Synthesis of ZnO nanorods via chemical bath deposition method: The effects of physicochemical factors

Abstract In the present work, the chemical bath deposition (CBD) of ZnO nanorods was studied. The effects of pertinent factors – seed layer thickness, temperature, initial Zn concentration and Polyethylenimine (PEI) level – were indentified in the presence of hexamethylenetetramine (HMTA). The uniformity (order), growth orientation and the length and diameter (aspect ratio) of ZnO nanorods were considered as the criteria for achieving the favorable conditions of the synthesis process. The size characteristics, texture and uniformity of the ZnO nanorods were evaluated by scanning electron microscopy. X-ray diffraction (XRD) technique was also employed for the phase characterization of the obtained ZnO nanorods.

[1]  Supakorn Pukird,et al.  Effect of synthesis conditions on the growth of ZnO nanorods via hydrothermal method , 2008 .

[2]  Xingbo Liu,et al.  Hydrothermal synthesis of oriented ZnO nanorod-nanosheets hierarchical architecture on zinc foil as flexible photoanodes for dye-sensitized solar cells , 2014 .

[3]  Sebastian Wille,et al.  Rapid Fabrication Technique for Interpenetrated ZnO Nanotetrapod Networks for Fast UV Sensors , 2014, Advanced materials.

[4]  J SmithDavid,et al.  超高真空透過電子顕微鏡法を用いたSi(110)上におけるCoSi2ナノワイヤーのエンドタキシャル成長のその場観測 , 2011 .

[5]  Joshua E. Goldberger,et al.  Low‐Temperature Wafer‐Scale Production of ZnO Nanowire Arrays. , 2003 .

[6]  G. Chung,et al.  Controllable growth of oriented ZnO nanorods using Ga-doped seed layers and surface acoustic wave humidity sensor , 2014 .

[7]  F. Ahmed,et al.  Growth temperature dependent properties of ZnO nanorod arrays on glass substrate prepared by wet chemical method , 2014 .

[8]  M. Kumar,et al.  Epitaxial growth of vertically aligned highly conducting ZnO nanowires by modified aqueous chemical growth process , 2014 .

[9]  Yunfei Liu,et al.  Seed layer-free electrodeposition and characterization of vertically aligned ZnO nanorod array film , 2009 .

[10]  Md. Eaqub Ali,et al.  Sol–gel synthesis of Pd doped ZnO nanorods for room temperature hydrogen sensing applications , 2013 .

[11]  Sung-Hwan Han,et al.  Hydrophobic and textured ZnO films deposited by chemical bath deposition: Annealing effect , 2005 .

[12]  I. Azid,et al.  Effect of seed annealing temperature and growth duration on hydrothermal ZnO nanorod structures and their electrical characteristics , 2013 .

[13]  Sebastian Wille,et al.  Fabrication of Macroscopically Flexible and Highly Porous 3D Semiconductor Networks from Interpenetrating Nanostructures by a Simple Flame Transport Approach , 2013 .

[14]  M. McLachlan,et al.  Hydrothermal growth of ZnO nanorods: The role of KCl in controlling rod morphology , 2013 .

[15]  Jih-Jen Wu,et al.  Low‐Temperature Growth of Well‐Aligned ZnO Nanorods by Chemical Vapor Deposition. , 2002 .

[16]  B. Su,et al.  Simple approach to highly oriented ZnO nanowire arrays: large-scale growth, photoluminescence and photocatalytic properties , 2006 .

[17]  Zhong Lin Wang,et al.  Nanopropeller arrays of zinc oxide , 2004 .

[18]  C. Soci,et al.  ZnO nanowire UV photodetectors with high internal gain. , 2007, Nano letters.

[19]  Jiahong Zheng,et al.  Low temperature hydrothermal growth and optical properties of ZnO nanorods , 2009 .

[20]  Gareth M. Fuge,et al.  Growth of aligned ZnO nanorod arrays by catalyst-free pulsed laser deposition methods , 2004 .

[21]  Tianyou Zhai,et al.  Template Deformation‐Tailored ZnO Nanorod/Nanowire Arrays: Full Growth Control and Optimization of Field‐Emission , 2009 .

[22]  R. Adelung,et al.  Prophylactic, therapeutic and neutralizing effects of zinc oxide tetrapod structures against herpes simplex virus type-2 infection. , 2012, Antiviral research.

[23]  Amit Kumar Chawla,et al.  VLS-like growth and characterizations of dense ZnO nanorods grown by e-beam process , 2009 .

[24]  M. Willander,et al.  Growth of ZnO nanostructures by vapor–liquid–solid method , 2007 .

[25]  Kijung Yong,et al.  Controlled growth of well-aligned ZnO nanorod array using a novel solution method. , 2005, The journal of physical chemistry. B.

[26]  Shui-Tong Lee,et al.  ZnS/ZnO Heterojunction Nanoribbons , 2009 .

[27]  M. Hashim,et al.  One-dimensional ZnO nanostructure growth prepared by thermal evaporation on different substrates: Ultraviolet emission as a function of size and dimensionality , 2013 .

[28]  J. Dutta,et al.  pH-dependent growth of zinc oxide nanorods , 2009 .

[29]  Y. Kajikawa,et al.  Preferred Orientation of Chemical Vapor Deposited Polycrystalline Silicon Carbide Films , 2002 .

[30]  S. Liou,et al.  RETRACTED: Growth behavior and microstructure evolution of ZnO nanorods grown on Si in aqueous solution , 2005 .

[31]  T. Tseng,et al.  Effects of Preparation Conditions on the Growth of ZnO Nanorod Arrays Using Aqueous Solution Method , 2008 .

[32]  M. Naughton,et al.  Aligned Ultralong ZnO Nanobelts and Their Enhanced Field Emission , 2006 .

[33]  Xin Li,et al.  Improved seedless hydrothermal synthesis of dense and ultralong ZnO nanowires , 2011, Nanotechnology.

[34]  Jin Zhai,et al.  Reversible super-hydrophobicity to super-hydrophilicity transition of aligned ZnO nanorod films. , 2004, Journal of the American Chemical Society.

[35]  M. Willander,et al.  Size-controlled growth of well-aligned ZnO nanorod arrays with two-step chemical bath deposition method , 2009 .

[36]  R. Adelung,et al.  Virostatic potential of micro-nano filopodia-like ZnO structures against herpes simplex virus-1. , 2011, Antiviral research.

[37]  B. A. Patterson,et al.  Increased interyarn friction through ZnO nanowire arrays grown on aramid fabric , 2015 .

[38]  L. Vayssieres Growth of Arrayed Nanorods and Nanowires of ZnO from Aqueous Solutions , 2003 .

[39]  J. E. Mark Polymer Data Handbook , 2009 .

[40]  P. Yang,et al.  Solution-Grown Zinc Oxide Nanowires , 2006 .

[41]  Jong Yeog Son,et al.  Vertical ZnO nanorod array as an effective hydrogen gas sensor , 2013 .

[42]  Mohamed Faiz,et al.  Low temperature synthesis of hexagonal ZnO nanorods and their hydrogen sensing properties , 2011 .

[43]  Bingqiang Cao,et al.  Ultraviolet-light-emitting ZnO nanosheets prepared by a chemical bath deposition method , 2005 .

[44]  Weizhen He,et al.  Solution-derived 40 µm vertically aligned ZnO nanowire arrays as photoelectrodes in dye-sensitized solar cells , 2010, Nanotechnology.

[45]  M. Mahmood,et al.  Optical properties of well-aligned ZnO nanostructure arrays synthesized by an electric field-assisted aqueous solution method , 2014 .

[46]  R. Adelung,et al.  A Novel Concept for Self‐Reporting Materials: Stress Sensitive Photoluminescence in ZnO Tetrapod Filled Elastomers , 2013, Advanced materials.

[47]  Dong Chan Kim,et al.  Growth of ZnO nanorod arrays by hydrothermal method using homo‐seed layers annealed at various temperatures , 2010 .

[48]  Zhong Lin Wang,et al.  Controlled synthesis and manipulation of ZnO nanorings and nanobows , 2005 .

[49]  Sangsig Kim,et al.  ZnO nanomaterials synthesized from thermal evaporation of ball-milled ZnO powders , 2003 .

[50]  G. Zou,et al.  Fabrication and Optical Properties of Large-Scale ZnO Nanotube Bundles via a Simple Solution Route , 2007 .

[51]  P. O’Brien,et al.  Understanding the factors that govern the deposition and morphology of thin films of ZnO from aqueous solution , 2004 .

[52]  Sangwoo Lim,et al.  Effect of Seed Layer on the Growth of ZnO Nanorods , 2007 .