Optical and structure characterization of cinnamon nanoparticles synthesized by pulse laser ablation in liquid (PLAL)

Organic nanoparticles development is under exploration due to its beneficial applications in nanobiomedical and research interests. PLAL technique of Q-switched 1064-Nd: YAG (10 ns pulse duration, repetition rate 1 Hz and laser energy 20-100 mJ) has inherent advantages and rapid growth of nanoparticles when compared to conventional methods because of the controlled fabricated nanoparticles, stability, and purity. Cinnamon sticks as a target are immersed in 5 ml ethanol medium and irradiated by a laser beam for the growth process. The morphology, optical characteristic, and bonding structure of cinnamon nanoparticles (CNPs) are determined and evaluated by transmission electron microscope (TEM), UV-Visible spectroscopy and Fourier transform infrared spectroscopy (FTIR). Spherical, homogenous and high crystallinity CNPs was revealed within the particle size range of 2 - 28 nm. The absorption band was found in the ultraviolent region around 259 nm and 319 nm. The present of FTIR spectra confirmed that the nanoparticles were covered by plant secondary metabolites. The experimental findings revealed that the synthesize CNPs in ethanol has a potential for nanomedicine applications.

[1]  Mayurdhvajsinh R Sindha,et al.  Advanced drug delivery systems: Nanotechnology of health design and its potential clinical Application , 2020 .

[2]  N. Bidin,et al.  Pulse Q-switched Nd:YAG laser ablation grown cinnamon nanomorphologies: Influence of different liquid medium , 2017 .

[3]  F. Huyop,et al.  Antibacterial activity of PLAL synthesized nanocinnamon , 2017 .

[4]  Samiuela Lee,et al.  Anti-inflammatory activity of cinnamon (C. zeylanicum and C. cassia) extracts - identification of E-cinnamaldehyde and o-methoxy cinnamaldehyde as the most potent bioactive compounds. , 2015, Food & function.

[5]  Shakeel Ahmed,et al.  A review on plants extract mediated synthesis of silver nanoparticles for antimicrobial applications: A green expertise , 2015, Journal of advanced research.

[6]  J. Safari,et al.  Advanced drug delivery systems: Nanotechnology of health design A review , 2014 .

[7]  A. Love,et al.  “Green” Nanotechnologies: Synthesis of Metal Nanoparticles Using Plants , 2014, Acta naturae.

[8]  Joshua M. Pearce,et al.  Physics: Make nanotechnology research open-source , 2012, Nature.

[9]  Guowei Yang Laser Ablation in Liquids: Principles and Applications in the Preparation of Nanomaterials , 2012 .

[10]  Stephan Barcikowski,et al.  Transfer-Matrix Method for Efficient Ablation by Pulsed Laser Ablation and Nanoparticle Generation in Liquids , 2011 .

[11]  Y. Yun,et al.  Immobilization of silver nanoparticles synthesized using Curcuma longa tuber powder and extract on cotton cloth for bactericidal activity. , 2010, Bioresource technology.

[12]  Boris N. Chichkov,et al.  Pulsed Laser Ablation of Zinc in Tetrahydrofuran: Bypassing the Cavitation Bubble , 2010 .

[13]  S. Nie,et al.  A systematic examination of surface coatings on the optical and chemical properties of semiconductor quantum dots. , 2006, Physical chemistry chemical physics : PCCP.

[14]  M. Fatima,et al.  In Vitro Antiviral Activity of Cinnamomum cassia and Its Nanoparticles Against H7N3 Influenza A Virus. , 2016, Journal of microbiology and biotechnology.

[15]  K. Ramanathan,et al.  Phytochemical Analysis of Bark Extract of Cinnamomum verum : A Medicinal Herb Used for the Treatment of Coronary Heart Disease in Malayali Tribes , Pachamalai Hills , Tamil Nadu , India , 2016 .