Modeling and optimization of red currants vacuum drying process by response surface methodology (RSM).

Fresh red currants were dried by vacuum drying process under different drying conditions. Box-Behnken experimental design with response surface methodology was used for optimization of drying process in terms of physical (moisture content, water activity, total color change, firmness and rehydratation power) and chemical (total phenols, total flavonoids, monomeric anthocyanins and ascorbic acid content and antioxidant activity) properties of dried samples. Temperature (48-78 °C), pressure (30-330 mbar) and drying time (8-16 h) were investigated as independent variables. Experimental results were fitted to a second-order polynomial model where regression analysis and analysis of variance were used to determine model fitness and optimal drying conditions. The optimal conditions of simultaneously optimized responses were temperature of 70.2 °C, pressure of 39 mbar and drying time of 8 h. It could be concluded that vacuum drying provides samples with good physico-chemical properties, similar to lyophilized sample and better than conventionally dried sample.

[1]  José A. Fernández-López,et al.  DEPENDENCE BETWEEN APPARENT COLOR AND EXTRACTABLE COLOR IN PAPRIKA , 1999 .

[2]  K. Šavikin,et al.  Pomological and biochemical characterization of European currant berry (Ribes sp.) cultivars , 2014 .

[3]  N. Tepic,et al.  Optimization of frozen wild blueberry vacuum drying process , 2015 .

[4]  P. H. Santos,et al.  Retention of Vitamin C in Drying Processes of Fruits and Vegetables—A Review , 2008 .

[5]  A. Sienkiewicz,et al.  Antioxidative properties of vitamins C and E in micellar systems and in microemulsions , 2011 .

[6]  A. H. El-Sebae,et al.  The role of vitamin C as antioxidant in protection of oxidative stress induced by imidacloprid. , 2010, Food and chemical toxicology : an international journal published for the British Industrial Biological Research Association.

[7]  M. Planinić,et al.  Influence of process parameters and pre-treatments on quality and drying kinetics of apple samples. , 2018 .

[8]  S. Vidovic,et al.  Optimization of frozen sour cherries vacuum drying process. , 2013, Food chemistry.

[9]  Unisist,et al.  Vacuum freeze-drying, a method used to salvage water-damaged archival and library materials : a RAMP study with guidelines , 1987 .

[10]  H. Kunzek,et al.  Aspects of material science in food processing: changes in plant cell walls of fruits and vegetables , 1999 .

[11]  D. Kostić,et al.  Phenolic profile and antioxidant capacities of dried red currant from Serbia, extracted with different solvent , 2011 .

[12]  G. Diamantidis,et al.  Antioxidant capacity, phenol, anthocyanin and ascorbic acid contents in raspberries, blackberries, red currants, gooseberries and Cornelian cherries , 2007 .

[13]  U. S. Shivhare,et al.  Color Degradation Kinetics of Spinach, Mustard Leaves, and Mixed Puree , 2002 .

[14]  L. Rockland,et al.  Influence of water activity on food product quality and stability , 1980 .

[15]  P. Denev,et al.  Solid-phase extraction of berries’ anthocyanins and evaluation of their antioxidative properties , 2010 .

[16]  Douglas C. Montgomery,et al.  Response Surface Methodology: Process and Product Optimization Using Designed Experiments , 1995 .

[17]  Peter Eck,et al.  Vitamin C as an Antioxidant: Evaluation of Its Role in Disease Prevention , 2003, Journal of the American College of Nutrition.

[18]  Urszula Szymanowska,et al.  Anti-inflammatory and antioxidative activity of anthocyanins from purple basil leaves induced by selected abiotic elicitors. , 2015, Food chemistry.

[19]  A. Wojdyło,et al.  The influence of different the drying methods on chemical composition and antioxidant activity in chokeberries , 2016 .

[20]  M. Heinonen,et al.  Antioxidant activity of plant extracts containing phenolic compounds. , 1999, Journal of agricultural and food chemistry.

[21]  M. Bezerra,et al.  Response surface methodology (RSM) as a tool for optimization in analytical chemistry. , 2008, Talanta.

[22]  F. Lamb,et al.  Vacuum drying of small wood components at room temperature , 2001 .

[23]  A. Crozier,et al.  Identification of flavonoid and phenolic antioxidants in black currants, blueberries, raspberries, red currants, and cranberries. , 2010, Journal of agricultural and food chemistry.

[24]  Piotr P. Lewicki,et al.  Design of hot air drying for better foods , 2006 .

[25]  Robert H. Falk,et al.  Performance of fasteners in wood flour-thermoplastic composite panels , 2001 .

[26]  J. Harborne Methods of Plant Analysis , 1984 .

[27]  T. Yokota,et al.  Secondary Metabolites in Fruits, Vegetables, Beverages and Other Plant‐based Dietary Components , 2007 .

[28]  Ilknur Alibas,et al.  Energy Consumption and Colour Characteristics of Nettle Leaves during Microwave, Vacuum and Convective Drying , 2007 .

[29]  Deniz Baş,et al.  Modeling and optimization I: Usability of response surface methodology , 2007 .

[30]  G. Derringer,et al.  Simultaneous Optimization of Several Response Variables , 1980 .

[31]  V. L. Singleton,et al.  Colorimetry of Total Phenolics with Phosphomolybdic-Phosphotungstic Acid Reagents , 1965, American Journal of Enology and Viticulture.

[32]  J. Espín,et al.  Characterization of the total free radical scavenger capacity of vegetable oils and oil fractions using 2,2-diphenyl-1-picrylhydrazyl radical. , 2000, Journal of agricultural and food chemistry.

[33]  H. Rupasinghe,et al.  IMPACT OF DRYING PROCESSES ON BIOACTIVE PHENOLICS, VITAMIN C AND ANTIOXIDANT CAPACITY OF RED-FLESHED APPLE SLICES , 2011 .

[34]  B. Malaurie In vitro storage and safe international exchange of yam ( Dioscorea spp.) germplasm , 1998 .

[35]  F. Stampar,et al.  Changes in fruit quality parameters of four Ribes species during ripening. , 2015, Food chemistry.

[36]  M. Raimbault,et al.  General and microbiological aspects of solid substrate fermentation , 1998 .

[37]  M. Mupa,et al.  Anthocyanin content and antioxidant activities of common bean species (Phaseolus vulgaris L.) grown in Mashonaland Central, Zimbabwe , 2013 .

[38]  M. Mohamed,et al.  Phytochemicals and antioxidant activity of different parts of bambangan (Mangifera pajang) and tarap (Artocarpus odoratissimus) , 2009 .