Fatigue testing of a NiTi rotary instrument. Part 1: Strain-life relationship.

AIM To examine the fatigue behaviour using a strain-life approach, and to determine the effect of water on the fatigue life of a NiTi rotary instrument. METHODOLOGY Instruments of one brand of NiTi engine-file (size 25, ProFile 0.04 and 0.06) were subjected to rotational bending either in air or under water, the number of revolutions to fracture (N(f)) being recorded using an optical counter and an electronic break-detection circuit. The effective surface strain amplitude (epsilon(a)) for each specimen was determined from the curvature of the instrument (on a photograph) and the diameter of the fracture cross-section (from a scanning electron micrograph of the fracture surface). Strain was plotted against fatigue life and the low-cycle fatigue (LCF) region identified. Values were examined using two-way analysis of variance for difference between various instrument-environment combinations. RESULTS A total of 212 instruments were tested. A strain-life relationship typical of metals was found. N(f) declined with an inverse power function dependence on epsilon(a). A fatigue limit was present at about 0.7% strain. The apparent fatigue-ductility exponent, a material constant for the LCF life of metals, was found to be between -0.45 and -0.55. There was a significant effect of the environmental condition on the LCF life, water being more detrimental than air. CONCLUSIONS The fatigue behaviour of NiTi rotary instrument is typical of most metals, provided that the analysis is based on the surface strain amplitude, and showed a high-cycle and a LCF region. The LCF life is adversely affected by water.

[1]  J. P. Pruett,et al.  Cyclic fatigue testing of nickel-titanium endodontic instruments. , 1997, Journal of endodontics.

[2]  E. Pavlidou,et al.  Effect of heat sterilization on surface characteristics and microstructure of Mani NRT rotary nickel-titanium instruments. , 2006, International endodontic journal.

[3]  P Machtou,et al.  Failure of ProFile instruments used with high and low torque motors. , 2001, International endodontic journal.

[4]  G Gambarini,et al.  Cyclic fatigue testing of ProTaper NiTi rotary instruments after clinical use. , 2004, Oral surgery, oral medicine, oral pathology, oral radiology, and endodontics.

[5]  Hisaaki Tobushi,et al.  Rotating-bending fatigue of a TiNi shape-memory alloy wire , 1997 .

[6]  A C D Viana,et al.  Influence of sterilization on mechanical properties and fatigue resistance of nickel-titanium rotary endodontic instruments. , 2006, International endodontic journal.

[7]  J. Fuentes,et al.  Phase Change Behavior of Nitinol Shape Memory Alloys , 2002 .

[8]  G. Cheung,et al.  Defects in ProTaper S1 instruments after clinical use: fractographic examination. , 2005, International endodontic journal.

[9]  R O Ritchie,et al.  Fatigue-crack propagation in Nitinol, a shape-memory and superelastic endovascular stent material. , 1999, Journal of biomedical materials research.

[10]  O. Peters,et al.  Effect of cyclic fatigue on static fracture loads in ProTaper nickel-titanium rotary instruments. , 2005, Journal of endodontics.

[11]  G. Bateman,et al.  A new method for the quantitative analysis of endodontic microleakage. , 1999, Journal of endodontics.

[12]  Bor-Shiunn Lee,et al.  Cyclic fatigue of endodontic nickel titanium rotary instruments: static and dynamic tests. , 2002, Journal of endodontics.

[13]  B Peng,et al.  Defects in ProTaper S1 instruments after clinical use: longitudinal examination. , 2005, International endodontic journal.

[14]  G. Yared,et al.  Cyclic fatigue of Profile rotary instruments after simulated clinical use. , 1999, International endodontic journal.

[15]  H. Tobushi,et al.  Low-Cycle Fatigue of TiNi Shape Memory Alloy and Formulation of Fatigue Life , 2000 .

[16]  Peter Parashos,et al.  Factors influencing defects of rotary nickel-titanium endodontic instruments after clinical use. , 2004, Journal of endodontics.

[17]  Fred Barbakow,et al.  Engine-driven preparation of curved root canals: measuring cyclic fatigue and other physical parameters. , 2002, Australian endodontic journal : the journal of the Australian Society of Endodontology Inc.

[18]  G. Cheung,et al.  Comparison of defects in ProFile and ProTaper systems after clinical use. , 2006, Journal of endodontics.

[19]  B. Sattapan,et al.  Defects in rotary nickel-titanium files after clinical use. , 2000, Journal of endodontics.

[20]  John C. Mitchell,et al.  Scanning electron microscope observations of new and used nickel-titanium rotary files. , 2003, Journal of endodontics.

[21]  V. Buono,et al.  Decrease in the fatigue resistance of nickel-titanium rotary instruments after clinical use in curved root canals. , 2005, Oral surgery, oral medicine, oral pathology, oral radiology, and endodontics.