Synthesis and Characterization of Zirconia Nanorods

ZrO2 nanorods are prepared by annealing precursor powders produced in the novel inverse microemulsion system. The length and diameter of ZrO2 nanorods are a few micrometers and 40–100 nm, respectively. The microstructure of the resultant nanorods are studied by XRD, TEM, selected area electron diffraction, and Raman spectroscopy. The ZrO2 nanorods are single crystalline and have monoclinic structure. The formation of ZrO2 nanorods is discussed.

[1]  A. G. Haerle,et al.  Microstructural Characterization of Alumina and Silicon Carbide Slip‐Cast Cakes , 2005 .

[2]  Mei Li,et al.  Synthesis of Prussian Blue Nanoparticles and Nanocrystal Superlattices in Reverse Microemulsions , 2000 .

[3]  Zuyao Chen,et al.  Synthesis of α-Fe ultrafine particles in a saturated salt solution/isopropanol/PVP microemulsion and their structural characterization , 2000 .

[4]  Yuhan Sun,et al.  Synthesis of highly stabilized zirconia sols from zirconium n-propoxide±diglycol system , 2000 .

[5]  I. Capek Radical polymerization of polar unsaturated monomers in direct microemulsion systems , 1999 .

[6]  Helmuth Möhwald,et al.  Novel Hollow Polymer Shells by Colloid-Templated Assembly of Polyelectrolytes. , 1998, Angewandte Chemie.

[7]  Wuxia Li,et al.  Synthesis of yttria-stabilized zirconia nanoparticles by heating of alcohol-aqueous salt solutions , 1998 .

[8]  K. Yoon,et al.  Molten salt synthesis of lead-based relaxors , 1998 .

[9]  C. H. Byers,et al.  Nucleation and growth for synthesis of nanometric zirconia particles by forced hydrolysis , 1998 .

[10]  J. Allison,et al.  Materials chemistry issues related to advanced materials applications in the automotive industry , 1996 .

[11]  N. Minh Ceramic Fuel Cells , 1993 .

[12]  M. Pichavant,et al.  Morphology of Zirconia Synthesized Hydrothermally from Zirconium Oxychloride , 1992 .

[13]  E. Liarokapis,et al.  Pressure and Temperature Dependence of the Raman Spectra of Zirconia and Hafnia , 1991 .

[14]  F. Wakai,et al.  Effects of solute ion and grain size on superplasticity of ZrO2 polycrystals , 1991 .

[15]  T. Nieh,et al.  Superplastic properties of a fine-grained yttria-stabilized tetragonal polycrystal of zirconia , 1988 .

[16]  K. Prewo Tension and flexural strength of silicon carbide fibre-reinforced glass ceramics , 1986 .

[17]  D. J. Johnson,et al.  Strength-structure relationships in PAN-based carbon fibres , 1983 .

[18]  T. Sakurai,et al.  Temperature Dependence of the Raman Spectra of ZrO2 , 1977 .