Dependence of temperature coefficient of frequency (TCf) on crystallography and eigenmode in N-doped silicon contour mode micromechanical resonators

Abstract This paper reports the effects of crystal orientations on the temperature coefficient of frequency (TCf) of single crystal silicon square-plate micromechanical resonators vibrating in two distinct contour modes: Lame mode and square extensional (SE). For the Lame mode, the same TCf was found over several devices aligned to the 〈1 1 0〉 direction, while much greater variation in the TCf was observed among the devices aligned against the 〈1 0 0〉 direction. For the SE mode, the devices in both 〈1 0 0〉 and 〈1 1 0〉 orientations exhibit similar TCf values for varying doping levels. The sensitivity of TCf to doping concentration is also investigated. The TCf of Lame 〈1 0 0〉 device is more easily influenced by n-type doping concentration than SE mode devices in both orientations while the Lame 〈1 0 0〉 device is almost immune to doping variation. Devices with different dimensions are tested, and the TCf values are proved to be free of size scaling. Quantitative study based on free carrier contribution on elastic constants is performed and supports our observations. Close agreement among experiments, theoretical predictions and simulations is achieved.

[1]  John J. Hall,et al.  Electronic Effects in the Elastic Constants of n -Type Silicon , 1967 .

[3]  B. Murmann,et al.  Phase Lock Loop based Temperature Compensation for MEMS Oscillators , 2009, 2009 IEEE 22nd International Conference on Micro Electro Mechanical Systems.

[4]  G. Casinovi,et al.  Passive TCF compensation in high Q silicon micromechanical resonators , 2010, 2010 IEEE 23rd International Conference on Micro Electro Mechanical Systems (MEMS).

[5]  F. Ayazi,et al.  Temperature compensation of silicon micromechanical resonators via degenerate doping , 2009, 2009 IEEE International Electron Devices Meeting (IEDM).

[6]  Farrokh Ayazi,et al.  Micromechanical IBARs: Tunable High-$Q$ Resonators for Temperature-Compensated Reference Oscillators , 2010, Journal of Microelectromechanical Systems.

[7]  R. Keyes Electronic Effects in the Elastic Properties of Semiconductors , 1968 .

[8]  Siavash Pourkamali,et al.  Sub-100ppb/°C temperature stability in thermally actuated high frequency silicon resonators via degenerate phosphorous doping and bias current optimization , 2010, 2010 International Electron Devices Meeting.

[9]  Joshua E-Y Lee,et al.  Crystallographic and eigenmode dependence of TCf for single crystal silicon contour mode resonators , 2013, 2013 IEEE 26th International Conference on Micro Electro Mechanical Systems (MEMS).

[10]  R. Howe,et al.  Fully-differential poly-SiC Lame mode resonator and checkerboard filter , 2005, 18th IEEE International Conference on Micro Electro Mechanical Systems, 2005. MEMS 2005..

[11]  J. Wortman,et al.  Young's Modulus, Shear Modulus, and Poisson's Ratio in Silicon and Germanium , 1965 .

[12]  T. Kenny,et al.  Temperature-Insensitive Composite Micromechanical Resonators , 2009, Journal of Microelectromechanical Systems.

[13]  M. Prunnila,et al.  Temperature compensated resonance modes of degenerately n-doped silicon MEMS resonators , 2012, 2012 IEEE International Frequency Control Symposium Proceedings.

[14]  Don Berlincourt,et al.  Elastic and Piezoelectric Coefficients of Single-Crystal Barium Titanate , 1958 .

[15]  H. Seppa,et al.  Nonlinear limits for single-crystal silicon microresonators , 2004, Journal of Microelectromechanical Systems.

[16]  A. Partridge,et al.  Low jitter and temperature stable MEMS oscillators , 2012, 2012 IEEE International Frequency Control Symposium Proceedings.

[17]  J. Dekker,et al.  Temperature compensation of silicon MEMS Resonators by Heavy Doping , 2011, 2011 IEEE International Ultrasonics Symposium.

[18]  F. Ayazi,et al.  A 27 MHz temperature compensated MEMS oscillator with sub-ppm instability , 2012, 2012 IEEE 25th International Conference on Micro Electro Mechanical Systems (MEMS).

[19]  R. Abdolvand,et al.  Turnover Temperature Point in Extensional-Mode Highly Doped Silicon Microresonators , 2013, IEEE Transactions on Electron Devices.

[20]  J. Kiihamaki,et al.  Square-extensional mode single-crystal silicon micromechanical resonator for low-phase-noise oscillator applications , 2004, IEEE Electron Device Letters.

[21]  Robert Puers,et al.  A review of MEMS oscillators for frequency reference and timing applications , 2011 .

[22]  R. Rebel,et al.  Wafer-level chip scale MEMS oscillator for wireless applications , 2012, 2012 IEEE International Frequency Control Symposium Proceedings.

[23]  H. Ekstein Free Vibrations of Anisotropic Bodies , 1944 .

[24]  Myron A. Jeppesen Young's Modulus , 1955 .

[25]  E. C. Stoner,et al.  The Computation of Fermi-Dirac Functions , 1938 .

[26]  R. Abdolvand,et al.  Zero temperature coefficient of frequency in extensional-mode highly doped silicon microresonators , 2012, 2012 IEEE International Frequency Control Symposium Proceedings.

[27]  H. J. Mcskimin Measurement of Elastic Constants at Low Temperatures by Means of Ultrasonic Waves–Data for Silicon and Germanium Single Crystals, and for Fused Silica , 1953 .