Influence of Pressure and Temperature on Microstructure and Mechanical Behavior of Squeeze Cast Mg-10Gd-3Y-0.5Zr Alloy

The influence of applied pressure and pouring temperature on the microstructure and mechanical properties of a squeeze cast (SC) Mg-10Gd-3Y-0.5Zr (GW103K) alloy was systematically investigated. Our results show that increasing the applied pressure leads to microstructure refinement of the GW103K alloy with accompanying enhancement of tensile yield strength (TYS), ultimate tensile strength (UTS), and elongation to failure (Ef); a decrease in pouring temperature also leads to grain refinement and increases of TYS while decreasing the UTS and Ef. Our results show that, for the range of parameters studied herein, an applied pressure of ~160 MPa, in combination with a pouring temperature of ~993 K (720 °C), represents optimum process parameters for squeeze casting of GW103K. Using these process parameters, the TYS, UTS, and Ef of squeeze cast GW103K alloy are 151 MPa, 232 MPa, and 3.0 pct in the as-cast state, and 264 MPa, 383 MPa, and 1.5 pct, respectively, in the as-T6 heat-treated state, both of which represent significant improvements over those of the gravity cast (GC) counterpart material.

[1]  A. Luo,et al.  Cast magnesium alloys for elevated temperature applications , 1994 .

[2]  R. Labusch A Statistical Theory of Solid Solution Hardening , 1970 .

[3]  W. Ding,et al.  Formation of denuded zones in crept Mg–2.5Gd–0.1Zr alloy , 2015 .

[4]  H. Hu,et al.  Pressurized solidification of magnesium alloy AM50A , 2007 .

[5]  A. Luo,et al.  Study on Pressurized Solidification Behavior and Microstructure Characteristics of Squeeze Casting Magnesium Alloy AZ91D , 2015, Metallurgical and Materials Transactions B.

[6]  Shuming Xing,et al.  Influence of technical parameters on strength and ductility of AlSi9Cu3 alloys in squeeze casting , 2013 .

[7]  장윤희,et al.  Y. , 2003, Industrial and Labor Relations Terms.

[8]  G. G. Stokes "J." , 1890, The New Yale Book of Quotations.

[9]  Zhizhong Sun,et al.  Influence of Section Thickness on Microstructure and Mechanical Properties of Squeeze Cast Magnesium Alloy AM60 , 2012 .

[10]  Li Zhao,et al.  Microstructure and mechanical properties of a novel Mg–RE–Zn–Y alloy fabricated by rheo-squeeze casting , 2016 .

[11]  E. Han,et al.  Microstructure and strengthening mechanisms of a cast Mg–1.48Gd–1.13Y–0.16Zr (at.%) alloy , 2009, Journal of Materials Science.

[12]  K. E. Easterling,et al.  Phase Transformations in Metals and Alloys (Revised Reprint) , 2009 .

[13]  Hao Zhou,et al.  Effect of Ag on interfacial segregation in Mg–Gd–Y–(Ag)–Zr alloy , 2015 .

[14]  C. Hutchinson,et al.  Modeling the precipitation processes and strengthening mechanisms in a Mg-Al-(Zn) AZ91 alloy , 2005 .

[15]  M. Gibson,et al.  On the unexpected formation of rare earth hydrides in magnesium-rare earth casting alloys , 2014 .

[16]  Qudong Wang,et al.  Creep behavior of Mg–9Gd–1Y–0.5Zr (wt.%) alloy piston by squeeze casting , 2013 .

[17]  N. Mufti,et al.  Investigating cooling curve profile and microstructure of a squeeze cast Al–4%Cu alloy , 2012 .

[18]  Weiweng Zhang,et al.  Comparative study on microstructures and mechanical properties of the heat-treated Al–5.0Cu–0.6Mn–xFe alloys prepared by gravity die casting and squeeze casting , 2014 .

[19]  H. Hu,et al.  Influence of applied pressure on microstructure and tensile properties of squeeze cast magnesium Mg-Al-Ca alloy , 2011 .

[20]  Liming Peng,et al.  Microstructure and strengthening mechanism of high strength Mg–10Gd–2Y–0.5Zr alloy , 2007 .

[21]  L. Nastac,et al.  Computational Multi-Scale Modeling of the Microstructure and Segregation of Cast Mg Alloys at Low Superheat , 2013 .

[22]  H. Hu Squeeze casting of magnesium alloys and their composites , 1998 .

[23]  E. Han,et al.  Effects of rare-earth elements Gd and Y on the solid solution strengthening of Mg alloys , 2009 .

[24]  Guohua Wu,et al.  Effects of processing parameters on microstructure and mechanical properties of squeeze-cast Mg–12Zn–4Al–0.5Ca alloy , 2014 .

[25]  W. D. Callister,et al.  Fundamentals of Materials Science and Engineering , 2004 .

[26]  M. R. Ghomashchi,et al.  Squeeze casting: an overview , 2000 .

[27]  B. Chua,et al.  Effect of squeeze casting parameters on the mechanical properties of AZ91–Ca Mg alloys , 2010 .

[28]  P. Lukáč Solid solution hardening in MgCd single crystals , 1992 .

[29]  C. H. Cáceres,et al.  Strain hardening behaviour and the Taylor factor of pure magnesium , 2008 .

[30]  M. Mabuchi,et al.  Effect of hot extrusion on mechanical properties of a MgSiAl alloy , 1994 .

[31]  Mohamed Ben Amar,et al.  Optimization of Squeeze Casting Parameters for 2017 A Wrought Al Alloy Using Taguchi Method , 2014 .

[32]  Zhizhong Sun,et al.  Determination of heat transfer coefficients by extrapolation and numerical inverse methods in squeeze casting of magnesium alloy AM60 , 2011 .

[33]  M. Easton,et al.  Strengthening Micromechanisms in Cold-Chamber High-Pressure Die-Cast Mg-Al Alloys , 2014, Metallurgical and Materials Transactions A.

[34]  J. Nie Effects of precipitate shape and orientation on dispersion strengthening in magnesium alloys , 2003 .

[35]  Guohua Wu,et al.  Effect of Zr on the microstructure, mechanical properties and corrosion resistance of Mg–10Gd–3Y magnesium alloy , 2009 .

[36]  F. Hauser,et al.  Deformation and Fracture Mechanics of Engineering Materials , 1976 .

[37]  J. Nie Precipitation and Hardening in Magnesium Alloys , 2012, Metallurgical and Materials Transactions A.

[38]  Y. Gan,et al.  Effect of cooling rate on microstructure and mechanical properties of squeeze cast Al–Cu–Mg alloy , 2015 .

[39]  J. E. Bailey,et al.  The dislocation distribution, flow stress, and stored energy in cold-worked polycrystalline silver , 1960 .

[40]  C. J. Smithells,et al.  Smithells metals reference book , 1949 .

[41]  A. Luo,et al.  A quantitative model for describing crystal nucleation in pressurized solidification during squeeze casting , 2012 .

[42]  Guohua Wu,et al.  Preparation of an Mg–Gd–Zn alloy semisolid slurry by low frequency electro-magnetic stirring , 2015 .

[43]  Margaret Nichols Trans , 2015, De-centering queer theory.

[44]  A. Luo,et al.  Microstructure characteristics and effect of aging process on the mechanical properties of squeeze-cast AZ91 alloy , 2015 .

[45]  M. Gibson,et al.  Evaluation of Magnesium Die-Casting Alloys for Elevated Temperature Applications: Microstructure, Tensile Properties, and Creep Resistance , 2015, Metallurgical and Materials Transactions A.

[46]  William D. Callister,et al.  Fundamentals of Materials Science and Engineering: An Integrated Approach, 2nd Edition , 2004 .

[47]  Himadri Chattopadhyay,et al.  Simulation of transport processes in squeeze casting , 2007 .

[48]  大野 篤美 Solidification : the separation theory and its practical applications , 1987 .

[49]  E. Maire,et al.  Relationship between internal porosity and fracture strength of die-cast magnesium AM60B alloy , 2005 .

[50]  Alan A. Luo,et al.  Magnesium casting technology for structural applications , 2013 .