Characterization of Residual Strain in Si Ingots Grown by the Seed-Cast Method

The residual strain distribution in cast-grown mono-like Si ingots is analyzed. The effect of the crucible during solidification and the influence of different cooling rates is described. To clarify in which process steps residual strain accumulates, several Si ingots were grown in a laboratory scale furnace (100mm) using different cooling conditions after completion of the solidification. For the cooling, two different cooling rates were distinguished: fast cooling (12deg/min) and slow cooling (5deg/min). It was found that changes in cooling gradients greatly influence the amount of residual strain. The results show that slow cooling in any temperature range leads to strain reduction. The greatest reduction could be found when the temperature gradient was changed to slow cooling in the high temperature region.

[1]  T. Sekiguchi,et al.  Quantitative Photoelastic Characterization of Residual Strains in Grains of Multicrystalline Silicon , 2010 .

[2]  M. Yamaguchi,et al.  Directional solidification of polycrystalline silicon ingots by successive relaxation of supercooling method , 2007 .

[3]  Nathan Stoddard,et al.  Casting Single Crystal Silicon: Novel Defect Profiles from BP Solar's Mono2 TM Wafers , 2007 .

[4]  L. Arnberg,et al.  State-of-the-art growth of silicon for PV applications , 2012 .

[5]  G. G. Stokes "J." , 1890, The New Yale Book of Quotations.

[6]  John B. Shoven,et al.  I , Edinburgh Medical and Surgical Journal.

[7]  K. Kakimoto,et al.  Three-dimensional global analysis of thermal stress and dislocations in a silicon ingot during a unidirectional solidification process with a square crucible , 2010 .

[8]  Shreyes N. Melkote,et al.  Analysis of stresses and breakage of crystalline silicon wafers during handling and transport , 2009 .

[9]  T. Sekiguchi,et al.  Reduction of polycrystalline grains region near the crucible wall during seeded growth of monocrystalline silicon in a unidirectional solidification furnace , 2012 .

[10]  T. Sekiguchi,et al.  Effect of Crystallinity on Residual Strain Distribution in Cast-Grown Si , 2013 .

[11]  Masayoshi Yamada,et al.  High-sensitivity computer-controlled infrared polariscope , 1993 .

[12]  P. Haasen,et al.  Dislocations and Plastic Flow in the Diamond Structure , 1969 .

[13]  I. J. Bennett,et al.  Effect of silicon solar cell processing parameters and crystallinity on mechanical strength , 2011 .