Influences of planarization modification and morphological filtering by AFM probe-tip on the evaluation accuracy of fractal dimension

Abstract The scaling characteristic of surface roughness could reveal the fractal property of a surface, which is common for the thin films fabricated via physical vapor deposition. In our previous study, a roughness scaling extraction (RSE) method was proposed to accurately calculate the fractal dimension (D), which is an effective parameter to represent the irregularity and fragmental property of a fractal surface. RSE method was based on a single morphological image of the concerned surface, and was much more accurate than the traditional methods with a low mean relative error of 0.64%. In this study, RSE method was firstly optimized by using the planarization modification on the morphological images of artificial surfaces with ideal dimensions (Di) ranging from 2.1 to 2.9, which were generated through Weierstrass-Mandelbrot (W-M) function. The calculation accuracy of RSE method could be enhanced by using the second order planarization modification, with a lowest mean relative error of only 0.42% between Di and the calculated dimensions (Dc). Secondly, artificial surfaces with high resolution and Di from 2.2 to 2.8 were utilized to investigate the influence of atomic force microscopy (AFM) probe-tip geometry on the calculation accuracy. A typical geometry with a probe-tip radius (r) of 10 nm was employed to carry out the simulation of morphological filtering for the surface images, and the filtered images with various scales (L) from 0.5 μm to 7.5 μm were generated. RSE method was found to be robust only when the ratio of L/r was above 400, while a significant deviation occurred at lower ratio values, which would be instructive for the fractal analysis on the AFM images of various surface morphologies.

[1]  Sudibyo,et al.  Magneto-electro deposition of tin dendrites , 2015 .

[2]  Feng Feng,et al.  Fractal analysis and atomic force microscopy measurements of surface roughness for Hastelloy C276 substrates and amorphous alumina buffer layers in coated conductors , 2012 .

[3]  Tomohiro Onda,et al.  Super-Water-Repellent Fractal Surfaces , 1995 .

[4]  Yanjie Yao,et al.  Thickness modulation effect of CeO2 layer for YBCO films grown by pulsed laser deposition , 2018, Rare Metals.

[5]  Y. Bruynseraede,et al.  Scanning tunneling microscopy observation of self-affine fractal roughness in ion-bombarded film surfaces. , 1993, Physical review letters.

[6]  Xiangsong Zhang,et al.  Surface scaling analysis of textured MgO thin films fabricated by energetic particle self-assisted deposition , 2018 .

[7]  Slawomir Kulesza,et al.  A comparative study of correlation methods for determination of fractal parameters in surface characterization , 2014 .

[8]  A. Barabasi,et al.  Fractal concepts in surface growth , 1995 .

[9]  T. R. Thomas,et al.  The spatial representation of surface roughness by means of the structure function: A practical alternative to correlation , 1977 .

[10]  Xiangsong Zhang,et al.  Roughness scaling extraction method for fractal dimension evaluation based on a single morphological image , 2018, Applied Surface Science.

[11]  Gunnar Suchaneck,et al.  Evaluation of the fractal dimension of sol-gel deposited oxide films by means of the power spectral density , 2014, Glass Physics and Chemistry.

[12]  P. Feng,et al.  Scaling analysis of current influence on Hastelloy surface roughness in electro-polishing process , 2018, Rare Metals.

[13]  R. Jackson,et al.  An analysis of generated fractal and measured rough surfaces in regards to their multi-scale structure and fractal dimension , 2017 .

[14]  B. Mandelbrot How Long Is the Coast of Britain? Statistical Self-Similarity and Fractional Dimension , 1967, Science.

[15]  A. Perry The surface topography of titanium nitride made by chemical vapor deposition , 2000 .

[16]  Shigeyasu Amada,et al.  Influence of grit blasting pre-treatment on the adhesion strength of plasma sprayed coatings: fractal analysis of roughness , 1998 .

[17]  Eugenio Coronado,et al.  Correction of the tip convolution effects in the imaging of nanostructures studied through scanning force microscopy , 2014, Nanotechnology.

[18]  F. Ghodsi,et al.  The surface wettability and improved electrochemical performance of nanostructured CoxFe3 − xO4 thin film , 2017 .

[19]  Hongwei Zhou,et al.  Box-counting methods to directly estimate the fractal dimension of a rock surface , 2014 .

[20]  A. Sulpice,et al.  Wrinkling of YBa2Cu3O7−x film prepared by trifluoroacetate metal organic deposition , 2015 .

[21]  G. Nabiyouni,et al.  Fractal analysis of nanostructured silver film surface , 2017 .

[22]  Effects of grains’ features in surface roughness scaling , 2007, cond-mat/0703504.

[23]  Jiunn-Jong Wu Analyses and simulation of anisotropic fractal surfaces , 2002 .

[24]  Craig S. Criddle,et al.  Use of atomic force microscopy and fractal geometry to characterize the roughness of nano-, micro-, and ultrafiltration membranes , 2009 .

[25]  K. Komvopoulos,et al.  Contact analysis of elastic-plastic fractal surfaces , 1998 .

[26]  Y. Shiohara,et al.  Surface roughness of MgO thin film and its critical thickness for optimal biaxial texturing by ion-beam-assisted deposition , 2011 .

[27]  Ahm Arno Smets,et al.  Temperature dependence of the surface roughness evolution during hydrogenated amorphous silicon film growth , 2003 .