catena -Poly[[[aqua(pyrazino[2,3- f ][1,10]phenanthroline-κ 2 N , N ′)copper(II)]-μ-isophthalato-κ 2 O : O ′] N , N -dimethylformamide solvate monohydrate]
暂无分享,去创建一个
In the title compound, {[Cu(C8H4O4)(C14H8N4)(H2O)]·C3H7NO·H2O}n, the CuII atom binds a water molecule and is chelated by the pyrazinophenanthroline N-heterocycle. It is also linked covalently to an isophthalate dianion that lies on a special position of site symmetry 2. The dianion serves as a spacer that connects adjacent square-pyramidal metal atoms into a zigzag chain propagating along the c axis of the orthorhombic unit cell. The chain motif is consolidated into a layer structure by hydrogen bonds involving both the coordinated and uncoordinated water molecules. The copper atom and the coordinated water molecule lie on a mirror plane, while the N-heterocycle, the disordered uncoordinated water molecule and the disordered dimethylformamide solvent molecule lie across a mirror plane.
[1] P. Cheng,et al. Synthesis and crystal structure of a terephthalato-bridged copper(II) complex [Cu2(tpt)(bpy)2(H2O)4] [Cu2(tpt)3 (bpy)2(H2O)2] , 2003 .
[2] Wenlian Li,et al. Hydrothermal Syntheses of Some Derivatives of Tetraazatriphenylene , 2006 .
[3] G. Guo,et al. Solvothermal synthesis and crystal structures of two new copper(II) terephthalates , 2003 .
[4] Q. J. Meng,et al. Dinuclear copper(II) complexes with different bridging connectors , 2003 .