3D nanorobotic manipulations of multi-walled carbon nanotubes

Multi-walled carbon nanotubes (MWNTs) are manipulated in 3D space with a 10-DOF nanorobotic manipulator, which is actuated with PZTs and Picomotors/sup TM/ (New Focus Inc.) and operated inside a scanning electronic microscope (SEM). The coarse linear resolutions of the manipulator are better than 30 nm (X, Y, Z stages actuated by Picomotors) and the rotary one 2 mrad, while the resolutions of fine motions (actuated by PZTs) are within nano-order. AFM cantilevers are used as the end-effector. Several kinds of manipulations of MWNTs are performed with the developed manipulators with the assistance of dielectrophoresis and van der Waals forces. A single MWNT with estimated dimensions of /spl phi/ 40 nm /spl times/7 /spl mu/m has been picked up on an AFM cantilever. Another /spl phi/ 50 nm /spl times/6 /spl mu/m MWNT is placed between two cantilevers, and still another /spl phi/ 40 nm /spl times/8 /spl mu/m MWNT is bent between a cantilever and sample substrate. Carbon nanotube (CNT) junctions are basic building blocks for more complex devices based on CNTs. A cross-junction was constructed with two MWNTs of dimensions of /spl sim//spl phi/ 40 nm /spl times/6 /spl mu/m and /spl sim//spl phi/ 50 nm /spl times/7 /spl mu/m, and a T-junction was made of two MWNTs with the dimensions of /spl sim//spl phi/ 40 nm /spl times/3 /spl mu/m and /spl sim//spl phi/ 50 nm /spl times/2 /spl mu/m. Force measurements are performed and the flexural rigidity and Young's modulus of an /spl sim//spl phi/ 30 nm /spl times/7 /spl mu/m MWNT are estimated to be 8.641/spl times/10/sup -20/ Nm/sup 2/ and 2.17 TPa respectively. Such manipulations are essential for both the property research of CNTs and the fabrication of CNT-based NEMS.

[1]  H. Lezec,et al.  Electrical conductivity of individual carbon nanotubes , 1996, Nature.

[2]  Yoshinori Ando,et al.  Pentagons, heptagons and negative curvature in graphite microtubule growth , 1992, Nature.

[3]  Charles M. Lieber,et al.  Probing Electrical Transport in Nanomaterials: Conductivity of Individual Carbon Nanotubes , 1996, Science.

[4]  H. Dai,et al.  Nanotubes as nanoprobes in scanning probe microscopy , 1996, Nature.

[5]  H. Dai,et al.  Individual single-wall carbon nanotubes as quantum wires , 1997, Nature.

[6]  Paul L. McEuen,et al.  Single-Electron Transport in Ropes of Carbon Nanotubes , 1997, Science.

[7]  Tomomasa Sato,et al.  Pick and place operation of a micro-object with high reliability and precision based on micro-physics under SEM , 1999, Proceedings 1999 IEEE International Conference on Robotics and Automation (Cat. No.99CH36288C).

[8]  Sawada,et al.  New one-dimensional conductors: Graphitic microtubules. , 1992, Physical review letters.

[9]  Charlier,et al.  Structural and electronic properties of pentagon-heptagon pair defects in carbon nanotubes. , 1996, Physical review. B, Condensed matter.

[10]  Madhu Menon,et al.  Carbon Nanotube ``T Junctions'': Nanoscale Metal-Semiconductor-Metal Contact Devices , 1997 .

[11]  Hideki Hashimoto,et al.  Tele-touch feedback of surfaces at the micro/nano scale: modeling and experiments , 1999, Proceedings 1999 IEEE/RSJ International Conference on Intelligent Robots and Systems. Human and Environment Friendly Robots with High Intelligence and Emotional Quotients (Cat. No.99CH36289).

[12]  T. Ichihashi,et al.  Single-shell carbon nanotubes of 1-nm diameter , 1993, Nature.

[13]  S. Iijima Helical microtubules of graphitic carbon , 1991, Nature.

[14]  M. Dresselhaus,et al.  Physical properties of carbon nanotubes , 1998 .

[15]  R. Ruoff,et al.  Strength and breaking mechanism of multiwalled carbon nanotubes under tensile load , 2000, Science.

[16]  T. Fukuda,et al.  Integrated microendeffector for micromanipulation , 1998 .

[17]  Rodney S. Ruoff,et al.  Radial deformation of carbon nanotubes by van der Waals forces , 1993, Nature.

[18]  Zhong Lin Wang,et al.  Carbon nanotube quantum resistors , 1998, Science.

[19]  Charles M. Lieber,et al.  Nanobeam Mechanics: Elasticity, Strength, and Toughness of Nanorods and Nanotubes , 1997 .

[20]  Fumihito Arai,et al.  Micro manipulation based on micro physics-strategy based on attractive force reduction and stress measurement , 1995, Proceedings 1995 IEEE/RSJ International Conference on Intelligent Robots and Systems. Human Robot Interaction and Cooperative Robots.

[21]  T. Ebbesen,et al.  Exceptionally high Young's modulus observed for individual carbon nanotubes , 1996, Nature.

[22]  S. Tans,et al.  Room-temperature transistor based on a single carbon nanotube , 1998, Nature.

[23]  Fumihito Arai,et al.  3D nanorobotic manipulation of nano-order objects inside SEM , 2000, MHS2000. Proceedings of 2000 International Symposium on Micromechatronics and Human Science (Cat. No.00TH8530).

[24]  Shirley Dex,et al.  JR 旅客販売総合システム(マルス)における運用及び管理について , 1991 .

[25]  W. G. Matthews,et al.  Controlled manipulation of molecular samples with the nanoManipulator , 2000 .

[26]  M. Dresselhaus,et al.  Tunneling conductance of connected carbon nanotubes. , 1996, Physical review. B, Condensed matter.

[27]  Benedict,et al.  Pure carbon nanoscale devices: Nanotube heterojunctions. , 1996, Physical review letters.

[28]  Young Hee Lee,et al.  Crystalline Ropes of Metallic Carbon Nanotubes , 1996, Science.

[29]  Langer,et al.  Quantum transport in a multiwalled carbon nanotube. , 1996, Physical review letters.