  C. Belouet,et al.  Autoradiography as a tool for studying iron segregation and related defects in KH2PO4 single crystals , 1975 .

[81]  J. D. Lee,et al.  The effect of dislocation cores on growth hillock vicinality and normal growth rates of KDP ?1 0 1? surfaces , 1997 .

[82]  V. Bredikhin,et al.  Rapid growth of DKDP crystals from high-acidity solutions , 1999 .

[83]  A. Myerson,et al.  Thermodynamic Studies of Levitated Microdroplets of Highly Supersaturated Electrolyte Solutions , 1996 .

[84]  Michael J. Runkel,et al.  Effect of impurities and stress on the damage distributions of rapidly grown KDP crystals , 1998, Laser Damage.

[85]  J. Nývlt Über kristallisation IV. Über die kristallkeimbildung in lösungen , 1963 .

[86]  C. Belouet,et al.  X-ray topographic study of dislocations in KH2(1−x)D2xPO4 single crystals , 1976 .

[87]  T. P. Melia,et al.  Secondary Nucleation from Aqueous Solution , 1964 .

[88]  K. Roberts,et al.  Glancing angle EXAFS investigation of the habit modification of ADP by the incorporation of iron , 1989 .

[89]  P. Bennema,et al.  The mechanism of tapering on KDP-type crystals , 1986 .

[90]  M. Jiang,et al.  Polymorphism and metastable growth of DKDP , 1981 .

[91]  H. Klapper,et al.  Elastic energy and line directions of grown-in dislocations in KDP crystals , 1974 .

[92]  J. Baruchel,et al.  Rapid growth of hybrid organic-inorganic crystals for nonlinear optics , 1999 .

[93]  Natalia P. Zaitseva,et al.  Rapid growth of large-scale (40–55 cm) KH2PO4 crystals , 1997 .

[94]  G. Loiacono,et al.  In-line bulk supersaturation measurement by electrical conductometry in KDP crystal growth from aqueous solution , 1984 .

[95]  H. Klapper,et al.  Röntgentopographische untersuchungen von gitterstörungen in Benzil-Einkristallen , 1971 .

[96]  J. L. Torgesen,et al.  Growth Layers on Ammonium Dihydrogen Phosphate , 1965, Science.

[97]  J. Garside,et al.  Direct observation of secondary nuclei production , 1978 .

[98]  L. N. Rashkovich,et al.  Growth kinetics and morphology of potassium dihydrogen phosphate crystal faces in solutions of varying acidity , 1995 .